Highly compressible 3D periodic graphene aerogel microlattices

Zhu, Cheng; Han, T. Yong-Jin; Duoss, Eric B.; Golobic, Alexandra M.; Kuntz, Joshua D.; Spadaccini, Christopher M.; Worsley, Marcus A.

doi:10.1038/ncomms7962

Highly compressible 3D periodic graphene aerogel microlattices

Journal Article · Wed Apr 22 00:00:00 EDT 2015 · Nature Communications

DOI:https://doi.org/10.1038/ncomms7962· OSTI ID:1259507

Zhu, Cheng ^[1]; Han, T. Yong-Jin ^[1]; Duoss, Eric B. ^[1]; Golobic, Alexandra M. ^[1]; Kuntz, Joshua D. ^[1]; Spadaccini, Christopher M. ^[1]; ^[1]

Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States)

Graphene is a two-dimensional material that offers a unique combination of low density, exceptional mechanical properties, large surface area and excellent electrical conductivity. Recent progress has produced bulk 3D assemblies of graphene, such as graphene aerogels, but they possess purely stochastic porous networks, which limit their performance compared with the potential of an engineered architecture. Here we report the fabrication of periodic graphene aerogel microlattices, possessing an engineered architecture via a 3D printing technique known as direct ink writing. The 3D printed graphene aerogels are lightweight, highly conductive and exhibit supercompressibility (up to 90% compressive strain). Moreover, the Young’s moduli of the 3D printed graphene aerogels show an order of magnitude improvement over bulk graphene materials with comparable geometric density and possess large surface areas. Ultimately, adapting the 3D printing technique to graphene aerogels realizes the possibility of fabricating a myriad of complex aerogel architectures for a broad range of applications.

View Accepted Manuscript (DOE)

Research Organization:: Lawrence Livermore National Laboratory (LLNL), Livermore, CA (United States)

Sponsoring Organization:: USDOE Laboratory Directed Research and Development (LDRD) Program

Grant/Contract Number:: AC52-07NA27344

OSTI ID:: 1259507

Alternate ID(s):: OSTI ID: 1410001

Report Number(s):: LLNL-JRNL--665510; ncomms7962

Journal Information:: Nature Communications, Journal Name: Nature Communications Vol. 6; ISSN 2041-1723

