Five-dimensional visualization of phase transition in BiNiO{sub 3} under high pressure

Liu, Yijin; Wang, Junyue; Yang, Wenge; Azuma, Masaki; Mao, Wendy L.

doi:10.1063/1.4863229

Title: Five-dimensional visualization of phase transition in BiNiO{sub 3} under high pressure

Journal Article · Mon Jan 27 00:00:00 EST 2014 · Applied Physics Letters

DOI:https://doi.org/10.1063/1.4863229· OSTI ID:22280549

Liu, Yijin ^[1]; Wang, Junyue; Yang, Wenge ^[2]; Azuma, Masaki ^[3]; Mao, Wendy L. ^[4]

Stanford Synchrotron Radiation Lightsource, SLAC National Accelerator Laboratory, 2575 Sand Hill Road, Menlo Park, California 94025 (United States)
Center of High Pressure Science and Technology Advanced Research (HPSTAR), Shanghai 201203 (China)
Materials and Structures Laboratory, Tokyo Institute of Technology, 4259 Nagatsuta, Yokohama 226-8503 (Japan)
Geological and Environmental Sciences, 450 Serra Mall, Stanford University, Stanford, California 94305 (United States)

Colossal negative thermal expansion was recently discovered in BiNiO{sub 3} associated with a low density to high density phase transition under high pressure. The varying proportion of co-existing phases plays a key role in the macroscopic behavior of this material. Here, we utilize a recently developed X-ray Absorption Near Edge Spectroscopy Tomography method and resolve the mixture of high/low pressure phases as a function of pressure at tens of nanometer resolution taking advantage of the charge transfer during the transition. This five-dimensional (X, Y, Z, energy, and pressure) visualization of the phase boundary provides a high resolution method to study the interface dynamics of high/low pressure phase.

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OSTI ID:: 22280549

Journal Information:: Applied Physics Letters, Vol. 104, Issue 4; Other Information: (c) 2014 AIP Publishing LLC; Country of input: International Atomic Energy Agency (IAEA); ISSN 0003-6951

Country of Publication:: United States

Language:: English

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