Two mechanisms of nanoparticle generation in picosecond laser ablation in liquids: the origin of the bimodal size distribution

Shih, Cheng-Yu; Streubel, René; Heberle, Johannes; Letzel, Alexander; Shugaev, Maxim V.; Wu, Chengping; Schmidt, Michael; Gökce, Bilal; Barcikowski, Stephan; Zhigilei, Leonid V.

doi:10.1039/C7NR08614H

Title: Two mechanisms of nanoparticle generation in picosecond laser ablation in liquids: the origin of the bimodal size distribution

Journal Article · Thu Mar 08 00:00:00 EST 2018 · Nanoscale

DOI:https://doi.org/10.1039/C7NR08614H· OSTI ID:1510258

Shih, Cheng-Yu ^[1]; Streubel, René ^[2]; Heberle, Johannes ^[3]; Letzel, Alexander ^[2]; Shugaev, Maxim V. ^[1];

^[1]; Schmidt, Michael ^[3];

^[2];

^[1]

Univ. of Virginia, Charlottesville, VA (United States). Dept. of Materials Science and Engineering
Univ. of Duisburg-Essen, Essen (Germany). Technical Chemistry I and Center for Nanointegration Duisburg-Essen (CENIDE)
Friedrich-Alexander Univ. Erlangen-Nürnberg, Erlangen (Germany). Inst. of Photonic Technologies

The synthesis of chemically clean and environmentally friendly nanoparticles through pulsed laser ablation in liquids has shown a number of advantages over conventional chemical synthesis methods and has evolved into a thriving research field attracting laboratory and industrial applications. The fundamental understanding of processes leading to the nanoparticle generation, however, still remains elusive. In particular, the origin of bimodal nanoparticle size distributions in femto- and picosecond laser ablation in liquids, where small nanoparticles (several nanometers) with narrow size distribution are commonly observed to coexist with larger (tens to hundreds of nanometers) ones, has not been explained so far. In this paper, joint computational and experimental efforts are applied to understand the mechanisms of nanoparticle formation in picosecond laser ablation in liquids and to explain the bimodal nanoparticle size distributions. The results of a large-scale atomistic simulation reveal the critical role of the dynamic interaction between the ablation plume and the liquid environment, leading to the generation of large nanoparticles through a sequence of hydrodynamic instabilities at the plume-liquid interface and a concurrent nucleation and growth of small nanoparticles in an expanding metal-liquid mixing region. The computational predictions are supported by a series of stroboscopic videography experiments showing the emergence of small satellite bubbles surrounding the main cavitation bubble generated in single pulse experiments. Lastly, carefully timed double pulse irradiation triggers expansion of secondary cavitation bubbles indicating, in accord with the simulation results, the presence of localized sites of laser energy deposition (possibly large nanoparticles) injected into the liquid at the early stage of the bubble formation.

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Research Organization:: Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States). Oak Ridge Leadership Computing Facility (OLCF)

Sponsoring Organization:: USDOE Office of Science (SC)

Grant/Contract Number:: DMR-1610936; CMMI-1663429

OSTI ID:: 1510258

Journal Information:: Nanoscale, Vol. 10, Issue 15; ISSN 2040-3364

Publisher:: Royal Society of ChemistryCopyright Statement

Country of Publication:: United States

Language:: English

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Cited by: 141 works

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36 MATERIALS SCIENCE
37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY

Title: Two mechanisms of nanoparticle generation in picosecond laser ablation in liquids: the origin of the bimodal size distribution

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