Publisher:: Nature Publishing GroupCopyright Statement

Country of Publication:: United States

Language:: English

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3D-Printed, All-in-One Evaporator for High-Efficiency Solar Steam Generation under 1 Sun Illumination Li, Yiju; Gao, Tingting; Yang, Zhi Advanced Materials, Vol. 29, Issue 26 https://doi.org/10.1002/adma.201700981	journal	May 2017
Extremely Low Density and Super‐Compressible Graphene Cellular Materials Qiu, Ling; Huang, Bing; He, Zijun Advanced Materials, Vol. 29, Issue 36 https://doi.org/10.1002/adma.201701553	journal	July 2017
Extrusion-Based 3D Printing of Hierarchically Porous Advanced Battery Electrodes Lacey, Steven D.; Kirsch, Dylan J.; Li, Yiju Advanced Materials, Vol. 30, Issue 12 https://doi.org/10.1002/adma.201705651	journal	January 2018
A Supercompressible, Elastic, and Bendable Carbon Aerogel with Ultrasensitive Detection Limits for Compression Strain, Pressure, and Bending Angle Zhuo, Hao; Hu, Yijie; Tong, Xing Advanced Materials, Vol. 30, Issue 18 https://doi.org/10.1002/adma.201706705	journal	March 2018
A Plesiohedral Cellular Network of Graphene Bubbles for Ultralight, Strong, and Superelastic Materials Yeo, Seon Ju; Oh, Min Jun; Jun, Hyun Min Advanced Materials, Vol. 30, Issue 45 https://doi.org/10.1002/adma.201802997	journal	August 2018
Laser-Induced Graphene: From Discovery to Translation Ye, Ruquan; James, Dustin K.; Tour, James M. Advanced Materials, Vol. 31, Issue 1 https://doi.org/10.1002/adma.201803621	journal	October 2018
Structurally Controlled Cellular Architectures for High‐Performance Ultra‐Lightweight Materials Yeo, Seon Ju; Oh, Min Jun; Yoo, Pil J. Advanced Materials, Vol. 31, Issue 34 https://doi.org/10.1002/adma.201803670	journal	November 2018
3D Heteroatom‐Doped Carbon Nanomaterials as Multifunctional Metal‐Free Catalysts for Integrated Energy Devices Paul, Rajib; Du, Feng; Dai, Liming Advanced Materials, Vol. 31, Issue 13 https://doi.org/10.1002/adma.201805598	journal	January 2019
Superelastic Hard Carbon Nanofiber Aerogels Yu, Zhi‐Long; Qin, Bing; Ma, Zhi‐Yuan Advanced Materials, Vol. 31, Issue 23 https://doi.org/10.1002/adma.201900651	journal	March 2019
3D Printing of Ultralight Biomimetic Hierarchical Graphene Materials with Exceptional Stiffness and Resilience Peng, Meiwen; Wen, Zhen; Xie, Lingjie Advanced Materials, Vol. 31, Issue 35 https://doi.org/10.1002/adma.201902930	journal	July 2019
Bayesian Machine Learning in Metamaterial Design: Fragile Becomes Supercompressible Bessa, Miguel A.; Glowacki, Piotr; Houlder, Michael Advanced Materials, Vol. 31, Issue 48 https://doi.org/10.1002/adma.201904845	journal	October 2019
Direct 3D Printing of Reactive Agitating Impellers for the Convenient Treatment of Various Pollutants in Water Sun, Xueyan; Yan, Ying; Zhang, Lijing Advanced Materials Interfaces, Vol. 5, Issue 8 https://doi.org/10.1002/admi.201701626	journal	February 2018
Recent Progress of Polysaccharide‐Based Hydrogel Interfaces for Wound Healing and Tissue Engineering Zhu, Tianxue; Mao, Jiajun; Cheng, Yan Advanced Materials Interfaces, Vol. 6, Issue 17 https://doi.org/10.1002/admi.201900761	journal	July 2019
3D-Printed, Superelastic Polypyrrole-Graphene Electrodes with Ultrahigh Areal Capacitance for Electrochemical Energy Storage Qi, Zhen; Ye, Jianchao; Chen, Wen Advanced Materials Technologies, Vol. 3, Issue 7 https://doi.org/10.1002/admt.201800053	journal	June 2018
Dual‐Tunable Structural Colors from Liquid‐Infused Aerogels Wang, Zhen; Zou, Weizhi; Zhao, Han Advanced Optical Materials, Vol. 8, Issue 7 https://doi.org/10.1002/adom.201901825	journal	February 2020
