Eliminating the non-Gaussian spectral response of X-ray absorbers for transition-edge sensors

Divan, Ralu; Gades, Lisa M.; Kenesei, Peter; Madden, Timothy J.; Miceli, Antonino; Park, Jun-Sang; Patel, Umeshkumar M.; Quaranta, Orlando; Sharma, Hemant; Bennett, Douglas A.; Doriese, William B.; Fowler, Joseph W.; Gard, Johnathon D.; Hays-Wehle, James P.; Morgan, Kelsey M.; Schmidt, Daniel R.; Swetz, Daniel S.; Ullom, Joel N.

doi:10.1063/1.5001198

Title: Eliminating the non-Gaussian spectral response of X-ray absorbers for transition-edge sensors

Journal Article · Wed Nov 08 00:00:00 EST 2017 · Applied Physics Letters

DOI:https://doi.org/10.1063/1.5001198· OSTI ID:1412693

Divan, Ralu ^[1]; Gades, Lisa M. ^[2]; Kenesei, Peter ^[2]; Madden, Timothy J. ^[2]; Miceli, Antonino ^[2]; Park, Jun-Sang ^[2];

^[2];

^[1]; Sharma, Hemant ^[2];

^[3]; Doriese, William B. ^[3]; Fowler, Joseph W. ^[3]; Gard, Johnathon D. ^[4]; Hays-Wehle, James P. ^[3];

^[4]; Schmidt, Daniel R. ^[3];

^[3]; Ullom, Joel N. ^[4]

Argonne National Lab. (ANL), Argonne, IL (United States); Northwestern Univ., Evanston, IL (United States)
Argonne National Lab. (ANL), Argonne, IL (United States)
National Inst. of Standards and Technology (NIST), Boulder, CO (United States)
National Inst. of Standards and Technology (NIST), Boulder, CO (United States); Univ. of Colorado, Boulder, CO (United States)

Transition-edge sensors (TESs) as microcalorimeters for high-energy-resolution X-ray spectroscopy are often fabricated with an absorber made of materials with high Z (for X-ray stopping power) and low heat capacity (for high resolving power). Bismuth represents one of the most compelling options. TESs with evaporated bismuth absorbers have shown spectra with undesirable and unexplained low-energy tails. We have developed TESs with electroplated bismuth absorbers over a gold layer that are not afflicted by this problem and that retain the other positive aspects of this material. To better understand these phenomena, we have studied a series of TESs with gold, gold/evaporated bismuth, and gold/electroplated bismuth absorbers, fabricated on the same die with identical thermal coupling. Lastly, we show that the bismuth morphology is linked to the spectral response of X-ray TES microcalorimeters.

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Research Organization:: Argonne National Laboratory (ANL), Argonne, IL (United States)

Sponsoring Organization:: USDOE Office of Science (SC), Basic Energy Sciences (BES). Scientific User Facilities Division

Grant/Contract Number:: AC02-06CH11357

OSTI ID:: 1412693

Alternate ID(s):: OSTI ID: 1408056

Journal Information:: Applied Physics Letters, Vol. 111, Issue 19; ISSN 0003-6951

Publisher:: American Institute of Physics (AIP)Copyright Statement

Country of Publication:: United States

Language:: English

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Cited by: 30 works

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References (25)

