Solid matrix transformation and tracer addition using molten ammonium bifluoride salt as a sample preparation method for laser ablation inductively coupled plasma mass spectrometry

Grate, Jay W.; Gonzalez, Jhanis J.; O'Hara, Matthew J.; Kellogg, Cynthia M.; Morrison, Samuel S.; Koppenaal, David W.; Chan, George C. -Y.; Mao, Xianglei; Zorba, Vassilia; Russo, Richard E.

doi:10.1039/C7AN00777A

Solid matrix transformation and tracer addition using molten ammonium bifluoride salt as a sample preparation method for laser ablation inductively coupled plasma mass spectrometry

Journal Article · Sun Jan 01 04:00:00 EST 2017 · Analyst

DOI:https://doi.org/10.1039/C7AN00777A· OSTI ID:1390422

^[1]; Gonzalez, Jhanis J. ^[2]; ^[1]; Kellogg, Cynthia M. ^[1]; Morrison, Samuel S. ^[1]; Koppenaal, David W. ^[1]; Chan, George C. -Y. ^[3]; Mao, Xianglei ^[3]; Zorba, Vassilia ^[3]; Russo, Richard E. ^[2]

Pacific Northwest National Laboratory; Richland; USA
Lawrence Berkeley National Laboratory; Berkeley; USA; Applied Spectra; Fremont
Lawrence Berkeley National Laboratory; Berkeley; USA

Spike addition in reactive solid matrix transformation (SMT) enables internal standards for laser ablation analysis.

Research Organization:: Pacific Northwest National Laboratory (PNNL), Richland, WA (US)

Sponsoring Organization:: USDOE

DOE Contract Number:: AC05-76RL01830

OSTI ID:: 1390422

Report Number(s):: PNNL-SA-124596; DN2001000

Journal Information:: Analyst, Journal Name: Analyst Journal Issue: 18 Vol. 142; ISSN ANALAO; ISSN 0003-2654

Publisher:: Royal Society of Chemistry

Country of Publication:: United States

Language:: English

References (41)

