Toward comprehensive studies of liquids at high pressures and high temperatures: Combined structure, elastic wave velocity, and viscosity measurements in the Paris-Edinburgh cell
- CIW
Techniques for measuring liquid structure, elastic wave velocity, and viscosity under high pressure have been integrated using a Paris–Edinburgh cell at Beamline 16-BM-B, HPCAT of the Advanced Photon Source. The Paris–Edinburgh press allows for compressing large volume samples (up to 2 mm in both diameter and length) up to ~7 GPa and 2000 °C. Multi-angle energy dispersive X-ray diffraction provides structure factors of liquid to a large Q of ~19 Å. Ultrasonic techniques have been developed to investigate elastic wave velocity of liquids combined with the X-ray imaging. Falling sphere viscometry, using high-speed X-ray radiography (>1000 frames/s), enables us to investigate a wide range of viscosity, from those of high viscosity silicates or oxides melts to low viscosity (<1 mPa s) liquids and fluids such as liquid metals or salts. The integration of these multiple techniques has promoted comprehensive studies of structure and physical properties of liquids as well as amorphous materials at high pressures and high temperatures, making it possible to investigate correlations between structure and physical properties of liquids in situ.
- Research Organization:
- Advanced Photon Source (APS), Argonne National Laboratory (ANL), Argonne, IL (US)
- Sponsoring Organization:
- NSFDOE - BASIC ENERGY SCIENCES
- OSTI ID:
- 1126804
- Journal Information:
- Phys. Earth Planet. In., Journal Name: Phys. Earth Planet. In. Journal Issue: 03, 2014 Vol. 228
- Country of Publication:
- United States
- Language:
- ENGLISH
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X-ray imaging for studying behavior of liquids at high pressures and high temperatures using Paris-Edinburgh press