Mesoporous Li ₃ VO ₄ /C Submicron-Ellipsoids Supported on Reduced Graphene Oxide as Practical Anode for High-Power Lithium-Ion Batteries Li, Qidong; Wei, Qiulong; Sheng, Jinzhi Advanced Science, Vol. 2, Issue 12 https://doi.org/10.1002/advs.201500284	journal	October 2015
3D Carbon Materials for Efficient Oxygen and Hydrogen Electrocatalysis Jorge, Ana Belen; Jervis, Rhodri; Periasamy, Arun Prakash Advanced Energy Materials, Vol. 10, Issue 11 https://doi.org/10.1002/aenm.201902494	journal	November 2019
Strained 2D Layered Materials and Heterojunctions Huang, Tiantian; Wei, Wei; Chen, Xin Annalen der Physik, Vol. 531, Issue 4 https://doi.org/10.1002/andp.201800465	journal	February 2019
Ring Shuttling Controls Macroscopic Motion in a Three-Dimensional Printed Polyrotaxane Monolith Lin, Qianming; Hou, Xisen; Ke, Chenfeng Angewandte Chemie, Vol. 129, Issue 16 https://doi.org/10.1002/ange.201612440	journal	March 2017
MXene Aerogel Scaffolds for High‐Rate Lithium Metal Anodes Zhang, Xinyue; Lv, Ruijing; Wang, Aoxuan Angewandte Chemie, Vol. 130, Issue 46 https://doi.org/10.1002/ange.201808714	journal	October 2018
Ring Shuttling Controls Macroscopic Motion in a Three-Dimensional Printed Polyrotaxane Monolith Lin, Qianming; Hou, Xisen; Ke, Chenfeng Angewandte Chemie International Edition, Vol. 56, Issue 16 https://doi.org/10.1002/anie.201612440	journal	March 2017
Low-Density Open Cellular Sponges as Functional Materials Jiang, Shaohua; Agarwal, Seema; Greiner, Andreas Angewandte Chemie International Edition, Vol. 56, Issue 49 https://doi.org/10.1002/anie.201700684	journal	November 2017
MXene Aerogel Scaffolds for High-Rate Lithium Metal Anodes Zhang, Xinyue; Lv, Ruijing; Wang, Aoxuan Angewandte Chemie International Edition, Vol. 57, Issue 46 https://doi.org/10.1002/anie.201808714	journal	October 2018
Hierarchical FeCo ₂ S ₄ Nanotube Arrays Deposited on 3D Carbon Foam as Binder-free Electrodes for High-performance Asymmetric Pseudocapacitors Huang, Yunpeng; Cui, Fen; Hua, Mingqing Chemistry - An Asian Journal, Vol. 13, Issue 21 https://doi.org/10.1002/asia.201801203	journal	October 2018
3D Printing of Electrochemical Energy Storage Devices: A Review of Printing Techniques and Electrode/Electrolyte Architectures Cheng, Meng; Deivanayagam, Ramasubramonian; Shahbazian‐Yassar, Reza Batteries & Supercaps, Vol. 3, Issue 2 https://doi.org/10.1002/batt.201900130	journal	November 2019
Facile Assembly of 3D Porous Reduced Graphene Oxide/Ultrathin MnO ₂ Nanosheets-S Aerogels as Efficient Polysulfide Adsorption Sites for High-Performance Lithium-Sulfur Batteries Zhao, Xiaojun; Wang, Hui; Zhai, Gaohong Chemistry - A European Journal, Vol. 23, Issue 29 https://doi.org/10.1002/chem.201604828	journal	May 2017
Functional Inks for Printable Energy Storage Applications based on 2 D Materials Wang, Libin; Chen, Shi; Shu, Ting ChemSusChem, Vol. 13, Issue 6 https://doi.org/10.1002/cssc.201902019	journal	March 2020
3D-printed Electrodes for Sensing of Biologically Active Molecules Liyarita, Bella Rosa; Ambrosi, Adriano; Pumera, Martin Electroanalysis, Vol. 30, Issue 7 https://doi.org/10.1002/elan.201700828	journal	January 2018
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3D Printing of Highly Conductive Nanocomposites for the Functional Optimization of Liquid Sensors Chizari, Kambiz; Daoud, Mohamed Amine; Ravindran, Anil Raj Small, Vol. 12, Issue 44 https://doi.org/10.1002/smll.201601695	journal	September 2016
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3D Printing Hierarchical Silver Nanowire Aerogel with Highly Compressive Resilience and Tensile Elongation through Tunable Poisson's Ratio Yan, Pengli; Brown, Emery; Su, Qing Small, Vol. 13, Issue 38 https://doi.org/10.1002/smll.201701756	journal	August 2017
