Analytical capabilities for iodine detection: Review of possibilities for different applications

Riley, Brian J.; Beck, Chelsie L.; Evarts, Jonathan S.; Chong, Saehwa; Lines, Amanda M.; Felmy, Heather M.; McFarlane, Joanna; Andrews, Hunter B.; Bryan, Samuel A.; McHugh, Kelly C.; Cunningham, Heather S.; Asmussen, R. Matthew; Dhas, Jeffrey A.; Zhu, Zihua; Crum, Jarrod V.; Shen, Steve D.; McCloy, John S.; Heiden, Zachariah M.

doi:10.1063/5.0208591

Title: Analytical capabilities for iodine detection: Review of possibilities for different applications

Journal Article · Thu Aug 01 00:00:00 UTC 2024 · AIP Advances

DOI: https://doi.org/10.1063/5.0208591 · OSTI ID:2428072

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Pacific Northwest National Laboratory (PNNL), Richland, WA (United States)
Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)
Washington State Univ., Pullman, WA (United States)

This Review summarizes a range of analytical techniques that can be used to detect, quantify, and/or distinguish between isotopes of iodine (e.g., long-lived ¹²⁹I, short-lived ¹³¹I, stable ¹²⁷I). One reason this is of interest is that understanding potential radioiodine release from nuclear processes is crucial to prevent environmental contamination and to protect human health as it can incorporate into the thyroid leading to cancer. It is also of interest for evaluating iodine retention performances of next-generation iodine off-gas capture materials and long-term waste forms for immobilizing radioiodine for disposal in geologic repositories. Depending upon the form of iodine (e.g., molecules, elemental, and ionic) and the matter state (i.e., solid, liquid, and gaseous), the available options can vary. In addition, several other key parameters vary between the methods discussed herein, including the destructive vs nondestructive nature of the measurement process (including in situ vs ex situ measurement options), the analytical data collection times, and the amount of sample required for analysis.

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Research Organization:: Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States); Pacific Northwest National Laboratory (PNNL), Richland, WA (United States)

Sponsoring Organization:: USDOE Office of Nuclear Energy (NE)

Grant/Contract Number:: AC05-00OR22725; AC05-76RL01830

OSTI ID:: 2428072

Report Number(s):: PNNL-SA--195189

Journal Information:: AIP Advances, Journal Name: AIP Advances Journal Issue: 8 Vol. 14; ISSN 2158-3226