Laser Ablation in Analytical Chemistry Russo, Richard E.; Mao, Xianglei; Gonzalez, Jhanis J. Analytical Chemistry, Vol. 85, Issue 13 https://doi.org/10.1021/ac4005327	journal	May 2013
Recent advances in quantitative LA-ICP-MS analysis: challenges and solutions in the life sciences and environmental chemistry Limbeck, Andreas; Galler, Patrick; Bonta, Maximilian Analytical and Bioanalytical Chemistry, Vol. 407, Issue 22 https://doi.org/10.1007/s00216-015-8858-0	journal	July 2015
Study on aerosol characteristics and fractionation effects of organic standard materials for bioimaging by means of LA-ICP-MS Niehaus, Rebecca; Sperling, Michael; Karst, Uwe Journal of Analytical Atomic Spectrometry, Vol. 30, Issue 10 https://doi.org/10.1039/C5JA00221D	journal	January 2015
Particle size-related elemental fractionation in laser ablation in liquid inductively coupled plasma mass spectrometry Machida, Ryo; Nakazawa, Takashi; Sakuraba, Yuka Journal of Analytical Atomic Spectrometry, Vol. 30, Issue 12 https://doi.org/10.1039/C5JA00349K	journal	January 2015
Laser ablation—laser induced breakdown spectroscopy (LA-LIBS): A means for overcoming matrix effects leading to improved analyte response Windom, Bret C.; Hahn, David W. Journal of Analytical Atomic Spectrometry, Vol. 24, Issue 12 https://doi.org/10.1039/b913495f	journal	January 2009
Femtosecond laser ablation inductively coupled plasma mass spectrometry: Fundamentals and capabilities for depth profiling analysis Pisonero, Jorge; Günther, Detlef Mass Spectrometry Reviews, Vol. 27, Issue 6 https://doi.org/10.1002/mas.20180	journal	November 2008
Accuracy and precision of non-matrix-matched calibration for lead isotope ratio measurements of lead-poor minerals by LA-MC-ICPMS Souders, A. Kate; Sylvester, Paul J. Journal of Analytical Atomic Spectrometry, Vol. 25, Issue 7 https://doi.org/10.1039/c002729d	journal	January 2010
An uncertainty budget for trace analysis by isotope-dilution ICP-MS with proper consideration of correlation Moser, J.; Wegscheider, W.; Meisel, T. Analytical and Bioanalytical Chemistry, Vol. 377, Issue 1 https://doi.org/10.1007/s00216-003-2028-5	journal	September 2003
Elemental analyses of soil and sediment fused with lithium borate using isotope dilution laser ablation-inductively coupled plasma-mass spectrometry Malherbe, Julien; Claverie, Fanny; Alvarez, Aitor Analytica Chimica Acta, Vol. 793 https://doi.org/10.1016/j.aca.2013.07.031	journal	September 2013
The Development of Laser Ablation ICP-MS and Calibration Strategies: Examples from the Analysis of Trace Elements in Volcanic Glass Shards and Sulfide Minerals Perkins, William T.; Pearce, Nicholas J. G.; Westgate, John A. Geostandards and Geoanalytical Research, Vol. 21, Issue 2 https://doi.org/10.1111/j.1751-908X.1997.tb00669.x	journal	December 1997
Non-matrix matched calibration of major and minor concentrations of Zn and Cu in brass, aluminium and silicate glass using NIR femtosecond laser ablation inductively coupled plasma mass spectrometry Bian, Qunzhou; Garcia, Carmen C.; Koch, Joachim J. Anal. At. Spectrom., Vol. 21, Issue 2 https://doi.org/10.1039/B513690C	journal	January 2006
Determination of minor and trace elements in obsidian rock samples and archaeological artifacts by laser ablation inductively coupled plasma mass spectrometry using synthetic obsidian standards de B. Pereira, Carlos E.; Miekeley, Norbert; Poupeau, Gerard Spectrochimica Acta Part B: Atomic Spectroscopy, Vol. 56, Issue 10 https://doi.org/10.1016/S0584-8547(01)00339-1	journal	October 2001
Isotope dilution mass spectrometry as a calibration method for the analysis of trace elements in powder samples by LA-ICP-MS Tibi, Markus; Heumann, Klaus G. J. Anal. At. Spectrom., Vol. 18, Issue 9 https://doi.org/10.1039/B301835K	journal	January 2003
Calibration and correction of LA-ICP-MS and LA-MC-ICP-MS analyses for element contents and isotopic ratios Lin, Jie; Liu, Yongsheng; Yang, Yueheng Solid Earth Sciences, Vol. 1, Issue 1 https://doi.org/10.1016/j.sesci.2016.04.002	journal	June 2016
Applications of inductively coupled plasma mass spectrometry and laser ablation inductively coupled plasma mass spectrometry in materials science Becker, Johanna Sabine Spectrochimica Acta Part B: Atomic Spectroscopy, Vol. 57, Issue 12 https://doi.org/10.1016/S0584-8547(02)00213-6	journal	December 2002
Validation of LA-ICP-MS trace element analysis of geological glasses using a new solid-state 193 nm Nd:YAG laser and matrix-matched calibration Jochum, K. P.; Stoll, B.; Herwig, K. J. Anal. At. Spectrom., Vol. 22, Issue 2 https://doi.org/10.1039/B609547J	journal	January 2007
Laser ablation sampling Russo, Richard E.; Mao, Xianglei; Borisov, Oleg V. TrAC Trends in Analytical Chemistry, Vol. 17, Issue 8-9 https://doi.org/10.1016/S0165-9936(98)00047-8	journal	August 1998
Non-matrix matched calibration using near-IR femtosecond laser ablation inductively coupled plasma optical emission spectrometry Bian, Q. Z.; Koch, J.; Lindner, H. Journal of Analytical Atomic Spectrometry, Vol. 20, Issue 8 https://doi.org/10.1039/b500632e	journal	January 2005
Current approaches to calibration of LA-ICP-MS analysis Miliszkiewicz, Natalia; Walas, Stanisław; Tobiasz, Anna Journal of Analytical Atomic Spectrometry, Vol. 30, Issue 2 https://doi.org/10.1039/C4JA00325J	journal	January 2015
Application of isotope-dilution laser ablation ICP?MS for direct determination of Pu concentrations in soils at pg�g?1 levels Heumann, Klaus G.; Boulyga, Sergei F.; Tibi, Markus Analytical and Bioanalytical Chemistry, Vol. 378, Issue 2 https://doi.org/10.1007/s00216-003-2193-6	journal	January 2004
