Calibration of X-ray imaging devices for accurate intensity measurement

Journal Article · Fri Jun 15 04:00:00 EDT 2012 · Powder Diffraction

DOI:https://doi.org/10.1017/S0885715612000413· OSTI ID:1055486

Haugh, Michael J.; Charest, Michael R.; Ross, Patrick W.; Lee, Joshua J.; Schneider, Marilyn B.; Palmer, Nathan E.; Teruya, Alan T.

National Security Technologies (NSTec) has developed calibration procedures for X-ray imaging systems using NIST traceable sources. The X-ray sources that are used for calibration are both diode type and diode/fluorescer combinations. Calibrating the X-ray detectors is the key to accurate calibration of the X-ray sources. Both energy dispersive detectors and photodiodes measuring total flux were used. We have developed calibration techniques for the detectors using radioactive sources that are traceable to the National Institute of Standards and Technology (NIST). The German synchrotron at Physikalische Technische Bundestalt (PTB) is used to calibrate silicon photodiodes over the energy range from 50 eV to 60 keV. The measurements on X-ray cameras made using the NSTec X-ray sources have included the quantum efficiency averaged over all pixels, the camera counts per photon per pixel, and response variation across the sensor. The instrumentation required to accomplish the calibrations is described. X-ray energies ranged from 720 eV to 22.7 keV. The X-ray sources produce narrow energy bands, allowing us to determine the properties as a function of X-ray energy. The calibrations were done for several types of imaging devices. There were back illuminated and front illuminated CCD (charge coupled device) sensors, and a CID (charge injection device) type camera. The CCD and CID camera types differ significantly in some of their properties that affect the accuracy of X-ray intensity measurements. All cameras discussed here are silicon based. The measurements of quantum efficiency variation with X-ray energy are compared to models for the sensor structure. Cameras that are not back-thinned are compared to those that are.

• Research Organization: Nevada Test Site/National Security Technologies, LLC (United States)
• Sponsoring Organization: USDOE National Nuclear Security Administration (NNSA)
• DOE Contract Number: AC52-06NA25946
• OSTI ID: 1055486
• Report Number(s): DOE/NV/25946--1306
• Journal Information: Powder Diffraction, Journal Name: Powder Diffraction Journal Issue: 02 Vol. 27; ISSN 0885-7156; ISSN applab
• Publisher: Cambridge University Press
• Country of Publication: United States
• Language: English

Related Subjects

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND TECHNOLOGY
x-ray
calibration