Skip to main content
U.S. Department of Energy
Office of Scientific and Technical Information

A Tale of Two Trimers from Two Different Worlds: A COF-Inspired Synthetic Strategy for Pore-Space Partitioning of MOFs

Journal Article · · Angewandte Chemie (International Edition)
 [1];  [2];  [3];  [3];  [4];  [4];  [5];  [2]
  1. Univ. of California, Riverside, CA (United States); UC Riverside
  2. Univ. of California, Riverside, CA (United States)
  3. California State Univ. (CalState), Long Beach, CA (United States)
  4. Univ. of California, Riverside, CA (United States); Taiyuan Univ. of Technology (China)
  5. Taiyuan Univ. of Technology (China)

The introduction of a symmetry- and size-matching pore-partitioning agent in the form of either a molecular ligand, such as 2,4,6-tri(4-pyridinyl)-1,3,5-triazine (tpt), or a metal-complex cluster, into the hexagonal channels of MIL-88/MOF-235-type (the acs net) to create pacs-type (partitioned acs) crystalline porous materials is an effective strategy to develop high-performance gas adsorbents. We have developed here an integrated COF–MOF coassembly strategy as a new method for pore-space partitioning through the coassembly of [(M3(OH)1-x(O)x(COO)6] MOF-type and [B3O3(py)3] COF-type trimers. With this strategy, the coordination-driven assembly of the acs framework occurred concurrently and synergistically with the COF-1-type condensation of pyridine-4-boronic acid into a C3-symmetric trimeric boroxine molecule. Furthermore, the resulting boroxine-based pacs materials exhibited dramatically enhanced gas-sorption properties as compared to nonpartitioned acs-type materials and are among the most efficient NH3-sorption materials

Research Organization:
Univ. of California, Riverside, CA (United States)
Sponsoring Organization:
USDOE Office of Science (SC), Basic Energy Sciences (BES) (SC-22). Materials Sciences & Engineering Division
Grant/Contract Number:
SC0010596
OSTI ID:
1596459
Alternate ID(s):
OSTI ID: 1504511
Journal Information:
Angewandte Chemie (International Edition), Journal Name: Angewandte Chemie (International Edition) Journal Issue: 19 Vol. 58; ISSN 1433-7851
Publisher:
WileyCopyright Statement
Country of Publication:
United States
Language:
English

References (67)

