La 0.6 Sr 0.4 CoO 3−δ Films Under Deoxygenation: Magnetic And Electronic Transitions Are Apart from The Structural Phase Transition
Abstract
Abstract Topotactic phase transitions induced by changes in the oxygen vacancy concentration can largely alter the physical properties of complex oxides, including electronic and magnetic phases, while maintaining the structural integrity of the crystal lattice. An oxygen‐vacancy‐induced topotactic phase transition from perovskite (PV) to brownmillerite (BM) is achieved in epitaxial La 0.6 Sr 0.4 CoO 3−δ (LSCO) thin films. Two novel intermediate states with different oxygen content are identified by X‐ray diffraction, which involves a single‐phase reduced PV state and a mixed state of co‐existing PV and BM. The combination of depth‐sensitive polarized neutron reflectometry (PNR) and Rutherford backscattering (RBS) allows a quantitative determination of magnetization and the mean oxygen content in all states, revealing a continuous transition from La 0.6 Sr 0.4 CoO 2.97 to La 0.6 Sr 0.4 CoO 2.5 . BM formation is observed for an LSCO layer with an oxygen content of 2.67, while the magnetic and electronic transition already occurs for a layer with a higher oxygen content of 2.77 (and above) and in the absence of a BM signature. These results demonstrate that the physics of electronic metal‐to‐insulator transition (MIT), magnetic ferromagnet‐to‐non‐ferromagnet transition (FM‐to‐non‐FM), and structural PV‐to‐BM phase transition should be considered within themore »
- Authors:
-
- Peter Grünberg Institute (PGI‐7) Forschungszentrum Jülich GmbH 52425 Jülich Germany, Jülich Centre for Neutron Science (JCNS‐2) and Peter Grünberg Institut (PGI‐4) JARA‐FIT Forschungszentrum Jülich GmbH 52425 Jülich Germany, Jülich‐Aachen Research Alliance (JARA‐FIT) RWTH Aachen University 52056 Aachen Germany
- Jülich Centre for Neutron Science (JCNS‐2) and Peter Grünberg Institut (PGI‐4) JARA‐FIT Forschungszentrum Jülich GmbH 52425 Jülich Germany
- Neutron Scattering Division Neutron Sciences Directorate Oak Ridge National Laboratory Oak Ridge TN 37831 USA
- Jülich Centre for Neutron Science (JCNS‐2) and Peter Grünberg Institut (PGI‐4) JARA‐FIT Forschungszentrum Jülich GmbH 52425 Jülich Germany, Institute of Ion Beam Physics and Materials Research Helmholtz‐Zentrum Dresden‐Rossendorf 01328 Dresden Germany
- Institute of Ion Beam Physics and Materials Research Helmholtz‐Zentrum Dresden‐Rossendorf 01328 Dresden Germany
- Peter Grünberg Institute (PGI‐7) Forschungszentrum Jülich GmbH 52425 Jülich Germany, Jülich‐Aachen Research Alliance (JARA‐FIT) RWTH Aachen University 52056 Aachen Germany
- Semiconductor Nanoelectronics (PGI‐9) Forschungszentrum Jülich GmbH 52425 Jülich Germany
- Peter Grünberg Institute (PGI‐7) Forschungszentrum Jülich GmbH 52425 Jülich Germany, Jülich‐Aachen Research Alliance (JARA‐FIT) RWTH Aachen University 52056 Aachen Germany, Institut für Werkstoffe der Elektrotechnik 2 RWTH Aachen University 52056 Aachen Germany
- Jülich Centre for Neutron Science (JCNS‐2) and Peter Grünberg Institut (PGI‐4) JARA‐FIT Forschungszentrum Jülich GmbH 52425 Jülich Germany, Jülich‐Aachen Research Alliance (JARA‐FIT) RWTH Aachen University 52056 Aachen Germany
- Publication Date:
- Research Org.:
- Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)
- Sponsoring Org.:
- USDOE Office of Science (SC), Basic Energy Sciences (BES)
- OSTI Identifier:
- 2308865
- Alternate Identifier(s):
- OSTI ID: 2301657; OSTI ID: 2308867
- Grant/Contract Number:
- AC05-00OR22725
- Resource Type:
- Published Article
- Journal Name:
- Advanced Functional Materials
- Additional Journal Information:
- Journal Name: Advanced Functional Materials; Journal ID: ISSN 1616-301X
- Publisher:
- Wiley Blackwell (John Wiley & Sons)
- Country of Publication:
- Germany
- Language:
- English
- Subject:
- electronic and magnetic phase transitions; ionotronics; oxide electronics; polarized neutron reflectivity; topotactic phase transition
Citation Formats
He, Suqin, Petracic, Oleg, Lauter, Valeria, Cao, Lei, Zhou, Yunxia, Weber, Moritz Lukas, Schubert, Jürgen, Concepción, Omar, Dittmann, Regina, Waser, Rainer, Brückel, Thomas, and Gunkel, Felix. La 0.6 Sr 0.4 CoO 3−δ Films Under Deoxygenation: Magnetic And Electronic Transitions Are Apart from The Structural Phase Transition. Germany: N. p., 2024.
