Far-Field High-Energy Diffraction Microscopy: A Non-Destructive Tool for Characterizing the Microstructure and Micromechanical State of Polycrystalline Materials

Park, Jun-Sang; Zhang, Xuan; Kenesei, Peter; Wong, Su Leen; Li, Meimei; Almer, Jonathan

doi:10.1017/S1551929517000827

Title: Far-Field High-Energy Diffraction Microscopy: A Non-Destructive Tool for Characterizing the Microstructure and Micromechanical State of Polycrystalline Materials

Journal Article · Thu Aug 31 00:00:00 EDT 2017 · Microscopy Today

DOI:https://doi.org/10.1017/S1551929517000827· OSTI ID:1390810

Park, Jun-Sang ^[1]; Zhang, Xuan ^[2]; Kenesei, Peter ^[1]; Wong, Su Leen ^[3]; Li, Meimei ^[2]; Almer, Jonathan ^[1]

Argonne National Lab. (ANL), Argonne, IL (United States). X-ray Science Division
Argonne National Lab. (ANL), Argonne, IL (United States). Nuclear Engineering Division
Max Planck Inst. for Iron Research, Dusseldorf (Germany)

A suite of non-destructive, three-dimensional X-ray microscopy techniques have recently been developed and used to characterize the microstructures of polycrystalline materials. These techniques utilize high-energy synchrotron radiation and include near-field and far-field diffraction microscopy (NF- and FF-HEDM, respectively) and absorption tomography. Several compatible sample environments have also been developed, enabling a wide range of 3D studies of material evolution. In this article, the FF-HEDM technique is described in detail, including its implementation at the 1-ID beamline of the Advanced Photon Source. Examples of how the information obtained from FF-HEDM can be used to deepen our understanding of structure-property-processing relationships in selected materials are presented.

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Research Organization:: Argonne National Lab. (ANL), Argonne, IL (United States)

Sponsoring Organization:: USDOE Office of Science (SC), Basic Energy Sciences (BES); USDOE Office of Nuclear Energy (NE)

Grant/Contract Number:: AC02-06CH11357; FG02-10ER46758

OSTI ID:: 1390810

Journal Information:: Microscopy Today, Vol. 25, Issue 05; ISSN 1551-9295

Publisher:: Cambridge University PressCopyright Statement

Country of Publication:: United States

Language:: English

References (27)

