Solidification and loss of hydrostaticity in liquid media used for pressure measurements

Torikachvili, M. S.; Kim, S. K.; Colombier, E.; Bud’ko, S. L.; Canfield, P. C.

doi:10.1063/1.4937478

Title: Solidification and loss of hydrostaticity in liquid media used for pressure measurements

Journal Article · Wed Dec 16 00:00:00 EST 2015 · Review of Scientific Instruments

DOI:https://doi.org/10.1063/1.4937478· OSTI ID:1249336

^[1]; Kim, S. K. ^[2]; Colombier, E. ^[2]; Bud’ko, S. L. ^[2]; Canfield, P. C. ^[2]

San Diego State Univ., San Diego, CA (United States)
Ames Lab. and Iowa State Univ., Ames, IA (United States)

We carried out a study of the pressure dependence of the solidification temperature in nine pressure transmitting media that are liquid at ambient temperature, under pressures up to 2.3 GPa. These fluids are 1:1 isopentane/n-pentane, 4:6 light mineral oil/n-pentane, 1:1 isoamyl alcohol/n-pentane, 4:1 methanol/ethanol, 1:1 FC72/FC84 (Fluorinert), Daphne 7373, isopentane, and Dow Corning PMX silicone oils 200 and 60,000 cS. We relied on the high sensitivity of the electrical resistivity of Ba(Fe_1–xRu_x)₂As₂ single crystals to the freezing of the pressure media and cross-checked with corresponding anomalies observed in the resistance of the manganin coil that served as the ambient temperature resistive manometer. In addition to establishing the temperature-pressure line separating the liquid (hydrostatic) and frozen (non-hydrostatic) phases, these data permit rough estimates of the freezing pressure of these media at ambient temperature. As a result, this pressure establishes the extreme limit for the medium to be considered hydrostatic. For higher applied pressures, the medium has to be treated as non-hydrostatic.

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Research Organization:: Ames Laboratory (AMES), Ames, IA (United States)

Sponsoring Organization:: USDOE

Grant/Contract Number:: AC02-07CH11358

OSTI ID:: 1249336

Alternate ID(s):: OSTI ID: 1229920

Report Number(s):: IS-J-8942; RSINAK

Journal Information:: Review of Scientific Instruments, Vol. 86, Issue 12; ISSN 0034-6748

Publisher:: American Institute of Physics (AIP)Copyright Statement

Country of Publication:: United States

Language:: English

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Cited by: 56 works

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References (25)

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