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Development of sour resistant modified 13Cr OCTG

Book ·
OSTI ID:106092
;  [1]; ;  [2]
  1. Nippon Steel Corp., Futtsu, Chiba (Japan). Steel Research Lab.
  2. Nippon Steel Corp., Tobata, Kitakyushu (Japan). Yawata R and D Lab.

Sour resistant 13% Cr martensitic OCTG (Oil Country Tubular Goods) with so far unexpected high CO{sub 2} corrosion resistance was developed. CO{sub 2} corrosion resistance was remarkably increased by complex additions of Cu and Ni, of which contribution to CO{sub 2} corrosion resistance corresponds to that by a further addition of 6% Cr at 180 C. SSC resistance was improved by an addition of Mo. Based on such knowledge of roles of chemical elements on corrosion properties and phase stability, 0.02%C-12.5%Cr-4.5%Ni-1.5%Mo-1.5%Cu steel was developed. This steel has good hot-workability and was produced into seamless OCTG. Corrosion rates in a high pressure CO{sub 2} environment were less than 0.1 mm/y at temperatures up to 200 C (392 F) compared with 100 C of conventional API L80-13CR. No SSC occurred in sour environments with partial pressure of 0.001MPA or less even at low pH of 3.5. At elevated temperatures no cracking and no pitting was observed in H{sub 2}S containing CO{sub 2}-brine environments. The properties of the developed steel are much better in CO{sub 2} corrosion and SSC resistance compared with those of conventional 13Cr steel and are close to those of duplex stainless steel.

OSTI ID:
106092
Report Number(s):
CONF-950304--
Country of Publication:
United States
Language:
English