Presence of Li clusters in molten LiCl-Li

Merwin, Augustus; Phillips, William C.; Williamson, Mark A.; Willit, James L.; Motsegood, Perry N.; Chidambaram, Dev

doi:10.1038/srep25435

Title: Presence of Li clusters in molten LiCl-Li

Journal Article · Thu May 05 00:00:00 EDT 2016 · Scientific Reports

DOI:https://doi.org/10.1038/srep25435· OSTI ID:1307568

Merwin, Augustus ^[1]; Phillips, William C. ^[1]; Williamson, Mark A. ^[2]; Willit, James L. ^[2]; Motsegood, Perry N. ^[2]; Chidambaram, Dev ^[1]

Univ. of Nevada, Reno, NV (United States)
Argonne National Lab. (ANL), Argonne, IL (United States)

Molten mixtures of lithium chloride and metallic lithium are of significant interest in various metal oxide reduction processes. These solutions have been reported to exhibit seemingly anomalous physical characteristics that lack a comprehensive explanation. ln the current work, the physical chemistry of molten solutions of lithium chloride and metallic lithium, with and without lithium oxide, was investigated using in situ Raman spectroscopy. The Raman spectra obtained from these solutions were in agreement with the previously reported spectrum of the lithium cluster, Li₈. Furthermore, this observation is indicative of a nanofluid type colloidal suspension of Li₈, in a molten salt matrix. It is suggested that the formation and suspension of lithium clusters in lithium chloride is the cause of various phenomena exhibited by these solutions that were previously unexplainable.

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Research Organization:: Argonne National Laboratory (ANL), Argonne, IL (United States)

Sponsoring Organization:: U.S. Nuclear Regulatory Commission (NRC); USDOE Office of Nuclear Energy (NE)

Grant/Contract Number:: AC02-06CH11357

OSTI ID:: 1307568

Journal Information:: Scientific Reports, Vol. 6; ISSN 2045-2322

Publisher:: Nature Publishing GroupCopyright Statement

Country of Publication:: United States

Language:: English

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Cited by: 24 works

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padding-left: 0; line-height:1.8em;"> <li class="authors">Liu, J.; Poignet, J. -C.</li> <li class="mb-0-5 source"> <span class="mr-1">Journal of Applied Electrochemistry, Vol. 20, Issue 5</span> <span class="text-muted"><a href="https://doi.org/10.1007/BF01094318" class="text-muted" target="_blank" rel="noopener noreferrer">https://doi.org/10.1007/BF01094318<span class="fa fa-external-link" aria-hidden="true"></span></a></span> </li> </ul> </td> <td class="small text-muted biblio-refs-td-secondary"> <span class="biblio-refs-type-badge ml-1 type" data-type="journal">journal</span> </td> <td class="small text-muted biblio-refs-td-secondary biblio-refs-td-secondary-date"><span class="date" data-date="1990-09-01">September 1990</span></td> </tr><tr> <td> <a href="https://doi.org/10.1007/978-94-010-0458-9_2" target="_blank" rel="noopener noreferrer" class="title" data-title="Electronic Properties of MetalMolten Salt Solutions">Electronic Properties of Metal/Molten Salt Solutions<span class="fa fa-external-link" aria-hidden="true"></span></a> <ul class="small references-list mb-0 mt-0" style="list-style-type:none; padding-left: 0; line-height:1.8em;"> <li class="authors">Warren, William W.</li> <li class="mb-0-5 source"> <span class="mr-1">Molten Salts: From Fundamentals to Applications</span> <span class="text-muted"><a href="https://doi.org/10.1007/978-94-010-0458-9_2" class="text-muted" target="_blank" rel="noopener noreferrer">https://doi.org/10.1007/978-94-010-0458-9_2<span class="fa fa-external-link" aria-hidden="true"></span></a></span> </li> </ul> </td> <td class="small text-muted biblio-refs-td-secondary"> <span class="biblio-refs-type-badge ml-1 type" data-type="book">book</span> </td> <td class="small text-muted biblio-refs-td-secondary biblio-refs-td-secondary-date"><span class="date" data-date="2002-01-01">January 2002</span></td> </tr></tbody></table> </div> </div> </section> <hr class="mt-2 mb-2"/> <section id="section-citations" data-list="list_cite" class="tab-content-sec osti-curated biblio-section section-scroll" style="scroll-margin-top:110px;"> <div class="biblio-section-navbar active row"> <div class="col"> <h2 class="abstract biblio-section-title mt-0 mb-0-5" style="cursor:pointer;"><span class="fa indicator"></span> Cited By (3) <span class="text-muted list-table-filternum"></span></h2> </div> <div class="col-md-12 col-lg-auto"> <form class="pure-form reference-filter d-print-none"> <div class="small biblio-section-navbar-tool"> <label for="list-table-search-citations" class="sr-only">Search citations: </label> <input type="text" class="list-table-search mt-0 mb-0-5 ml-1" id="list-table-search-citations" placeholder="Search citations ..."> </div> <div class="small biblio-section-navbar-tool"> <select class="list-table-sort mt-0 mb-0-5"> <option value="date">Sort by Date</option> <option value="title">Sort by Title</option> </select> </div> <div class="small biblio-section-navbar-tool"> <button type="reset" class="pure-button list-table-reset mt-0 mb-0-5">↺</button> </div> </form> </div> </div> <div class="row"> <div class="col-sm-12"> <table id="list-table-citations" class="truncate-rows list-table table-striped" data-rows="5" style="width:100%;"><tbody class="list"><tr> <td> <a href="https://doi.org/10.1149/2.0231911jes" target="_blank" rel="noopener noreferrer" class="title" data-title="Effect of Metallic Li on the Surface Chemistry of Inconel 625 Exposed to Molten LiClLi sub2sub OLi">Effect of Metallic Li on the Surface Chemistry of Inconel 625 Exposed to Molten LiCl-Li <sub>2</sub> O-Li<span class="fa fa-external-link" aria-hidden="true"></span></a> <ul class="small references-list mb-0 mt-0" style="list-style-type:none; 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Title: Presence of Li clusters in molten LiCl-Li

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