Developments in time-resolved high pressure x-ray diffraction using rapid compression and decompression

Smith, Jesse S.; Sinogeikin, Stanislav V.; Lin, Chuanlong; Rod, Eric; Bai, Ligang; Shen, Guoyin

doi:10.1063/1.4926887

Title: Developments in time-resolved high pressure x-ray diffraction using rapid compression and decompression

Journal Article · Fri Jul 24 00:00:00 EDT 2015 · Review of Scientific Instruments

DOI:https://doi.org/10.1063/1.4926887· OSTI ID:1203748

Smith, Jesse S. ^[1]; Sinogeikin, Stanislav V. ^[1]; Lin, Chuanlong ^[1]; Rod, Eric ^[1]; Bai, Ligang ^[1]; Shen, Guoyin ^[1]

Carnegie Inst. of Washington, Argonne, IL (United States). High Pressure Collaborative Access Team (HPCAT)

Complementary advances in high pressure research apparatus and techniques make it possible to carry out time-resolved high pressure research using what would customarily be considered static high pressure apparatus. This work specifically explores time-resolved high pressure x-ray diffraction with rapid compression and/or decompression of a sample in a diamond anvil cell. Key aspects of the synchrotron beamline and ancillary equipment are presented here, including source considerations, rapid (de)compression apparatus, high frequency imaging detectors, and software suitable for processing large volumes of data. A number of examples are presented, including fast equation of state measurements, compression rate dependent synthesis of metastable states in silicon and germanium, and ultrahigh compression rates using a piezoelectric driven diamond anvil cell.

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Research Organization:: Argonne National Laboratory (ANL), Argonne, IL (United States). Advanced Photon Source (APS)

Sponsoring Organization:: USDOE National Nuclear Security Administration (NNSA); National Science Foundation (NSF); USDOE Office of Science (SC), Basic Energy Sciences (BES)

Grant/Contract Number:: EAR-1128799; FG02-94ER14466; NA0001974; FG02-99ER45775; AC02-06CH11357

OSTI ID:: 1203748

Alternate ID(s):: OSTI ID: 1228699

Journal Information:: Review of Scientific Instruments, Vol. 86, Issue 7; ISSN 0034-6748

Publisher:: American Institute of Physics (AIP)Copyright Statement

Country of Publication:: United States

Language:: ENGLISH

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Cited by: 30 works

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References (27)

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Online remote control systems for static and dynamic compression and decompression using diamond anvil cells Sinogeikin, Stanislav V.; Smith, Jesse S.; Rod, Eric Review of Scientific Instruments, Vol. 86, Issue 7 https://doi.org/10.1063/1.4926892	journal	July 2015
A CO ₂ laser heating system for in situ high pressure-temperature experiments at HPCAT Smith, Dean; Smith, Jesse S.; Childs, Christian Review of Scientific Instruments, Vol. 89, Issue 8 https://doi.org/10.1063/1.5040508	journal	August 2018
Advanced Spectral Analysis Program Montgomery, J. M.; Lipp, M. J. Review of Scientific Instruments, Vol. 90, Issue 2 https://doi.org/10.1063/1.5048311	journal	February 2019
Fly scan apparatus for high pressure research using diamond anvil cells Smith, Jesse S.; Rod, Eric A.; Shen, Guoyin Review of Scientific Instruments, Vol. 90, Issue 1 https://doi.org/10.1063/1.5057445	journal	January 2019
Multimode scanning X-ray diffraction microscopy for diamond anvil cell experiments Hrubiak, Rostislav; Smith, Jesse S.; Shen, Guoyin Review of Scientific Instruments, Vol. 90, Issue 2 https://doi.org/10.1063/1.5057518	journal	February 2019
New dynamic diamond anvil cells for tera-pascal per second fast compression x-ray diffraction experiments Jenei, Zs.; Liermann, H. P.; Husband, R. Review of Scientific Instruments, Vol. 90, Issue 6 https://doi.org/10.1063/1.5098993	journal	June 2019
In situ x-ray diffraction study of polyamorphism in H ₂ O under isothermal compression and decompression Shen, Guoyin; Smith, Jesse S.; Kenney-Benson, Curtis The Journal of Chemical Physics, Vol. 150, Issue 24 https://doi.org/10.1063/1.5100958	journal	June 2019
Experimental evidence of low-density liquid water upon rapid decompression Lin, Chuanlong; Smith, Jesse S.; Sinogeikin, Stanislav V. Proceedings of the National Academy of Sciences, Vol. 115, Issue 9 https://doi.org/10.1073/pnas.1716310115	journal	February 2018
High-pressure studies with x-rays using diamond anvil cells Shen, Guoyin; Mao, Ho Kwang Reports on Progress in Physics, Vol. 80, Issue 1 https://doi.org/10.1088/1361-6633/80/1/016101	journal	November 2016
High pressure x-ray diffraction techniques with synchrotron radiation Liu, Jing Chinese Physics B, Vol. 25, Issue 7 https://doi.org/10.1088/1674-1056/25/7/076106	journal	July 2016
Venture into Water’s No Man’s Land: Structural Transformations of Solid $H_{2} O$ under Rapid Compression and Decompression Lin, Chuanlong; Smith, Jesse S.; Liu, Xuqiang Physical Review Letters, Vol. 121, Issue 22 https://doi.org/10.1103/physrevlett.121.225703	journal	November 2018
Nature of polyamorphic transformations in $H_{2} O$ under isothermal compression and decompression Shen, Guoyin; Smith, Jesse S.; Kenney-Benson, Curtis Physical Review Materials, Vol. 3, Issue 7 https://doi.org/10.1103/physrevmaterials.3.073404	journal	July 2019
Solids, liquids, and gases under high pressure Mao, Ho-Kwang; Chen, Xiao-Jia; Ding, Yang Reviews of Modern Physics, Vol. 90, Issue 1 https://doi.org/10.1103/revmodphys.90.015007	journal	March 2018
New dynamic diamond anvil cells for tera-pascal per second fast compression x-ray diffraction experiments Jenei, Zs.; Liermann, H. P.; Husband, R. Deutsches Elektronen-Synchrotron, DESY, Hamburg https://doi.org/10.3204/pubdb-2019-02611	text	January 2019
A metastable liquid melted from a crystalline solid under decompression Lin, Chuanlong; Smith, Jesse S.; Sinogeikin, Stanislav V. Nature Communications, Vol. 8, Issue 1 https://doi.org/10.1038/ncomms14260	journal	January 2017

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Title: Developments in time-resolved high pressure x-ray diffraction using rapid compression and decompression

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