Detection of exposure damage in composite materials using Fourier transform infrared technology.
Goal: to detect the subtle changes in laminate composite structures brought about by thermal, chemical, ultraviolet, and moisture exposure. Compare sensitivity of an array of NDI methods, including Fourier Transform Infrared Spectroscopy (FTIR), to detect subtle differences in composite materials due to deterioration. Inspection methods applied: ultrasonic pulse echo, through transmission ultrasonics, thermography, resonance testing, mechanical impedance analysis, eddy current, low frequency bond testing & FTIR. Comparisons between the NDI methods are being used to establish the potential of FTIR to provide the necessary sensitivity to non-visible, yet significant, damage in the resin and fiber matrix of composite structures. Comparison of NDI results with short beam shear tests are being used to relate NDI sensitivity to reduction in structural performance. Chemical analyses technique, which measures the infrared intensity versus wavelength of light reflected on the surface of a structure (chemical and physical information via this signature). Advances in instrumentation have resulted in hand-held portable devices that allow for field use (few seconds per scan). Shows promise for production quality assurance and in-service applications on composite aircraft structures (scarfed repairs). Statistical analysis on frequency spectrums produced by FTIR interrogations are being used to produce an NDI technique for assessing material integrity. Conclusions are: (1) Use of NDI to assess loss of composite laminate integrity brought about by thermal, chemical, ultraviolet, and moisture exposure. (2) Degradation trends between SBS strength and exposure levels (temperature and time) have been established for different materials. (3) Various NDI methods have been applied to evaluate damage and relate this to loss of integrity - PE UT shows greatest sensitivity. (4) FTIR shows promise for damage detection and calibration to predict structural integrity (short beam shear). (5) Detection of damage for medium exposure levels (possibly resin matrix degradation only) is more difficult and requires additional study. (6) These are initial results only - program is continuing with additional heat, UV, chemical and water exposure test specimens.
- Research Organization:
- Sandia National Laboratories (SNL), Albuquerque, NM, and Livermore, CA (United States)
- Sponsoring Organization:
- USDOE
- DOE Contract Number:
- AC04-94AL85000
- OSTI ID:
- 1026935
- Report Number(s):
- SAND2010-6441C; TRN: US201121%%149
- Resource Relation:
- Conference: Proposed for presentation at the Air Transport Association Nondestructive Testing Forum held September 21-23, 2010 in Albuquerque, NM.
- Country of Publication:
- United States
- Language:
- English
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