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Solid-state NMR experiments have been developed to probe crystallization behavior fluoropolymers (Progress Summary)

Technical Report ·
DOI:https://doi.org/10.2172/1557035· OSTI ID:1557035
 [1]
  1. Lawrence Livermore National Laboratory (LLNL), Livermore, CA (United States)
The FK-800 fluoropolymer elastomer is being developed as a replacement material for the Kel-F 800 binder in the plastic bonded explosive PBX-9502. These polymers are a random co-polymer of poly-vinylidene fluoride (PVDF) and poly-chlorotrifluoroetheylene (PCTFE) in nominal 1:3 ratio. Initial characterizations of the FK-800 replacement show similar characteristics as the legacy Kel-F 800. However, differences in bulk crystallinity and crystallization kinetics have been observed. These differences may be driven by small differences in the distribution of the monomers on the polymer backbone (sequence distribution).
Research Organization:
Lawrence Livermore National Laboratory (LLNL), Livermore, CA (United States)
Sponsoring Organization:
USDOE National Nuclear Security Administration (NNSA)
DOE Contract Number:
AC52-07NA27344
OSTI ID:
1557035
Report Number(s):
LLNL--TR-785030; 977026
Country of Publication:
United States
Language:
English