Targeted Synthesis of Porous Aromatic Frameworks and their Composites for Versatile, Facile, Efficacious, and Durable Antibacterial Polymer Coatings journal September 2013
Metal-Organic Frameworks as Platforms for Catalytic Applications journal November 2017
Acid and Base Resistant Zirconium Polyphenolate-Metalloporphyrin Scaffolds for Efficient CO 2 Photoreduction journal November 2017
Metal-Organic Frameworks for Separation journal March 2018
A Route to the Synthesis of Trivalent Transition-Metal Porous Carboxylates with Trimeric Secondary Building Units journal September 2004
Gasspeicherung in nanoporösen Materialien journal June 2008
Ionothermalsynthese von porösen kovalenten Triazin- Polymernetzwerken journal April 2008
Targeted Synthesis of a Porous Aromatic Framework with High Stability and Exceptionally High Surface Area journal November 2009
3D Microporous Base-Functionalized Covalent Organic Frameworks for Size-Selective Catalysis journal February 2014
Porous Solids Arising from Synergistic and Competing Modes of Assembly: Combining Coordination Chemistry and Covalent Bond Formation journal February 2015
In Situ Modification of Metal-Organic Frameworks in Mixed-Matrix Membranes journal June 2015
A Metal-Organic Framework with Exceptional Activity for C−H Bond Amination journal December 2017
Exploring the Performance Improvement of the Oxygen Evolution Reaction in a Stable Bimetal-Organic Framework System journal May 2018
Rational Design of MOF/COF Hybrid Materials for Photocatalytic H 2 Evolution in the Presence of Sacrificial Electron Donors journal August 2018
Ammonia Storage by Reversible Host-Guest Site Exchange in a Robust Metal-Organic Framework journal October 2018
A Route to the Synthesis of Trivalent Transition-Metal Porous Carboxylates with Trimeric Secondary Building Units journal September 2004
Gas Storage in Nanoporous Materials journal June 2008
Porous, Covalent Triazine-Based Frameworks Prepared by Ionothermal Synthesis journal April 2008
Targeted Synthesis of a Porous Aromatic Framework with High Stability and Exceptionally High Surface Area journal November 2009
3D Microporous Base-Functionalized Covalent Organic Frameworks for Size-Selective Catalysis journal February 2014
Porous Solids Arising from Synergistic and Competing Modes of Assembly: Combining Coordination Chemistry and Covalent Bond Formation journal February 2015
In Situ Modification of Metal-Organic Frameworks in Mixed-Matrix Membranes journal June 2015
A Metal-Organic Framework with Exceptional Activity for C−H Bond Amination journal December 2017
Exploring the Performance Improvement of the Oxygen Evolution Reaction in a Stable Bimetal-Organic Framework System journal May 2018
Rational Design of MOF/COF Hybrid Materials for Photocatalytic H 2 Evolution in the Presence of Sacrificial Electron Donors journal August 2018
Ammonia Storage by Reversible Host-Guest Site Exchange in a Robust Metal-Organic Framework journal October 2018
Chemistry of Covalent Organic Frameworks journal November 2015
Pore Space Partition in Metal–Organic Frameworks journal January 2017
Bimetallic Metal–Organic Frameworks for Gas Storage and Separation journal March 2017
Site Partition: Turning One Site into Two for Adsorbing CO 2 journal June 2016
Hierarchical Porous and High Surface Area Tubular Carbon as Dye Adsorbent and Capacitor Electrode journal May 2015
Introduction to Metal–Organic Frameworks journal September 2011
Metal-Organic Frameworks Based on Trigonal Prismatic Building Blocks and the New “acs” Topology journal May 2005
Very Large Swelling in Hybrid Frameworks:  A Combined Computational and Powder Diffraction Study journal November 2005
Reticular Synthesis of Microporous and Mesoporous 2D Covalent Organic Frameworks
  • Côté, Adrien P.; El-Kaderi, Hani M.; Furukawa, Hiroyasu
  • Journal of the American Chemical Society, Vol. 129, Issue 43, p. 12914-12915 https://doi.org/10.1021/ja0751781
journal October 2007
Tuning MOF CO 2 Adsorption Properties via Cation Exchange journal April 2010
Construction of Crystalline 2D Covalent Organic Frameworks with Remarkable Chemical (Acid/Base) Stability via a Combined Reversible and Irreversible Route journal November 2012
Entrapment of Metal Clusters in Metal–Organic Framework Channels by Extended Hooks Anchored at Open Metal Sites journal May 2013
An Azine-Linked Covalent Organic Framework journal November 2013
Pore Space Partition by Symmetry-Matching Regulated Ligand Insertion and Dramatic Tuning on Carbon Dioxide Uptake journal January 2015
Metalation of a Thiocatechol-Functionalized Zr(IV)-Based Metal–Organic Framework for Selective C–H Functionalization journal February 2015
A Crystalline Imine-Linked 3-D Porous Covalent Organic Framework
  • Uribe-Romo, Fernando J.; Hunt, Joseph R.; Furukawa, Hiroyasu
  • Journal of the American Chemical Society, Vol. 131, Issue 13, p. 4570-4571 https://doi.org/10.1021/ja8096256
journal April 2009
Photocatalytic Metal–Organic Frameworks for Selective 2,2,2-Trifluoroethylation of Styrenes journal September 2016
Multivariable Modular Design of Pore Space Partition journal November 2016
Water-Soluble and Ultrastable Ti 4 L 6 Tetrahedron with Coordination Assembly Function journal November 2017
Controlled Gas Uptake in Metal–Organic Frameworks with Record Ammonia Sorption journal February 2018
Creating Well-Defined Hexabenzocoronene in Zirconium Metal–Organic Framework by Postsynthetic Annulation journal January 2019
Protecting group and switchable pore-discriminating adsorption properties of a hydrophilic–hydrophobic metal–organic framework journal March 2011
An ultra-tunable platform for molecular engineering of high-performance crystalline porous materials journal December 2016
Engineering chiral porous metal-organic frameworks for enantioselective adsorption and separation journal July 2014
Designed synthesis of large-pore crystalline polyimide covalent organic frameworks journal July 2014
Coordination templated [2+2+2] cyclotrimerization in a porous coordination framework journal September 2015
Boroxine chemistry and applications: A perspective journal January 2010
Boronic acid building blocks: tools for self assembly journal January 2011
Covalent organic frameworks (COFs): from design to applications journal January 2013
A hydrazone-based covalent organic framework for photocatalytic hydrogen production journal January 2014
Liquid-phase epitaxial growth of a homochiral MOF thin film on poly( l -DOPA) functionalized substrate for improved enantiomer separation journal January 2016
Porphyrinic coordination lattices with fluoropillars journal January 2017
A new strategy for constructing a disulfide-functionalized ZIF-8 analogue using structure-directing ligand–ligand covalent interaction journal January 2018
Recent progress in covalent organic framework thin films: fabrications, applications and perspectives journal January 2019
Targeted synthesis of a porous borazine-linked covalent organic framework journal January 2012
Systematic Design of Pore Size and Functionality in Isoreticular MOFs and Their Application in Methane Storage journal January 2002
Porous, Crystalline, Covalent Organic Frameworks journal November 2005
Designed Synthesis of 3D Covalent Organic Frameworks journal April 2007
Pore chemistry and size control in hybrid porous materials for acetylene capture from ethylene journal May 2016
Ethane/ethylene separation in a metal-organic framework with iron-peroxo sites journal October 2018
A Hydrazone-based Covalent Organic Framework for Photocatalytic Hydrogen Production preprint January 2014

Cited By (3)

A Dual Threat: Redox‐Activity and Electronic Structures of Well‐Defined Donor–Acceptor Fulleretic Covalent‐Organic Materials journal February 2020
A Dual Threat: Redox‐Activity and Electronic Structures of Well‐Defined Donor–Acceptor Fulleretic Covalent‐Organic Materials journal February 2020
Adjustment of the performance and stability of isostructural zeolitic tetrazolate-imidazolate frameworks journal January 2020


Similar Records

A Tale of Two Trimers from Two Different Worlds: A COF‐Inspired Synthetic Strategy for Pore‐Space Partitioning of MOFs
Journal Article · Tue Apr 02 00:00:00 EDT 2019 · Angewandte Chemie · OSTI ID:1504507

A Strategy for Constructing Pore-Space-Partitioned MOFs with High Uptake Capacity for C2 Hydrocarbons and CO2
Journal Article · Wed Aug 26 00:00:00 EDT 2020 · Angewandte Chemie (International Edition) · OSTI ID:1755101