Advances on Microsized On-Chip Lithium-Ion Batteries Liu, Lixiang; Weng, Qunhong; Lu, Xueyi Small, Vol. 13, Issue 45 https://doi.org/10.1002/smll.201701847	journal	September 2017
Anticorrosive, Ultralight, and Flexible Carbon-Wrapped Metallic Nanowire Hybrid Sponges for Highly Efficient Electromagnetic Interference Shielding Wan, Yan-Jun; Zhu, Peng-Li; Yu, Shu-Hui Small, Vol. 14, Issue 27 https://doi.org/10.1002/smll.201800534	journal	May 2018
Conductivity Maximum in 3D Graphene Foams Liu, Feng; Wang, Chao; Tang, Qiheng Small, Vol. 14, Issue 32 https://doi.org/10.1002/smll.201801458	journal	July 2018
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A High-Performance Direct Methanol Fuel Cell Technology Enabled by Mediating High-Concentration Methanol through a Graphene Aerogel Liu, Xiaoteng; Xi, Jiabin; Xu, Ben Bin Small Methods, Vol. 2, Issue 10 https://doi.org/10.1002/smtd.201800138	journal	July 2018
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Perspective to the Potential Use of Graphene in Li‐Ion Battery and Supercapacitor Tian, Jiarui; Yang, Zhoufei; Yin, Zefang The Chemical Record, Vol. 19, Issue 7 https://doi.org/10.1002/tcr.201800090	journal	September 2018
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A novel fabrication method of carbon electrodes using 3D printing and chemical modification process Tian, Pan; Chen, Chaoyang; Hu, Jie Biomedical Microdevices, Vol. 20, Issue 1 https://doi.org/10.1007/s10544-017-0247-3	journal	November 2017
Super-compressible, fatigue resistant and anisotropic carbon aerogels for piezoresistive sensors Wang, Meng; Shao, Changyou; Zhou, Sukun Cellulose, Vol. 25, Issue 12 https://doi.org/10.1007/s10570-018-2080-0	journal	October 2018
Morphology of cross-linked cellulose nanocrystal aerogels: cryo-templating versus pressurized gas expansion processing Osorio, Daniel A.; Seifried, Bernhard; Moquin, Paul Journal of Materials Science, Vol. 53, Issue 13 https://doi.org/10.1007/s10853-018-2235-2	journal	March 2018
Recent advances on metal-free graphene-based catalysts for the production of industrial chemicals Wang, Zhiyong; Pu, Yuan; Wang, Dan Frontiers of Chemical Science and Engineering, Vol. 12, Issue 4 https://doi.org/10.1007/s11705-018-1722-y	journal	June 2018
Recent progress on printable power supply devices and systems with nanomaterials Lin, Yuanjing; Gao, Yuan; Fang, Fang Nano Research, Vol. 11, Issue 6 https://doi.org/10.1007/s12274-018-2068-y	journal	May 2018
Hierarchical Metal–Organic Frameworks with Macroporosity: Synthesis, Achievements, and Challenges Doan, Huan V.; Amer Hamzah, Harina; Karikkethu Prabhakaran, Prasanth Nano-Micro Letters, Vol. 11, Issue 1 https://doi.org/10.1007/s40820-019-0286-9	journal	July 2019
Ink-based 3D printing technologies for graphene-based materials: a review Wang, Jingfeng; Liu, Yuyan; Fan, Zhimin Advanced Composites and Hybrid Materials, Vol. 2, Issue 1 https://doi.org/10.1007/s42114-018-0067-9	journal	January 2019
Combustion synthesis of N-doped three-dimensional graphene networks using graphene oxide–nitrocellulose composites Zhang, Xin; Ziemer, Katherine S.; Weeks, Brandon L. Advanced Composites and Hybrid Materials, Vol. 2, Issue 3 https://doi.org/10.1007/s42114-019-00113-8	journal	August 2019
Highly stretchable carbon aerogels Guo, Fan; Jiang, Yanqiu; Xu, Zhen Nature Communications, Vol. 9, Issue 1 https://doi.org/10.1038/s41467-018-03268-y	journal	February 2018
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Chemistry from 3D printed objects Hartings, Matthew R.; Ahmed, Zeeshan Nature Reviews Chemistry, Vol. 3, Issue 5 https://doi.org/10.1038/s41570-019-0097-z	journal	April 2019
