A Reproducible Approach of Preparing High-Quality Overdoped Bi 2 Sr 2 CaCu 2 O 8+δ Single Crystals by Oxygen Annealing and Quenching Method

Zhang, Yu-Xiao; Zhao, Lin; Gu, Gen-Da; Zhou, Xing-Jiang

doi:10.1088/0256-307X/33/6/067403

Title: A Reproducible Approach of Preparing High-Quality Overdoped Bi ₂ Sr ₂ CaCu ₂ O _8+δ Single Crystals by Oxygen Annealing and Quenching Method

Journal Article · Wed Jun 01 00:00:00 EDT 2016 · Chinese Physics Letters

DOI:https://doi.org/10.1088/0256-307X/33/6/067403· OSTI ID:1336149

Zhang, Yu-Xiao ^[1]; Zhao, Lin ^[1]; Gu, Gen-Da ^[2]; Zhou, Xing-Jiang ^[3]

Chinese Academy of Sciences (CAS), Beijing (China). National Lab. for Superconductivity and Beijing National Lab. for Condensed Matter Physics
Brookhaven National Lab. (BNL), Upton, NY (United States). Condensed Matter Physics and Materials Science Dept.
Chinese Academy of Sciences (CAS), Beijing (China). National Lab. for Superconductivity and Beijing National Lab. for Condensed Matter Physics; Collaborative Innovation Center of Quantum Matter, Beijing (China)

Here, we report a reproducible approach in preparing high-quality overdoped Bi₂Sr₂ CaCu₂ O_8+δ (Bi2212) single crystals by annealing Bi2212 crystals in high oxygen pressure followed by a fast quenching. High-quality overdoped and heavily overdoped Bi2212 single crystals are obtained by controlling the annealing oxygen pressure. Furthermore, we find that, beyond a limit of oxygen pressure that can achieve most heavily overdoped Bi2212 with a T_c ~63 K, the annealed Bi2212 begins to decompose. This accounts for the existence of the hole-doping limit and thus the T_c limit in the heavily overdoped region of Bi2212 by the oxygen annealing process. Our results provide a reliable way in preparing high-quality overdoped and heavily overdoped Bi2212 crystals that are important for studies of the physical properties, electronic structure and superconductivity mechanism of the cuprate superconductors.

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Research Organization:: Brookhaven National Lab. (BNL), Upton, NY (United States)

Sponsoring Organization:: USDOE Office of Science (SC), Basic Energy Sciences (BES)

Grant/Contract Number:: SC00112704

OSTI ID:: 1336149

Report Number(s):: BNL-112651-2016-JA; R&D Project: PO010; KC0201060

Journal Information:: Chinese Physics Letters, Vol. 33, Issue 6; ISSN 0256-307X

Publisher:: IOP PublishingCopyright Statement

Country of Publication:: United States

Language:: English

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Cited by: 3 works

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Selective hybridization between the main band and the superstructure band in the ${Bi}_{2} {Sr}_{2} {CaCu}_{2} O_{8 + δ}$ superconductor Gao, Qiang; Yan, Hongtao; Liu, Jing Physical Review B, Vol. 101, Issue 1 https://doi.org/10.1103/physrevb.101.014513	journal	January 2020

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Title: A Reproducible Approach of Preparing High-Quality Overdoped Bi ₂ Sr ₂ CaCu ₂ O _8+δ Single Crystals by Oxygen Annealing and Quenching Method