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Title: Method of producing polyalkylated oligoalkylenepolyamines

Patent ·
OSTI ID:1125018

A method of preparing polyalkylated oligoalkylenepolyamines is provided. The method includes contacting oligoalkylenepolyamine with a reagent composition comprising (a) alkyl bromide and/or alkyl chloride; (b) a basic agent; and (c) iodide salt. The alkylation reaction may be carried out in a polar, aprotic organic solvent.

Research Organization:
NDSU Research Foundation, Fargo, ND, USA
Sponsoring Organization:
USDOE
DOE Contract Number:
FG36-08GO88160
Assignee:
NDSU Research Foundation (Fargo, ND)
Patent Number(s):
8,658,829
Application Number:
13/522,803
OSTI ID:
1125018
Resource Relation:
Patent File Date: 2011 Feb 04
Country of Publication:
United States
Language:
English

References (3)

Selective production of diethylenetriamine and aminoethylethanolamine patent November 1992
Selective production of linear pentaethylenehexamine and hydroxyethyldiethylenetriamine patent July 1993
Synthesis of hexylated triethylenetetramine: New ligand for homogeneous atom transfer radical polymerization journal April 2003

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