Direct Ink Write (DIW) 3D Printed Cellulose Nanocrystal Aerogel Structures Li, Vincent Chi-Fung; Dunn, Conner K.; Zhang, Zhe Scientific Reports, Vol. 7, Issue 1 https://doi.org/10.1038/s41598-017-07771-y	journal	August 2017
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3D-Printing of Meso-structurally Ordered Carbon Fiber/Polymer Composites with Unprecedented Orthotropic Physical Properties Lewicki, James P.; Rodriguez, Jennifer N.; Zhu, Cheng Scientific Reports, Vol. 7, Issue 1 https://doi.org/10.1038/srep43401	journal	March 2017
3D-printing technologies for electrochemical applications Ambrosi, Adriano; Pumera, Martin Chemical Society Reviews, Vol. 45, Issue 10 https://doi.org/10.1039/c5cs00714c	journal	January 2016
Hydrothermal self-assembly of graphene foams with controllable pore size Deng, Wei; Fang, Qile; Zhou, Xufeng RSC Advances, Vol. 6, Issue 25 https://doi.org/10.1039/c5ra26088d	journal	January 2016
Recent advances and progress in the development of graphene-based adsorbents for CO ₂ capture Balasubramanian, Rajasekhar; Chowdhury, Shamik Journal of Materials Chemistry A, Vol. 3, Issue 44 https://doi.org/10.1039/c5ta04822b	journal	January 2015
Ultralight, compressible and multifunctional carbon aerogels based on natural tubular cellulose Zhang, Junping; Li, Bucheng; Li, Lingxiao Journal of Materials Chemistry A, Vol. 4, Issue 6 https://doi.org/10.1039/c5ta10001a	journal	January 2016
Three dimensional printing of components and functional devices for energy and environmental applications Ruiz-Morales, J. C.; Tarancón, A.; Canales-Vázquez, J. Energy & Environmental Science, Vol. 10, Issue 4 https://doi.org/10.1039/c6ee03526d	journal	January 2017
Effect of temperature on the viscoelastic properties of nano-confined liquid mixtures Voïtchovsky, Kislon Nanoscale, Vol. 8, Issue 40 https://doi.org/10.1039/c6nr05879e	journal	January 2016
Synthesis and porous h-BN 3D architectures for effective humidity and gas sensors Gautam, Chandkiram; Tiwary, Chandra Sekhar; Machado, Leonardo D. RSC Advances, Vol. 6, Issue 91 https://doi.org/10.1039/c6ra18833h	journal	January 2016
The applications of carbon nanotubes and graphene in advanced rechargeable lithium batteries Yuan, Wenyu; Zhang, Yani; Cheng, Laifei Journal of Materials Chemistry A, Vol. 4, Issue 23 https://doi.org/10.1039/c6ta01546h	journal	January 2016
Air-dried, high-density graphene hybrid aerogels for phase change composites with exceptional thermal conductivity and shape stability Yang, Jing; Li, Xiaofeng; Han, Shuang Journal of Materials Chemistry A, Vol. 4, Issue 46 https://doi.org/10.1039/c6ta07869a	journal	January 2016
Smart supercapacitors with deformable and healable functions Guo, Kai; Yu, Neng; Hou, Zhiqiang Journal of Materials Chemistry A, Vol. 5, Issue 1 https://doi.org/10.1039/c6ta08458c	journal	January 2017
Emerging chemical strategies for imprinting magnetism in graphene and related 2D materials for spintronic and biomedical applications Tuček, Jiří; Błoński, Piotr; Ugolotti, Juri Chemical Society Reviews, Vol. 47, Issue 11 https://doi.org/10.1039/c7cs00288b	journal	January 2018
Graphene aerogels for efficient energy storage and conversion Mao, Jiajun; Iocozzia, James; Huang, Jianying Energy & Environmental Science, Vol. 11, Issue 4 https://doi.org/10.1039/c7ee03031b	journal	January 2018
Aerogel materials with periodic structures imprinted with cellulose nanocrystals Xu, Yi-Tao; Dai, Yiling; Nguyen, Thanh-Dinh Nanoscale, Vol. 10, Issue 8 https://doi.org/10.1039/c7nr07719j	journal	January 2018
Control of the microstructure and surface chemistry of graphene aerogels via pH and time manipulation by a hydrothermal method García-Bordejé, E.; Víctor-Román, S.; Sanahuja-Parejo, O. Nanoscale, Vol. 10, Issue 7 https://doi.org/10.1039/c7nr08732b	journal	January 2018
