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Method for high resolution magnetic resonance analysis using magic angle technique

Patent ·
OSTI ID:1174598
;

A method of performing a magnetic resonance analysis of a biological object that includes placing the biological object in a main magnetic field and in a radio frequency field, the main magnetic field having a static field direction; rotating the biological object at a rotational frequency of less than about 100 Hz around an axis positioned at an angle of about 54.degree.44' relative to the main magnetic static field direction; pulsing the radio frequency to provide a sequence that includes a magic angle turning pulse segment; and collecting data generated by the pulsed radio frequency. According to another embodiment, the radio frequency is pulsed to provide a sequence capable of producing a spectrum that is substantially free of spinning sideband peaks.

Research Organization:
Pacific Northwest National Laboratory (PNNL), Richland, WA (United States)
Sponsoring Organization:
USDOE
DOE Contract Number:
AC06-76RL01830
Assignee:
Battelle Memorial Institute (Richland, WA)
Patent Number(s):
6,653,832
Application Number:
09/803,381
OSTI ID:
1174598
Country of Publication:
United States
Language:
English

References (17)

Manipulation of phase and amplitude modulation of spin magnetization in magic angle spinning nuclear magnetic resonance in the presence of molecular diffusion journal April 2001
Fluorine-19 Solid-State NMR Magic-Angle-Turning Experiments Using Multiple-Pulse Homonuclear Decoupling journal June 1999
An investigation of rat mammary healthy and R3230AC tumor tissues and cells by means of solid-state 13C NMR journal December 1996
Two-Dimensional Sideband Separation in Magic-Angle-Spinning NMR journal July 1995
Gradient, high-resolution, magic angle spinning1H nuclear magnetic resonance spectroscopy of intact cells journal March 1998
High-resolution chemical shift and chemical shift anisotropy correlation in solids using slow magic angle spinning journal October 1992
Magic-Angle-Turning Experiments for Measuring Chemical-Shift-Tensor Principal Values in Powdered Solids journal April 1995
An Isotropic Chemical Shift-Chemical Shift Anisotropy Magic-Angle Slow-Spinning 2D NMR Experiment journal October 1993
High-resolution1H NMR spectroscopy in rat liver using magic angle turning at a 1 Hz spinning rate journal April 2002
Correlation of isotropic shifts and chemical shift anisotropies by two-dimensional fourier-transform magic-angle hopping nmr spectroscopy journal March 1983
Nuclear magnetic resonance in a rotating magnetic field journal March 1968
Low-speed magic-angle-spinning carbon-13 NMR of fruit tissue journal September 1992
Improvements to the magic angle hopping experiment journal October 1993
Selective excitation in Fourier transform nuclear magnetic resonance journal March 1978
Quantitative neuropathology by high resolution magic angle spinning proton magnetic resonance spectroscopy journal June 1997
A sensitive, high resolution magic angle turning experiment for measuring chemical shift tensor principal values journal December 1998
High-Resolution Magic Angle Spinning 1H NMR Spectroscopy of Intact Liver and Kidney: Optimization of Sample Preparation Procedures and Biochemical Stability of Tissue during Spectral Acquisition journal June 2000

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