Characterization of neutron-irradiated HT-UPS steel by high-energy X-ray diffraction microscopy Zhang, Xuan; Park, Jun-Sang; Almer, Jonathan Journal of Nuclear Materials, Vol. 471 https://doi.org/10.1016/j.jnucmat.2015.11.063	journal	April 2016
A rotational and axial motion system load frame insert for in situ high energy x-ray studies Shade, Paul A.; Blank, Basil; Schuren, Jay C. Review of Scientific Instruments, Vol. 86, Issue 9 https://doi.org/10.1063/1.4927855	journal	September 2015
i RadMat: A thermo-mechanical testing system for in situ high-energy X-ray characterization of radioactive specimens Zhang, Xuan; Xu, Chi; Wang, Leyun Review of Scientific Instruments, Vol. 88, Issue 1 https://doi.org/10.1063/1.4974246	journal	January 2017
Determining heterogeneous slip activity on multiple slip systems from single crystal orientation pole figures Pagan, Darren C.; Miller, Matthew P. Acta Materialia, Vol. 116 https://doi.org/10.1016/j.actamat.2016.06.020	journal	September 2016
High-energy diffraction microscopy at the advanced photon source Lienert, U.; Li, S. F.; Hefferan, C. M. JOM, Vol. 63, Issue 7 https://doi.org/10.1007/s11837-011-0116-0	journal	July 2011
Three-dimensional grain mapping by x-ray diffraction contrast tomography and the use of Friedel pairs in diffraction data analysis Ludwig, W.; Reischig, P.; King, A. Review of Scientific Instruments, Vol. 80, Issue 3 https://doi.org/10.1063/1.3100200	journal	March 2009
Combining flat crystals, bent crystals and compound refractive lenses for high-energy X-ray optics Shastri, S. D. Journal of Synchrotron Radiation, Vol. 11, Issue 2 https://doi.org/10.1107/S0909049503023586	journal	February 2004
The MAX IV storage ring project Tavares, Pedro F.; Leemann, Simon C.; Sjöström, Magnus Journal of Synchrotron Radiation, Vol. 21, Issue 5 https://doi.org/10.1107/S1600577514011503	journal	August 2014
Developing an austenitic stainless steel for improved performance in advanced fossil power facilities Maziasz, Philip J. JOM, Vol. 41, Issue 7 https://doi.org/10.1007/BF03220265	journal	July 1989
High-energy X-ray optics with silicon saw-tooth refractive lenses Shastri, S. D.; Almer, J.; Ribbing, C. Journal of Synchrotron Radiation, Vol. 14, Issue 2 https://doi.org/10.1107/S0909049507003962	journal	February 2007
Quantitative grain-scale ferroic domain volume fractions and domain switching strains from three-dimensional X-ray diffraction data Oddershede, Jette; Majkut, Marta; Cao, Qinghua Journal of Applied Crystallography, Vol. 48, Issue 3 https://doi.org/10.1107/S1600576715007669	journal	May 2015
Non-Destructive Characterization of Engineering Materials Using High-Energy X-rays at the Advanced Photon Source Park, Jun-Sang; Okasinski, John; Chatterjee, Kamalika Synchrotron Radiation News, Vol. 30, Issue 3 https://doi.org/10.1080/08940886.2017.1316125	journal	May 2017
Far-field high-energy diffraction microscopy: a tool for intergranular orientation and strain analysis Bernier, J. V.; Barton, N. R.; Lienert, U. The Journal of Strain Analysis for Engineering Design, Vol. 46, Issue 7 https://doi.org/10.1177/0309324711405761	journal	July 2011
Thermal and Electric Field-Dependent Evolution of Domain Structures in Polycrystalline ${BaTiO}_{3}$ Using the 3D-XRD Technique Varlioglu, Mesut; Lienert, Ulrich; Park, Jun-Sang Texture, Stress, and Microstructure, Vol. 2010 https://doi.org/10.1155/2010/910793	journal	January 2010
In situ single-grain peak profile measurements on Ti–7Al during tensile deformation Lienert, U.; Brandes, M. C.; Bernier, J. V. Materials Science and Engineering: A, Vol. 524, Issue 1-2 https://doi.org/10.1016/j.msea.2009.06.047	journal	October 2009
Big Data Staging with MPI-IO for Interactive X-ray Science Wozniak, Justin M.; Sharma, Hemant; Armstrong, Timothy G. 2014 IEEE/ACM International Symposium on Big Data Computing (BDC) https://doi.org/10.1109/BDC.2014.18	conference	December 2014
Characterization and application of a GE amorphous silicon flat panel detector in a synchrotron light source Lee, J. H.; Almer, J.; Aydιner, C. Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, Vol. 582, Issue 1 https://doi.org/10.1016/j.nima.2007.08.103	journal	November 2007
In situ assessment of lattice strain in an Al–Li alloy Beaudoin, A. J.; Obstalecki, M.; Tayon, W. Acta Materialia, Vol. 61, Issue 9 https://doi.org/10.1016/j.actamat.2013.02.037	journal	May 2013
From Historical Backgrounds to Recent Advances in 3D Characterization of Materials: An Overview Monteiro, Sergio Neves; Paciornik, Sidnei JOM, Vol. 69, Issue 1 https://doi.org/10.1007/s11837-016-2203-8	journal	December 2016
Quantitative X-ray tomography Maire, E.; Withers, P. J. International Materials Reviews, Vol. 59, Issue 1 https://doi.org/10.1179/1743280413Y.0000000023	journal	December 2013
High-energy synchrotron x-ray techniques for studying irradiated materials Park, Jun-Sang; Zhang, Xuan; Sharma, Hemant Journal of Materials Research, Vol. 30, Issue 9 https://doi.org/10.1557/jmr.2015.50	journal	March 2015
In situ X-ray peak shape analysis of embedded individual grains during plastic deformation of metals Pantleon, W.; Poulsen, H. F.; Almer, J. Materials Science and Engineering: A, Vol. 387-389 https://doi.org/10.1016/j.msea.2004.02.080	journal	December 2004
A framework for generating synthetic diffraction images from deforming polycrystals using crystal-based finite element formulations Wong, Su Leen; Park, Jun-Sang; Miller, Matthew P. Computational Materials Science, Vol. 77 https://doi.org/10.1016/j.commatsci.2013.03.019	journal	September 2013
Silicon saw-tooth refractive lens for high-energy X-rays made using a diamond saw Said, A. H.; Shastri, S. D. Journal of Synchrotron Radiation, Vol. 17, Issue 3 https://doi.org/10.1107/S0909049510003584	journal	March 2010
An introduction to three-dimensional X-ray diffraction microscopy Poulsen, Henning Friis Journal of Applied Crystallography, Vol. 45, Issue 6, p. 1084-1097 https://doi.org/10.1107/S0021889812039143	journal	October 2012
Probing Microstructure Dynamics With X-Ray Diffraction Microscopy Suter, R. M.; Hefferan, C. M.; Li, S. F. Journal of Engineering Materials and Technology, Vol. 130, Issue 2 https://doi.org/10.1115/1.2840965	journal	March 2008
Polychromatic X-ray micro- and nanodiffraction for spatially-resolved structural studies Budai, J. D.; Liu, W.; Tischler, J. Z. Thin Solid Films, Vol. 516, Issue 22 https://doi.org/10.1016/j.tsf.2008.04.045	journal	September 2008

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