Effect of flake size on the mechanical properties of graphene aerogels prepared by freeze casting Gao, Weiwei; Zhao, Nifang; Yao, Weiquan RSC Advances, Vol. 7, Issue 53 https://doi.org/10.1039/c7ra05557a	journal	January 2017
Printing assembly and structural regulation of graphene towards three-dimensional flexible micro-supercapacitors Li, Wenbo; Li, Yonghe; Su, Meng Journal of Materials Chemistry A, Vol. 5, Issue 31 https://doi.org/10.1039/c7ta02041d	journal	January 2017
Compressible and conductive carbon aerogels from waste paper with exceptional performance for oil/water separation Li, Lingxiao; Li, Bucheng; Sun, Hanxue Journal of Materials Chemistry A, Vol. 5, Issue 28 https://doi.org/10.1039/c7ta03511j	journal	January 2017
Sulfur and nitrogen co-doped holey graphene aerogel for structurally resilient solid-state supercapacitors under high compressions Kotal, Moumita; Kim, Hyunjun; Roy, Sandipan Journal of Materials Chemistry A, Vol. 5, Issue 33 https://doi.org/10.1039/c7ta05237e	journal	January 2017
Monolithic aerogel photocatalysts: a review Wan, Wenchao; Zhang, Ruiyang; Ma, Minzhi Journal of Materials Chemistry A, Vol. 6, Issue 3 https://doi.org/10.1039/c7ta09227j	journal	January 2018
A flyweight and superelastic graphene aerogel as a high-capacity adsorbent and highly sensitive pressure sensor Xiao, Jianliang; Tan, Yeqiang; Song, Yihu Journal of Materials Chemistry A, Vol. 6, Issue 19 https://doi.org/10.1039/c7ta11348j	journal	January 2018
Exploring the electrochemical performance of graphite and graphene paste electrodes composed of varying lateral flake sizes Slate, Anthony J.; Brownson, Dale A. C.; Abo Dena, Ahmed S. Physical Chemistry Chemical Physics, Vol. 20, Issue 30 https://doi.org/10.1039/c8cp02196a	journal	January 2018
Application of graphene-based materials in water purification: from the nanoscale to specific devices Yang, Kaijie; Wang, Jun; Chen, Xiaoxiao Environmental Science: Nano, Vol. 5, Issue 6 https://doi.org/10.1039/c8en00194d	journal	January 2018
Fully 2D and 3D printed anisotropic mechanoluminescent objects and their application for energy harvesting in the dark Patel, Dinesh K.; Cohen, Bat-El; Etgar, Lioz Materials Horizons, Vol. 5, Issue 4 https://doi.org/10.1039/c8mh00296g	journal	January 2018
Direct ink writing of organic and carbon aerogels Chandrasekaran, Swetha; Yao, Bin; Liu, Tianyu Materials Horizons, Vol. 5, Issue 6 https://doi.org/10.1039/c8mh00603b	journal	January 2018
Additive manufacturing of complex micro-architected graphene aerogels Hensleigh, Ryan M.; Cui, Huachen; Oakdale, James S. Materials Horizons, Vol. 5, Issue 6 https://doi.org/10.1039/c8mh00668g	journal	January 2018
High-performance composite phase change materials for energy conversion based on macroscopically three-dimensional structural materials Yang, Jie; Tang, Li-Sheng; Bai, Lu Materials Horizons, Vol. 6, Issue 2 https://doi.org/10.1039/c8mh01219a	journal	January 2019
Three-dimensional graphene-based polymer nanocomposites: preparation, properties and applications Guan, Li-Zhi; Zhao, Li; Wan, Yan-Jun Nanoscale, Vol. 10, Issue 31 https://doi.org/10.1039/c8nr03044h	journal	January 2018
Graphene aerogels that withstand extreme compressive stress and strain Li, Chenwei; Ding, Meichun; Zhang, Baoqing Nanoscale, Vol. 10, Issue 38 https://doi.org/10.1039/c8nr04824j	journal	January 2018
High-quality graphene aerogels for thermally conductive phase change composites with excellent shape stability Yang, Jing; Li, Xiaofeng; Han, Shuang Journal of Materials Chemistry A, Vol. 6, Issue 14 https://doi.org/10.1039/c8ta00078f	journal	January 2018