Optimized transition-edge x-ray microcalorimeter with 2.4eV energy resolution at 5.9keV Ullom, J. N.; Beall, J. A.; Doriese, W. B. Applied Physics Letters, Vol. 87, Issue 19 https://doi.org/10.1063/1.2061865	journal	November 2005
Optimizing detector geometry for trace element mapping by X-ray fluorescence Sun, Yue; Gleber, Sophie-Charlotte; Jacobsen, Chris Ultramicroscopy, Vol. 152 https://doi.org/10.1016/j.ultramic.2014.12.014	journal	May 2015
Performance of TES X-ray Microcalorimeters with a Novel Absorber Design Bandler, S. R.; Brekosky, R. P.; Brown, A. -D. Journal of Low Temperature Physics, Vol. 151, Issue 1-2 https://doi.org/10.1007/s10909-007-9673-6	journal	January 2008
Development of Thick Electroplated Bismuth Absorbers for Large Collection Area Hard X-ray Transition Edge Sensors Gades, Lisa M.; Cecil, Thomas W.; Divan, Ralu IEEE Transactions on Applied Superconductivity, Vol. 27, Issue 4 https://doi.org/10.1109/TASC.2017.2662007	journal	June 2017
A reassessment of absolute energies of the x-ray L lines of lanthanide metals Fowler, J. W.; Alpert, B. K.; Bennett, D. A. Metrologia, Vol. 54, Issue 4 https://doi.org/10.1088/1681-7575/aa722f	journal	June 2017
$K α_{1, 2}$ and $K β_{1, 3}$ x-ray emission lines of the $3 d$ transition metals Hölzer, G.; Fritsch, M.; Deutsch, M. Physical Review A, Vol. 56, Issue 6 https://doi.org/10.1103/PhysRevA.56.4554	journal	December 1997
The Scherrer Formula for X-Ray Particle Size Determination Patterson, A. L. Physical Review, Vol. 56, Issue 10 https://doi.org/10.1103/PhysRev.56.978	journal	November 1939
A fast methodology to determine the characteristics of thousands of grains using three-dimensional X-ray diffraction. II. Volume, centre-of-mass position, crystallographic orientation and strain state of grains Sharma, Hemant; Huizenga, Richard M.; Offerman, S. Erik Journal of Applied Crystallography, Vol. 45, Issue 4 https://doi.org/10.1107/S0021889812025599	journal	July 2012
High-energy diffraction microscopy at the advanced photon source Lienert, U.; Li, S. F.; Hefferan, C. M. JOM, Vol. 63, Issue 7 https://doi.org/10.1007/s11837-011-0116-0	journal	July 2011
Nanoscale Hard X-Ray Microscopy Methods for Materials Studies Holt, Martin; Harder, Ross; Winarski, Robert Annual Review of Materials Research, Vol. 43, Issue 1 https://doi.org/10.1146/annurev-matsci-071312-121654	journal	July 2013
Energy Down-Conversion and Thermalization in Metal Absorbers Kozorezov, A. Journal of Low Temperature Physics, Vol. 167, Issue 3-4 https://doi.org/10.1007/s10909-011-0426-1	journal	November 2011
Thermalization of X-rays in evaporated tin and bismuth films used as the absorbing materials in X-ray calorimeters Stahle, C. K.; Kelley, R. L.; Moseley, S. H. Journal of Low Temperature Physics, Vol. 93, Issue 3-4 https://doi.org/10.1007/BF00693429	journal	November 1993
The Practice of Pulse Processing Fowler, J. W.; Alpert, B. K.; Doriese, W. B. Journal of Low Temperature Physics, Vol. 184, Issue 1-2 https://doi.org/10.1007/s10909-015-1380-0	journal	December 2015
An analytic formula for the extrapolated range of electrons in condensed materials Tabata, Tatsuo; Andreo, Pedro; Shinoda, Kunihiko Nuclear Instruments and Methods in Physics Research Section B: Beam Interactions with Materials and Atoms, Vol. 119, Issue 4 https://doi.org/10.1016/S0168-583X(96)00687-8	journal	December 1996
Thermal conductivity of tin-doped bismuth between 50 mK and 7K Uher, C.; Heremans, J.; Issi, J. -P Journal of Physics C: Solid State Physics, Vol. 18, Issue 15 https://doi.org/10.1088/0022-3719/18/15/010	journal	May 1985
High-density arrays of x-ray microcalorimeters for Constellation-X Kilbourne, Caroline A.; Bandler, Simon R.; Brown, Ari D. SPIE Astronomical Telescopes + Instrumentation, SPIE Proceedings https://doi.org/10.1117/12.672419	conference	July 2006
Theoretical investigation of thermoelectric transport properties of cylindrical Bi nanowires Lin, Yu-Ming; Sun, Xiangzhong; Dresselhaus1,2, M. S. Physical Review B, Vol. 62, Issue 7 https://doi.org/10.1103/PhysRevB.62.4610	journal	August 2000
On the size of the secondary electron cloud in crystals irradiated by hard X-ray photons Grum-Grzhimailo, Alexei N.; Pikuz, Tatiana; Faenov, Anatoly The European Physical Journal D, Vol. 71, Issue 3 https://doi.org/10.1140/epjd/e2017-70767-8	journal	March 2017
Transport properties of Bi nanowire arrays Lin, Yu-Ming; Cronin, Stephen B.; Ying, Jackie Y. Applied Physics Letters, Vol. 76, Issue 26 https://doi.org/10.1063/1.126829	journal	June 2000
Large Magnetoresistance of Electrodeposited Single-Crystal Bismuth Thin Films Yang, F. Y. Science, Vol. 284, Issue 5418 https://doi.org/10.1126/science.284.5418.1335	journal	May 1999
Semimetal-to-semiconductor transition in bismuth thin films Hoffman, C. A.; Meyer, J. R.; Bartoli, F. J. Physical Review B, Vol. 48, Issue 15 https://doi.org/10.1103/PhysRevB.48.11431	journal	October 1993
Absolute Energy Calibration of X-ray TESs with 0.04 eV Uncertainty at 6.4 keV in a Hadron-Beam Environment Tatsuno, H.; Doriese, W. B.; Bennett, D. A. Journal of Low Temperature Physics, Vol. 184, Issue 3-4 https://doi.org/10.1007/s10909-016-1491-2	journal	January 2016
A practical superconducting-microcalorimeter X-ray spectrometer for beamline and laboratory science Doriese, W. B.; Abbamonte, P.; Alpert, B. K. Review of Scientific Instruments, Vol. 88, Issue 5 https://doi.org/10.1063/1.4983316	journal	May 2017
Discovery of Amorphous Iron Hydrides via Novel Quiescent Reaction in Aqueous Solution Taguchi, Kohei; Shinozaki, Kazuteru; Okumura, Hideyuki Scientific Reports, Vol. 10, Issue 1 https://doi.org/10.1038/s41598-020-63124-2	journal	April 2020
Performance Evaluation of the Cost-Effective and Lightweight Alphasense Optical Particle Counter for use Onboard Unmanned Aerial Vehicles Bezantakos, S.; Schmidt-Ott, F.; Biskos, G. Taylor & Francis https://doi.org/10.6084/m9.figshare.5660497.v1	text	January 2017