Decomposition of diverse solid inorganic matrices with molten ammonium bifluoride salt for constituent elemental analysis O'Hara, Matthew J.; Kellogg, Cyndi M.; Parker, Cyrena M. Chemical Geology, Vol. 466 https://doi.org/10.1016/j.chemgeo.2017.06.023	journal	September 2017
Development of ammonium bifluoride fusion method for rapid dissolution of trinitite samples and analysis by ICP-MS Hubley, Nickolas; Brown, John W. N.; Guthrie, James Journal of Radioanalytical and Nuclear Chemistry, Vol. 307, Issue 3 https://doi.org/10.1007/s10967-015-4371-3	journal	August 2015
Assessment of the precision and accuracy of thorium ( ²³² Th) and uranium ( ²³⁸ U) measured by quadrupole based inductively coupled plasma-mass spectrometry using liquid nebulization, nanosecond and femtosecond laser ablation Gonzalez, Jhanis J.; Oropeza, Dayana; Mao, Xianglei J. Anal. At. Spectrom., Vol. 23, Issue 2 https://doi.org/10.1039/B702754K	journal	January 2008
UV-femtosecond and nanosecond laser ablation-ICP-MS: internal and external repeatability González, Jhanis; Dundas, Siv H.; Yi Liu, Chun J. Anal. At. Spectrom., Vol. 21, Issue 8 https://doi.org/10.1039/B603492F	journal	January 2006
Development of Solid Calibration Standards for Trace Elemental Analyses of Tree Rings by Laser Ablation Inductively Coupled Plasma-Mass Spectrometry Watmough, Shaun A.; Hutchinson, Thomas C.; Evans, R. Douglas Environmental Science & Technology, Vol. 32, Issue 14 https://doi.org/10.1021/es980008x	journal	July 1998
Study of particle size influence on laser ablation inductively coupled plasma mass spectrometry using an in-line cascade impactor Liu, C. Y.; Mao, X. L.; González, J. J. Anal. At. Spectrom., Vol. 20, Issue 3 https://doi.org/10.1039/B414422H	journal	January 2005
A new strategy of solution calibration in laser ablation inductively coupled plasma mass spectrometry for multielement trace analysis of geological samples Pickhardt, Carola; Becker, J. S.; Dietze, Hans-Joachim Fresenius' Journal of Analytical Chemistry, Vol. 368, Issue 2-3 https://doi.org/10.1007/s002160000485	journal	September 2000
Laser ablation in analytical chemistry—a review Russo, R. Talanta, Vol. 57, Issue 3 https://doi.org/10.1016/S0039-9140(02)00053-X	journal	May 2002
Analysis of uranium in the insoluble residues after decomposition of soil samples by various techniques Jurečič, S.; Benedik, L.; Planinšek, P. Applied Radiation and Isotopes, Vol. 87 https://doi.org/10.1016/j.apradiso.2013.11.077	journal	May 2014
Direct determination of halogens in powdered geological and environmental samples using isotope dilution laser ablation ICP-MS Boulyga, Sergei F.; Heumann, Klaus G. International Journal of Mass Spectrometry, Vol. 242, Issue 2-3 https://doi.org/10.1016/j.ijms.2004.10.028	journal	April 2005
Laser Ablation ICP-MS Analysis of Geological Materials Prepared as Lithium Borate Glasses Eggins, Stephen M. Geostandards and Geoanalytical Research, Vol. 27, Issue 2 https://doi.org/10.1111/j.1751-908X.2003.tb00642.x	journal	July 2003
Critical revision of GD-MS, LA-ICP-MS and SIMS as inorganic mass spectrometric techniques for direct solid analysis Pisonero, Jorge; Fernández, Beatriz; Günther, Detlef Journal of Analytical Atomic Spectrometry, Vol. 24, Issue 9 https://doi.org/10.1039/b904698d	journal	January 2009
Biomonitoring of hair samples by laser ablation inductively coupled plasma mass spectrometry (LA-ICP-MS) Sela, H.; Karpas, Z.; Zoriy, M. International Journal of Mass Spectrometry, Vol. 261, Issue 2-3 https://doi.org/10.1016/j.ijms.2006.09.018	journal	March 2007
Analysis of U and Th in soils and sediments B—Why do we sometimes get the WRONG RESULT? Inn, Kenneth G. W.; Robin Hutchinson, J. M.; Kelly, William R. Journal of Radioanalytical and Nuclear Chemistry, Vol. 307, Issue 3 https://doi.org/10.1007/s10967-015-4566-7	journal	October 2015
Standard Addition Method for Laser Ablation ICPMS Using a Spinning Platform Claverie, Fanny; Malherbe, Julien; Bier, Naomi Analytical Chemistry, Vol. 85, Issue 7 https://doi.org/10.1021/ac303307u	journal	March 2013
Use of a single calibration graph for the determination of major elements in geological materials by laser ablation inductively coupled plasma atomic emission spectrometry with added internal standards Kanicky, V.; Mermet, Jean-Michel Fresenius' Journal of Analytical Chemistry, Vol. 363, Issue 3 https://doi.org/10.1007/s002160051191	journal	February 1999
Development of an accurate, sensitive, and robust isotope dilution laser ablation ICP-MS method for simultaneous multi-element analysis (chlorine, sulfur, and heavy metals) in coal samples Boulyga, Sergei F.; Heilmann, Jens; Prohaska, Thomas Analytical and Bioanalytical Chemistry, Vol. 389, Issue 3 https://doi.org/10.1007/s00216-007-1485-7	journal	July 2007
Solid-spiking isotope dilution laser ablation ICP-MS for the direct and simultaneous determination of trace elements in soils and sediments Fernández, Beatriz; Claverie, Fanny; Pécheyran, Christophe J. Anal. At. Spectrom., Vol. 23, Issue 3 https://doi.org/10.1039/B711247E	journal	January 2008
Fast Decomposition Procedure of Solid Samples by Lithium Borates Fusion Employing Salicylic Acid Trdin, Miha; Nečemer, Marijan; Benedik, Ljudmila Analytical Chemistry, Vol. 89, Issue 5 https://doi.org/10.1021/acs.analchem.6b04980	journal	February 2017
Total Rock Dissolution Using Ammonium Bifluoride (NH ₄ HF ₂ ) in Screw-Top Teflon Vials: A New Development in Open-Vessel Digestion Zhang, Wen; Hu, Zhaochu; Liu, Yongsheng Analytical Chemistry, Vol. 84, Issue 24 https://doi.org/10.1021/ac302327g	journal	November 2012
Quantification strategies for elemental imaging of biological samples using laser ablation-inductively coupled plasma-mass spectrometry Hare, Dominic; Austin, Christine; Doble, Philip The Analyst, Vol. 137, Issue 7 https://doi.org/10.1039/c2an15792f	journal	January 2012

