Fabrication of large area flexible nanoplasmonic templates with flow coating

Huang, Qian; Devetter, Brent M.; Roosendaal, Timothy; LaBerge, Max; Bernacki, Bruce E.; Alvine, Kyle J.

doi:10.1063/1.4994737

Title: Fabrication of large area flexible nanoplasmonic templates with flow coating

Journal Article · Tue Jul 25 00:00:00 EDT 2017 · Review of Scientific Instruments

DOI:https://doi.org/10.1063/1.4994737· OSTI ID:1373841

Huang, Qian ^[1]; Devetter, Brent M. ^[1]; Roosendaal, Timothy ^[1]; LaBerge, Max ^[2]; Bernacki, Bruce E. ^[1]; Alvine, Kyle J. ^[1]

Pacific Northwest National Lab. (PNNL), Richland, WA (United States)
Pacific Northwest National Lab. (PNNL), Richland, WA (United States); Univ. of Texas, Austin, TX (United States)

We describe the development of a custom-built two-axis flow coater for the deposition of polymeric nanosphere monolayers that could be used in the fabrication of large area nanoplasmonic films. The technique described here has the capability of depositing large areas (up to 7 in. × 10 in.) of self-assembled monolayers of polymeric nanospheres onto polyethylene terephthalate (PET) films. Here, three sets of films consisting of different diameters (ranging from 100 to 300 nm) of polymeric nanospheres were used to demonstrate the capabilities of this instrument. To improve the surface wettability of the PET substrates during wet-deposition, we enhanced the wettability by using a forced air blown-arc plasma treatment system. Both the local microstructure, as confirmed by scanning electron microscopy, describing monolayer and multilayer coverage, and the overall macroscopic uniformity of the resultant nanostructured film were optimized by controlling the relative stage to blade speed and nanosphere concentration. We also show using a smaller nanoparticle template that such monolayers can be used to form nanoplasmonic films. As this flow-coating approach is a scalable technique, large area films such as the ones described here have a variety of crucial emerging applications in areas such as energy, catalysis, and chemical sensing.

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Research Organization:: Pacific Northwest National Laboratory (PNNL), Richland, WA (United States)

Sponsoring Organization:: USDOE

Grant/Contract Number:: AC05-76RL01830

OSTI ID:: 1373841

Alternate ID(s):: OSTI ID: 1372510

Report Number(s):: PNNL-SA-123649

Journal Information:: Review of Scientific Instruments, Vol. 88, Issue 7; ISSN 0034-6748

Publisher:: American Institute of Physics (AIP)Copyright Statement

Country of Publication:: United States

Language:: English

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Cited by: 3 works

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