Robust aerogels based on conjugated microporous polymer nanotubes with exceptional mechanical strength for efficient solar steam generation Mu, Peng; Bai, Wei; Zhang, Zheng Journal of Materials Chemistry A, Vol. 6, Issue 37 https://doi.org/10.1039/c8ta05698f	journal	January 2018
Heteroatom-doped carbon materials and their composites as electrocatalysts for CO ₂ reduction Cui, Huijuan; Guo, Yibo; Guo, Limin Journal of Materials Chemistry A, Vol. 6, Issue 39 https://doi.org/10.1039/c8ta07430e	journal	January 2018
3D printed electrodes for efficient membrane capacitive deionization Vafakhah, Sareh; Sim, Glenn Joey; Saeedikhani, Mohsen Nanoscale Advances, Vol. 1, Issue 12 https://doi.org/10.1039/c9na00507b	journal	January 2019
Versatile route to core–shell reinforced network nanostructures Rusch, Pascal; Niemeyer, Fabian; Pluta, Denis Nanoscale, Vol. 11, Issue 32 https://doi.org/10.1039/c9nr03645h	journal	January 2019
Recent advances in soft functional materials: preparation, functions and applications Li, Jun; Wong, Wai-Yeung; Tao, Xiao-ming Nanoscale, Vol. 12, Issue 3 https://doi.org/10.1039/c9nr07035d	journal	January 2020
Precise control of versatile microstructure and properties of graphene aerogel via freezing manipulation Zhu, Xiangyu; Yang, Chao; Wu, Pingwei Nanoscale, Vol. 12, Issue 8 https://doi.org/10.1039/c9nr07861d	journal	January 2020
Direct 3D printing of a graphene oxide hydrogel for fabrication of a high areal specific capacitance microsupercapacitor Yun, Xiawei; Lu, Bingchuan; Xiong, Zhiyuan RSC Advances, Vol. 9, Issue 50 https://doi.org/10.1039/c9ra04882k	journal	January 2019
Three-dimensionally printed polylactic acid/cellulose acetate scaffolds with antimicrobial effect Zuo, Mengdi; Pan, Nengyu; Liu, Quanjing RSC Advances, Vol. 10, Issue 5 https://doi.org/10.1039/c9ra08916k	journal	January 2020
A carbon aerogel with super mechanical and sensing performances for wearable piezoresistive sensors Zhuo, Hao; Hu, Yijie; Chen, Zehong Journal of Materials Chemistry A, Vol. 7, Issue 14 https://doi.org/10.1039/c9ta00596j	journal	January 2019
Mass production of graphene materials from solid carbon sources using a molecular cracking and welding method Yan, Qiangu; Li, Jinghao; Zhang, Xuefeng Journal of Materials Chemistry A, Vol. 7, Issue 23 https://doi.org/10.1039/c9ta01332f	journal	January 2019
Three-dimensional nitrogen and phosphorus co-doped carbon quantum dots/reduced graphene oxide composite aerogels with a hierarchical porous structure as superior electrode materials for supercapacitors Li, Jingying; Yun, Xiaoru; Hu, Zhongliang Journal of Materials Chemistry A, Vol. 7, Issue 46 https://doi.org/10.1039/c9ta08151h	journal	January 2019
3D printing-based cellular microelectrodes for high-performance asymmetric quasi-solid-state micro-pseudocapacitors Wang, Teng; Tian, Xiaocong; Li, Liang Journal of Materials Chemistry A, Vol. 8, Issue 4 https://doi.org/10.1039/c9ta11386j	journal	January 2020
Highly compressible and superior low temperature tolerant supercapacitors based on dual chemically crosslinked PVA hydrogel electrolytes Liu, Zhenzhen; Zhang, Junmei; Liu, Jing Journal of Materials Chemistry A, Vol. 8, Issue 13 https://doi.org/10.1039/c9ta12424a	journal	January 2020
Synthesis and patterning of graphene: Strategies and prospects Shukla, Shobha; Kang, Seung-Yeon; Saxena, Sumit Applied Physics Reviews, Vol. 6, Issue 2 https://doi.org/10.1063/1.5055624	journal	June 2019
3D printed graphene/polydimethylsiloxane composite for stretchable strain sensor with tunable sensitivity Wang, Zhenyu; Zhang, Qiang; Yue, Yunong Nanotechnology, Vol. 30, Issue 34 https://doi.org/10.1088/1361-6528/ab1287	journal	May 2019
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Perspective of additive manufacturing for metamaterials development Wu, Xin; Su, Yutai; Shi, Jing Smart Materials and Structures, Vol. 28, Issue 9 https://doi.org/10.1088/1361-665x/ab2eb6	journal	August 2019