Cited By (3)

In situ analytical characterization and chemical imaging of tablet coatings using laser induced breakdown spectroscopy (LIBS) Zou, Lanfang; Kassim, Brittany; Smith, Joseph P. The Analyst, Vol. 143, Issue 20 https://doi.org/10.1039/c8an01262h	journal	January 2018
Atomic Spectrometry Update – a review of advances in environmental analysis Bacon, Jeffrey R.; Butler, Owen T.; Cairns, Warren R. L. Journal of Analytical Atomic Spectrometry, Vol. 34, Issue 1 https://doi.org/10.1039/c8ja90044b	journal	January 2019
Recent advances in single-cell analysis by mass spectrometry Yin, Lei; Zhang, Zhi; Liu, Yingze The Analyst, Vol. 144, Issue 3 https://doi.org/10.1039/c8an01190g	journal	January 2019

Similar Records

Solid matrix transformation and tracer addition using molten ammonium bifluoride salt as a sample preparation method for laser ablation inductively coupled plasma mass spectrometry

Journal Article · Wed Jun 21 20:00:00 EDT 2017 · Analyst · OSTI ID:1532263

Time-resolved studies of particle effects in laser ablation inductively coupled plasma-mass spectrometry

Journal Article · Mon Nov 12 23:00:00 EST 2007 · Journal of Analytical Atomic Spectrometry · OSTI ID:973931

Time-resolved studies of particle effects in laser ablation inductively coupled plasma-mass spectrometry

Journal Article · Mon Nov 12 23:00:00 EST 2007 · Journal of Analytical Atomic Spectrometry · OSTI ID:973933

Related Subjects

ICP
LIBS
Mass Spectometry
ammonium bifluoride
laser ablation
matrix transformation
uranium

Solid matrix transformation and tracer addition using molten ammonium bifluoride salt as a sample preparation method for laser ablation inductively coupled plasma mass spectrometry

Citation Formats

References (41)

Cited By (3)

Similar Records

Related Subjects