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No Evidence for Passivation Effects of Na and K at Grain Boundaries in Polycrystalline Cu(In,Ga)Se2 Thin Films for Solar Cells

Journal Article · · Solar RRL
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  1. Helmholtz-Zentrum Berlin fur Materialien und Energie GmbH
  2. National Renewable Energy Laboratory (NREL), Golden, CO (United States)
  3. Martin-Luther-University Halle-Wittenberg

Thin-film solar cells based on Cu(In,Ga)Se2 (CIGSe) absorber layers reach conversion efficiencies of above 20%. One key to this success is the incorporation of alkali metals, such as Na and K, into the surface and the volume of the CIGSe thin film. The present work discusses the impact of Na and K on the grain-boundary (GB) properties in CIGSe thin films, i.e., on the barriers for charge carriers, ..phi..b, and on the recombination velocities at the GBs, sGB. First, the physics connected with these two quantities as well as their impact on the device performance are revised, and then the values for the barrier heights and recombination velocities are provided from the literature. The sGB values are measured by means of a cathodoluminescence analysis of Na-/K-free CIGSe layers as well as on CIGSe layers on Mo/sapphire substrates, which are submitted to only NaF or only KF postdeposition treatments. Overall, passivating effects on GBs by neither Na nor K can be confirmed. The GB recombination velocities seem to remain on the same order of magnitude, in average about 10^3-10^4 cm s^-1, irrespective of whether CIGSe thin films are Na-/K-free or Na-/K-containing.

Research Organization:
National Renewable Energy Laboratory (NREL), Golden, CO (United States)
Sponsoring Organization:
USDOE Office of Energy Efficiency and Renewable Energy (EERE)
DOE Contract Number:
AC36-08GO28308
OSTI ID:
1598130
Report Number(s):
NREL/JA-5K00-75990
Journal Information:
Solar RRL, Journal Name: Solar RRL Journal Issue: 8 Vol. 3
Country of Publication:
United States
Language:
English

References (36)

Compositional and electrical properties of line and planar defects in Cu(In,Ga)Se 2 thin films for solar cells - a review journal March 2016
Formation of a K—In—Se Surface Species by NaF/KF Postdeposition Treatment of Cu(In,Ga)Se 2 Thin-Film Solar Cell Absorbers journal January 2017
Numerical simulation of carrier collection and recombination at grain boundaries in Cu(In,Ga)Se2 solar cells journal May 2008
Formation reactions of chalcopyrite compounds and the role of sodium doping journal May 2007
Effects of heavy alkali elements in Cu(In,Ga)Se 2 solar cells with efficiencies up to 22.6% journal July 2016
Assessment of elemental distributions at line and planar defects in Cu(In,Ga)Se2 thin films by atom probe tomography journal April 2018
Kelvin probe force microscopy of semiconductor surface defects journal August 2004
Nanometer-scale electronic and microstructural properties of grain boundaries in Cu(In,Ga)Se2 journal August 2011
Confined and Chemically Flexible Grain Boundaries in Polycrystalline Compound Semiconductors journal May 2012
Grain-boundary character distribution and correlations with electrical and optoelectronic properties of CuInSe2 thin films journal October 2016
Influence of RbF post deposition treatment on heterojunction and grain boundaries in high efficient (21.1%) Cu(In,Ga)Se2 solar cells journal June 2019
The effect of Na on the electronic properties of Cu(In,Ga)Se 2 thin films: A local-probe study journal April 2016
Spatially Resolved Recombination Analysis of CuIn x Ga 1-x Se 2 Absorbers With Alkali Postdeposition Treatments journal November 2018
Electrically Benign Behavior of Grain Boundaries in Polycrystalline CuInSe 2 Films journal December 2007
The determination of grain‐boundary recombination rates by scanned spot excitation methods journal August 1982
Direct Insight into Grain Boundary Reconstruction in Polycrystalline Cu ( In , Ga ) Se 2 with Atomic Resolution journal February 2012
Dielectric constant of CuInSe2 by capacitance measurements journal January 1979
Deep surface Cu depletion induced by K in high-efficiency Cu(In,Ga)Se 2 solar cell absorbers
  • Donzel-Gargand, Olivier; Thersleff, Thomas; Keller, Jan
  • Progress in Photovoltaics: Research and Applications, Vol. 26, Issue 9 https://doi.org/10.1002/pip.3010
journal March 2018
Optical and electrical characterization of Cu(In,Ga)Se 2 thin film solar cells with varied absorber layer thickness journal February 2015
Influence of grain boundaries on current collection in Cu(In,Ga)Se2 thin-film solar cells journal February 2009
Identifying the Real Minority Carrier Lifetime in Nonideal Semiconductors: A Case Study of Kesterite Materials journal May 2017
Properties of electronic potential barriers at grain boundaries in Cu(In,Ga)Se 2 thin films journal November 2014
Unveiling the effects of post-deposition treatment with different alkaline elements on the electronic properties of CIGS thin film solar cells journal January 2014
Kelvin probe force microscopy for the nano scale characterization of chalcopyrite solar cell materials and devices journal May 2003
Effects of Sodium on Polycrystalline Cu(In,Ga)Se2 and Its Solar Cell Performance journal January 1998
Growth of Cu(In,Ga)Se 2 thin films by coevaporation using alkaline precursors journal February 2000
Na incorporation into Cu(In,Ga)Se2 for high-efficiency flexible solar cells on polymer foils journal April 2005
Elemental redistributions at structural defects in Cu(In,Ga)Se 2 thin films for solar cells journal November 2016
Measurement of minority-carrier lifetime by time-resolved photoluminescence journal March 1992
Effect of the KF post-deposition treatment on grain boundary properties in Cu(In, Ga)Se2 thin films journal January 2017
Review of grain interior, grain boundary, and interface effects of K in CIGS solar cells: Mechanisms for performance enhancement journal December 2017
Revealing the beneficial role of K in grain interiors, grain boundaries, and at the buffer interface for highly efficient CuInSe 2 solar cells
  • Muzzillo, Christopher P.; Poplawsky, Jonathan D.; Tong, Ho Ming
  • Progress in Photovoltaics: Research and Applications, Vol. 26, Issue 10 https://doi.org/10.1002/pip.3022
journal June 2018
Grain-boundary recombination in Cu(In,Ga)Se2 solar cells journal December 2005
The electrical properties of polycrystalline silicon films journal December 1975
Diffusion of sodium in single crystal CuInSe 2 journal June 2017
A contactless method for measuring the recombination velocity of an individual grain boundary in thin-film photovoltaics journal August 2010

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