Exceptional energy and new insight with a sodium–selenium battery based on a carbon nanosheet cathode and a pseudographite anode

Ding, Jia; Zhou, Hui; Zhang, Hanlei; Stephenson, Tyler; Li, Zhi; Karpuzov, Dimitre; Mitlin, David

doi:10.1039/C6EE02274J

Title: Exceptional energy and new insight with a sodium–selenium battery based on a carbon nanosheet cathode and a pseudographite anode

Journal Article · Thu Sep 29 00:00:00 EDT 2016 · Energy & Environmental Science

DOI:https://doi.org/10.1039/C6EE02274J· OSTI ID:1470247

Ding, Jia ^[1]; Zhou, Hui ^[2]; Zhang, Hanlei ^[2]; Stephenson, Tyler ^[3]; Li, Zhi ^[3]; Karpuzov, Dimitre ^[4]; Mitlin, David ^[5]

Univ. of Alberta, Edmonton, AB (Canada). Chemical and Materials Engineering; State Univ. of New York (SUNY), Binghamton, NY (United States). NorthEast Center for Chemical Energy Storage
State Univ. of New York (SUNY), Binghamton, NY (United States). NorthEast Center for Chemical Energy Storage
Univ. of Alberta, Edmonton, AB (Canada). Chemical and Materials Engineering
Univ. of Alberta, Edmonton, AB (Canada). Alberta Center for Surface Engineering and Science (ACSES)
Clarkson Univ., Potsdam, NY (United States). Chemical & Biomolecular Engineering

We created a unique sodium ion battery (NIB, SIB) cathode based on selenium in cellulose-derived carbon nanosheets (CCNs), termed Se-CCN. The elastically compliant two-dimensional CCN host incorporates a high mass loading of amorphous Se (53 wt%), which is primarily impregnated into 1 cm³ g^-1 nanopores. The results in facile sodiation kinetics due to short solid-state diffusion distances and a large charge transfer area of the nanosheets were established. The architecture also leads to an intrinsic resistance to polyselenide shuttle and to disintegration/coarsening. As a Na half-cell, the Se-CCN cathode delivers a reversible capacity of 613 mA h g^-1 with 88% retention over 500 cycles. The exceptional stability is achieved by using a standard electrolyte (1 M NaClO4 EC-DMC) without secondary additives or high salt concentrations. The rate capability is also superb, achieving 300 mA h g^-1 at 10C. Compared to recent state-of-the-art literature, the Se-CCN is the most cyclically stable and offers the highest rate performance. As a Se–Na battery, the system achieves 992 W h kg^-1 at 68 W kg^-1 and 384 W h kg^-1 at 10144 W kg^-1 (by active mass in a cathode). We are the first to fabricate and test a Se-based full NIB, which is based on Se-CCN coupled to a Na intercalating pseudographitic carbon (PGC) anode. It is demonstrated that the PGC anode increases its structural order in addition to dilating as a result of Na intercalation at voltages below 0.2 V vs. Na/Na+. The {110} Na reflections are distinctly absent from the XRD patterns of PGC sodiated down to 0.001 V, indicating that the Na metal pore filling is not significant for pseudographitic carbons. Lastly, the battery delivers highly promising Ragone chart characteristics, for example yielding 203 and 50 W h kg^-1 at 70 and 14 000 W kg^-1 (via total material mass in the anode and cathode).

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Research Organization:: Energy Frontier Research Centers (EFRC) (United States). Northeastern Center for Chemical Energy Storage (NECCES)

Sponsoring Organization:: USDOE Office of Science (SC), Basic Energy Sciences (BES)

Grant/Contract Number:: SC0001294

OSTI ID:: 1470247

Journal Information:: Energy & Environmental Science, Vol. 10, Issue 1; Related Information: NECCES partners with Stony Brook University (lead); Argonne National Laboratory; Binghamton University; Brookhaven National University; University of California, San Diego; University of Cambridge, UK; Lawrence Berkeley National Laboratory; Massachusetts Institute of Technology; University of Michigan; Rutgers University; ISSN 1754-5692

Publisher:: Royal Society of ChemistryCopyright Statement

Country of Publication:: United States

Language:: English

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Cited by: 163 works

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Porous Amorphous FePO ₄ Nanoparticles Connected by Single-Wall Carbon Nanotubes for Sodium Ion Battery Cathodes Liu, Yonglin; Xu, Yunhua; Han, Xiaogang Nano Letters, Vol. 12, Issue 11 https://doi.org/10.1021/nl302819f	journal	October 2012
Insight into the Electrode Mechanism in Lithium-Sulfur Batteries with Ordered Microporous Carbon Confined Sulfur as the Cathode Li, Zhen; Yuan, Lixia; Yi, Ziqi Advanced Energy Materials, Vol. 4, Issue 7 https://doi.org/10.1002/aenm.201301473	journal	November 2013
Nanoflake-Assembled Hierarchical Na ₃ V ₂ (PO ₄ ) ₃ /C Microflowers: Superior Li Storage Performance and Insertion/Extraction Mechanism An, Qinyou; Xiong, Fangyu; Wei, Qiulong Advanced Energy Materials, Vol. 5, Issue 10 https://doi.org/10.1002/aenm.201401963	journal	February 2015
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Strong Lithium Polysulfide Chemisorption on Electroactive Sites of Nitrogen-Doped Carbon Composites For High-Performance Lithium-Sulfur Battery Cathodes Song, Jiangxuan; Gordin, Mikhail L.; Xu, Terrence Angewandte Chemie International Edition, Vol. 54, Issue 14 https://doi.org/10.1002/anie.201411109	journal	February 2015
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Multiple heterointerfaces boosted de-/sodiation kinetics towards superior Na storage and Na-Ion full battery Wang, Ying-Ying; Hou, Bao-Hua; Wang, Ya-Nan Journal of Materials Chemistry A, Vol. 6, Issue 15 https://doi.org/10.1039/c8ta01132j	journal	January 2018
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