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Heavy ion induced Ti X-ray satellite structure for Ti, TiN, and TiO ₂ thin films Käyhkö, Marko; Palosaari, Mikko R. J.; Laitinen, Mikko X-Ray Spectrometry, Vol. 47, Issue 6 https://doi.org/10.1002/xrs.2976	journal	September 2018
Characterization of High Aspect-Ratio TiAu TES X-ray Microcalorimeter Array Under AC Bias Taralli, E.; Gottardi, L.; Nagayoshi, K. Journal of Low Temperature Physics, Vol. 199, Issue 1-2 https://doi.org/10.1007/s10909-019-02254-y	journal	November 2019
On Low-Energy Tail Distortions in the Detector Response Function of X-Ray Microcalorimeter Spectrometers O’Neil, G. C.; Szypryt, P.; Takacs, E. Journal of Low Temperature Physics, Vol. 199, Issue 3-4 https://doi.org/10.1007/s10909-019-02270-y	journal	November 2019
A transition-edge sensor-based x-ray spectrometer for the study of highly charged ions at the National Institute of Standards and Technology electron beam ion trap Szypryt, P.; O’Neil, G. C.; Takacs, E. Review of Scientific Instruments, Vol. 90, Issue 12 https://doi.org/10.1063/1.5116717	journal	December 2019
Soft X-ray spectroscopy with transition-edge sensors at Stanford Synchrotron Radiation Lightsource beamline 10-1 Lee, Sang-Jun; Titus, Charles J.; Alonso Mori, Roberto Review of Scientific Instruments, Vol. 90, Issue 11 https://doi.org/10.1063/1.5119155	journal	November 2019
A Transition-edge Sensor-based X-ray Spectrometer for the Study of Highly Charged Ions at the National Institute of Standards and Technology Electron Beam Ion Trap Szypryt, P.; O'Neil, G. C.; Takacs, E. arXiv https://doi.org/10.48550/arxiv.2005.05483	text	January 2020

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