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Pb substitution in the Bi{sub 2}Sr{sub 2}CaCu{sub 2}O{sub 8+{delta}} high-T{sub c} superconductor: Cation overdoping

Journal Article · · Physical Review, B: Condensed Matter
; ;  [1]
  1. Naval Research Laboratory, Washington, DC 20375 (United States)

We study the effects of Pb substitution in single crystals of the high-temperature superconductor Bi{sub 2}Sr{sub 2}CaCu{sub 2}O{sub 8+{delta}}. We compare Pb-substituted samples with {open_quotes}pure{close_quotes} (unsubstituted) crystals in terms of structure, cation composition, and the temperature dependences of ac susceptibility and Raman scattering. We find that Pb{sup 2+} primarily substitutes for Bi{sup 3+}, leading directly to a T{sub c} reduction characteristic of overdoped samples. We also observe structural changes related to the superlattice modulation along b*. Raman scattering studies indicate that some Pb atoms go to Sr sites. Low-temperature electronic Raman scattering shows further evidence for cation overdoping by comparison with oxygen annealed pure Bi{sub 2}Sr{sub 2}CaCu{sub 2}O{sub 8+{delta}}.

OSTI ID:
550547
Journal Information:
Physical Review, B: Condensed Matter, Journal Name: Physical Review, B: Condensed Matter Journal Issue: 22 Vol. 56; ISSN PRBMDO; ISSN 0163-1829
Country of Publication:
United States
Language:
English