Publisher:: American Institute of Physics (AIP)Copyright Statement

Country of Publication:: United States

Language:: English

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Characterization and Optimization of a Spectral Window for Direct Gaseous Uranium Hexafluoride Enrichment Assay Using Laser-Induced Breakdown Spectroscopy Chan, George C. Y.; Martin, Leigh R.; Russo, Richard E. Applied Spectroscopy, Vol. 77, Issue 8 https://doi.org/10.1177/00037028221112953	journal	July 2022
Laser Ablation Plasmas and Spectroscopy for Nuclear Applications Kwapis, Emily H.; Borrero, Justin; Latty, Kyle S. Applied Spectroscopy, Vol. 78, Issue 1 https://doi.org/10.1177/00037028231211559	journal	December 2023
Chemical Speciation of Iodine Source Term to Containment McFarlane, Joanna; Wren, Jungsook C.; Lemire, Robert J. Nuclear Technology, Vol. 138, Issue 2 https://doi.org/10.13182/nt138-162	journal	May 2002
Determination of Specific Activity of¹³¹I Solutions via an Iodide Electrode Arino, Hirofumi; Kramer, Henry H. Nuclear Applications, Vol. 4, Issue 5 https://doi.org/10.13182/nt68-a26401	journal	May 1968
Online detection of halogen atoms in atmospheric VOCs by the LIBS-SPAMS technique Zhang, Qihang; Liu, Yuzhu; Chen, Yu Optics Express, Vol. 28, Issue 15 https://doi.org/10.1364/oe.400324	journal	July 2020
Molecular Iodine Fluorescence Spectra Generated with Helium-Neon Lasers for Spectrometer Calibration Williamson, J. Charles Applied Spectroscopy, Vol. 64, Issue 12 https://doi.org/10.1366/000370210793561637	journal	December 2010
Absorption of iodine from aqueous solutions on nuclear reactors alloys Bayri, B.; Rosset, R.; El Kacemi, K. Radiochimica Acta, Vol. 89, Issue 2 https://doi.org/10.1524/ract.2001.89.2.109	journal	January 2001
Measurement of I-129 in environmental samples by ICP-CRI-QMS: possibilities and limitations Li, K.; Vogel, E.; Krähenbühl, Urs Radiochimica Acta, Vol. 97, Issue 8 https://doi.org/10.1524/ract.2009.1639	journal	January 2009
Process optimization of caustic scrubber and iodine-129 immobilization in sodalite-based waste forms Bollinger, David L.; Erickson, Jessica; Bussey, John M. MRS Advances, Vol. 7, Issue 5-6 https://doi.org/10.1557/s43580-022-00229-y	journal	February 2022
Superiority of K-edge XANES over LIII-edge XANES in the Speciation of Iodine in Natural Soils Shimamoto, Yoko S.; Takahashi, Yoshio Analytical Sciences, Vol. 24, Issue 3 https://doi.org/10.2116/analsci.24.405	journal	January 2008
Organic Iodide Sorption from Dilute Gas Streams Greaney, Allison; Bruffey, Stephanie; Soelberg, Nick https://doi.org/10.2172/1831626	report	August 2021
The Preparation of an Iodate Selective Electrode Using Silver Iodate as the Active Agent in a Chitosan Support Mulyasuryani, Ani; Fardiyah, Qonitah; Sugiri, Rizki Indonesian Journal of Chemistry, Vol. 7, Issue 3 https://doi.org/10.22146/ijc.21670	journal	June 2010
Lead-vanadate sorbents for iodine trapping and their conversion into an iodoapatite-based conditioning matrix Pénélope, R.; Campayo, L.; Fournier, M. Frontiers in Chemistry, Vol. 10 https://doi.org/10.3389/fchem.2022.1085868	journal	December 2022
Functionality screening to help design effective materials for radioiodine abatement Robshaw, Thomas J.; Turner, Joshua; Tuck, Olivia Frontiers in Chemistry, Vol. 10 https://doi.org/10.3389/fchem.2022.997147	journal	October 2022
Application of Molecular Emissions in Laser-Induced Breakdown Spectroscopy: A Review Xu, Fanghao; Ma, Shixiang; Zhao, Chunjiang Frontiers in Physics, Vol. 10 https://doi.org/10.3389/fphy.2022.821528	journal	January 2022
Study on Volatile Organic Compounds from Diesel Engine Fueled with Palm Oil Biodiesel Blends at Low Idle Speed Kim, Ho Young; Choi, Nag Jung Applied Sciences, Vol. 10, Issue 14 https://doi.org/10.3390/app10144969	journal	July 2020
Dry Distillation of Radioiodine from TeO2 Targets Fonslet, Jesper; Koziorowski, Jacek Applied Sciences, Vol. 3, Issue 4 https://doi.org/10.3390/app3040675	journal	October 2013
Monitoring Xenon Capture in a Metal Organic Framework Using Laser-Induced Breakdown Spectroscopy Andrews, Hunter; Thallapally, Praveen; Robinson, Alexander Micromachines, Vol. 14, Issue 1 https://doi.org/10.3390/mi14010082	journal	December 2022
Comparison of the Detection Characteristics of Trace Species Using Laser-Induced Breakdown Spectroscopy and Laser Breakdown Time-of-Flight Mass Spectrometry Wang, Zhenzhen; Deguchi, Yoshihiro; Yan, Junjie Sensors, Vol. 15, Issue 3 https://doi.org/10.3390/s150305982	journal	March 2015
Impact of Glass Irradiation on Laser-Induced Breakdown Spectroscopy Data Analysis Garrett, Londrea J.; Morgan, Bryan W.; Burger, Miloš Sensors, Vol. 23, Issue 2 https://doi.org/10.3390/s23020691	journal	January 2023
Developments in the Field of Conducting and Non-conducting Polymer Based Potentiometric Membrane Sensors for Ions Over the Past Decade Faridbod, Farnoush; Norouzi, Parviz; Dinarvand, Rassoul Sensors, Vol. 8, Issue 4 https://doi.org/10.3390/s8042331	journal	April 2008
Validation and Comparison of Two Calibration Methods for the Measurement of Stable Iodine in the Urinary Matrix by ICP-MS: Standard Addition vs. External Calibration Landon, Géraldine; Bouvier-Capely, Céline; Legrand, Alexandre American Journal of Analytical Chemistry, Vol. 08, Issue 04 https://doi.org/10.4236/ajac.2017.84019	journal	January 2017
Rapid analysis of 129I in natural water samples using accelerator mass spectrometry Zhang, Mengting; Hou, Xiaolin Atomic Spectroscopy, Vol. 42, Issue 3 https://doi.org/10.46770/as.2021.071	journal	April 2021
Modelling molecular iodine emissions in a coastal marine environment: the link to new particle formation Saiz-Lopez, A.; Plane, J. M. C.; McFiggans, G. Atmospheric Chemistry and Physics, Vol. 6, Issue 4 https://doi.org/10.5194/acp-6-883-2006	journal	January 2006
A comparison of spectrophotometric and denuder based approaches for the determination of gaseous molecular iodine Chance, R. J.; Shaw, M.; Telgmann, L. Atmospheric Measurement Techniques, Vol. 3, Issue 1 https://doi.org/10.5194/amt-3-177-2010	journal	February 2010
Determination of trace level iodine in biological and botanical reference materials by isotope dilution mass spectrometry Gramlich, J. W.; Murphy, T. J. Journal of Research of the National Institute of Standards and Technology, Vol. 94, Issue 4 https://doi.org/10.6028/jres.094.022	journal	July 1989

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37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY
aqueous iodine
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iodine quantification
mass spectrometry
optical spectroscopy
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Title: Analytical capabilities for iodine detection: Review of possibilities for different applications

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