Web. doi:10.1002/adfm.202313208.
He, Suqin, Petracic, Oleg, Lauter, Valeria, Cao, Lei, Zhou, Yunxia, Weber, Moritz Lukas, Schubert, Jürgen, Concepción, Omar, Dittmann, Regina, Waser, Rainer, Brückel, Thomas, & Gunkel, Felix. La 0.6 Sr 0.4 CoO 3−δ Films Under Deoxygenation: Magnetic And Electronic Transitions Are Apart from The Structural Phase Transition. Germany. https://doi.org/10.1002/adfm.202313208
He, Suqin, Petracic, Oleg, Lauter, Valeria, Cao, Lei, Zhou, Yunxia, Weber, Moritz Lukas, Schubert, Jürgen, Concepción, Omar, Dittmann, Regina, Waser, Rainer, Brückel, Thomas, and Gunkel, Felix. Wed .
"La 0.6 Sr 0.4 CoO 3−δ Films Under Deoxygenation: Magnetic And Electronic Transitions Are Apart from The Structural Phase Transition". Germany. https://doi.org/10.1002/adfm.202313208.
@article{osti_2308865,
title = {La 0.6 Sr 0.4 CoO 3−δ Films Under Deoxygenation: Magnetic And Electronic Transitions Are Apart from The Structural Phase Transition},
author = {He, Suqin and Petracic, Oleg and Lauter, Valeria and Cao, Lei and Zhou, Yunxia and Weber, Moritz Lukas and Schubert, Jürgen and Concepción, Omar and Dittmann, Regina and Waser, Rainer and Brückel, Thomas and Gunkel, Felix},
abstractNote = {Abstract Topotactic phase transitions induced by changes in the oxygen vacancy concentration can largely alter the physical properties of complex oxides, including electronic and magnetic phases, while maintaining the structural integrity of the crystal lattice. An oxygen‐vacancy‐induced topotactic phase transition from perovskite (PV) to brownmillerite (BM) is achieved in epitaxial La 0.6 Sr 0.4 CoO 3−δ (LSCO) thin films. Two novel intermediate states with different oxygen content are identified by X‐ray diffraction, which involves a single‐phase reduced PV state and a mixed state of co‐existing PV and BM. The combination of depth‐sensitive polarized neutron reflectometry (PNR) and Rutherford backscattering (RBS) allows a quantitative determination of magnetization and the mean oxygen content in all states, revealing a continuous transition from La 0.6 Sr 0.4 CoO 2.97 to La 0.6 Sr 0.4 CoO 2.5 . BM formation is observed for an LSCO layer with an oxygen content of 2.67, while the magnetic and electronic transition already occurs for a layer with a higher oxygen content of 2.77 (and above) and in the absence of a BM signature. These results demonstrate that the physics of electronic metal‐to‐insulator transition (MIT), magnetic ferromagnet‐to‐non‐ferromagnet transition (FM‐to‐non‐FM), and structural PV‐to‐BM phase transition should be considered within the framework of separate but interrelated processes.},
doi = {10.1002/adfm.202313208},
journal = {Advanced Functional Materials},
number = ,
volume = ,
place = {Germany},
year = {Wed Feb 07 00:00:00 EST 2024},
month = {Wed Feb 07 00:00:00 EST 2024}
}
https://doi.org/10.1002/adfm.202313208
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