Laser Fabrication of Two-Dimensional Rotating-Lattice Single Crystal

Savytskii, Dmytro; Au-Yeung, Courtney; Dierolf, Volkmar; Tamura, Nobumichi; Jain, Himanshu

doi:10.1021/acs.cgd.6b01709

Title: Laser Fabrication of Two-Dimensional Rotating-Lattice Single Crystal

Journal Article · Thu Mar 09 00:00:00 EST 2017 · Crystal Growth and Design

DOI:https://doi.org/10.1021/acs.cgd.6b01709· OSTI ID:1379798

^[1]; Au-Yeung, Courtney ^[1];

^[1]; Tamura, Nobumichi ^[2];

^[1]

Lehigh Univ., Bethlehem, PA (United States)
Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States)

A rotating lattice single (RLS) crystal is a unique form of solid, which was fabricated recently as one-dimensional architecture in glass via solid state transformation induced by laser irradiation. In these objects, the lattice rotates gradually and predictably about an axis that lies in the plane of the crystal and is normal to the laser scanning direction. This paper reports on the fabrication of Sb₂S₃ two-dimensional (2D) RLS crystals on the surface of 16SbI₃-84Sb₂S₃ glass, as a model example: individual RLS crystal lines are joined together using "stitching" or "rastering" as two successful protocols. The electron back scattered diffraction mapping and scanning Laue X-ray microdiffraction of the 2D RLS crystals show gradual rotation of lattice comprising of two components, one along the length of each line and another normal to this direction. The former component is determined by the rotation of the first line of the 2D pattern, but the relative contribution of the last component depends on the extent of overlap between two successive lines. By the appropriate choice of initial seed orientation and the direction of scanning, it is possible to control the lattice rotation, and even to reduce it down to 5 for a 50 × 50 μm 2 2D pattern of Sb₂S₃ crystal.

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Research Organization:: Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States)

Sponsoring Organization:: USDOE Office of Science (SC), Basic Energy Sciences (BES)

Grant/Contract Number:: AC02-05CH11231

OSTI ID:: 1379798

Journal Information:: Crystal Growth and Design, Vol. 17, Issue 4; ISSN 1528-7483

Publisher:: American Chemical SocietyCopyright Statement

Country of Publication:: United States

Language:: English

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Cited by: 13 works

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Single Crystal Growth via Solid → Solid Transformation of Glass Jain, Himanshu; Savytskii, Dmytro; Dierolf, Volkmar Transactions of the Indian Institute of Metals, Vol. 72, Issue 8 https://doi.org/10.1007/s12666-019-01737-6	journal	June 2019
Crystal-in-glass architecture engineering: writing, erasing and rewriting by a femtosecond laser beam Lipatiev, Alexey S.; Lotarev, Sergey V.; Okhrimchuk, Andrey G. CrystEngComm, Vol. 20, Issue 22 https://doi.org/10.1039/c8ce00525g	journal	January 2018
In situ study of rotating lattice single‐crystal formation in Sb ₂ S ₃ glass by Laue μXRD Au‐Yeung, Courtney; Stan, Camelia; Tamura, Nobumichi Journal of the American Ceramic Society, Vol. 103, Issue 7 https://doi.org/10.1111/jace.16905	journal	November 2019

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