Graphene aerogels: a review Gorgolis, George; Galiotis, Costas 2D Materials, Vol. 4, Issue 3 https://doi.org/10.1088/2053-1583/aa7883	journal	June 2017
Extraordinary tensile strength and ductility of scalable nanoporous graphene Kashani, Hamzeh; Ito, Yoshikazu; Han, Jiuhui Science Advances, Vol. 5, Issue 2 https://doi.org/10.1126/sciadv.aat6951	journal	February 2019
Field responsive mechanical metamaterials Jackson, Julie A.; Messner, Mark C.; Dudukovic, Nikola A. Science Advances, Vol. 4, Issue 12 https://doi.org/10.1126/sciadv.aau6419	journal	December 2018
A performance metric for additively manufactured microlattice structures under different loading conditions Després, Nathaniel; Cyr, Edward; Mohammadi, Mohsen Proceedings of the Institution of Mechanical Engineers, Part L: Journal of Materials: Design and Applications, Vol. 233, Issue 9 https://doi.org/10.1177/1464420718793916	journal	August 2018
Versatile route to core-shell reinforced network nanostructures Rusch, Pascal; Niemeyer, Fabian; Pluta, Denis Cambridge : Royal Society of Chemistry https://doi.org/10.15488/8770	other	January 2019
Carbon aerogel evolution: Allotrope, graphene-inspired, and 3D-printed aerogels Chandrasekaran, Swetha; Campbell, Patrick G.; Baumann, Theodore F. Journal of Materials Research, Vol. 32, Issue 22 https://doi.org/10.1557/jmr.2017.411	journal	October 2017
Nanostructured resorcinol-formaldehyde ink for 3D direct writing Ge, Yingting; Zhang, Ting; Zhou, Bin Journal of Materials Research, Vol. 33, Issue 14 https://doi.org/10.1557/jmr.2018.104	journal	May 2018
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Compressive Response of Non-slender Octet Carbon Microlattices Kudo, Akira; Misseroni, Diego; Wei, Yuchen Frontiers in Materials, Vol. 6 https://doi.org/10.3389/fmats.2019.00169	journal	July 2019
Interfacing Graphene-Based Materials With Neural Cells Bramini, Mattia; Alberini, Giulio; Colombo, Elisabetta Frontiers in Systems Neuroscience, Vol. 12 https://doi.org/10.3389/fnsys.2018.00012	journal	April 2018
Direct Cryo Writing of Aerogels Via 3D Printing of Aligned Cellulose Nanocrystals Inspired by the Plant Cell Wall Kam, Doron; Chasnitsky, Michael; Nowogrodski, Chen Colloids and Interfaces, Vol. 3, Issue 2 https://doi.org/10.3390/colloids3020046	journal	April 2019
The Emerging Frontiers and Applications of High-Resolution 3D Printing Mao, Mao; He, Jiankang; Li, Xiao Micromachines, Vol. 8, Issue 4 https://doi.org/10.3390/mi8040113	journal	April 2017
Synthesis of Three-Dimensional Graphene-Based Hybrid Materials for Water Purification: A Review Wang, Yan; Guo, Lei; Qi, Pengfei Nanomaterials, Vol. 9, Issue 8 https://doi.org/10.3390/nano9081123	journal	August 2019
Preparation of Anisotropic Aerogels with Pristine Graphene by Heat Flow and Study of Their Effects on Heat Transfer in Paraffin Huang, Jinhui; Zhang, Buning; He, Ming Nanomaterials, Vol. 9, Issue 11 https://doi.org/10.3390/nano9111622	journal	November 2019
Nanomaterials in Advanced, High-Performance Aerogel Composites: A Review Barrios, Elizabeth; Fox, David; Li Sip, Yuen Yee Polymers, Vol. 11, Issue 4 https://doi.org/10.3390/polym11040726	journal	April 2019
Stiffness-independent Toughening of Beams through Coaxial Interfaces Mueller, Jochen; Raney, Jordan R.; Kochmann, Dennis ETH Zurich https://doi.org/10.3929/ethz-b-000295940	text	January 2018
Interfacing Graphene-Based Materials With Neural Cells Bramini, Mattia; Alberini, Giulio; Colombo, Elisabetta arXiv https://doi.org/10.48550/arxiv.1903.08440	text	January 2019

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