Femtosecond diffraction studies of the sodium chloride phase diagram under laser shock compression
Abstract
The phase diagram of sodium chloride (NaCl) under laser shock compression has been studied at Linac Coherent Light Source (LCLS) at the x-ray free-electron laser facility. Both solid–solid (B1 → B2) and solid–liquid (B2 → liquid) transitions have been observed along the Hugoniot over nanosecond time scales. By combining structural measurements through in situ x-ray diffraction, pressure determination through velocimetry, and a thermal equation-of-state, the shock-compressed data are used to constrain the phase diagram of NaCl. Transformation into the B2 phase is found to occur at 28(2) GPa, and B2–liquid coexistence is observed between 54(4) and 66(6) GPa, with near full melt at 66(6) GPa. Late-time pressure release from an initial shocked B2-state results in a B2 → B1 back transformation. Our results show agreement with previous static compression data, suggesting that the time scale for melting is very rapid and that equilibrium states in NaCl are being accessed over nanosecond time scales. Finally, a multiphase equation-of-state description of NaCl incorporated into a one-dimensional hydrocode is used to interpret pressure and temperature evolution over these rapid time scales.
- Authors:
-
[1];
[2];
[2];
[2];
[2];
[2];
[2];
[3];
[2];
[4];
[5];
[1]
- Johns Hopkins Univ., Baltimore, MD (United States)
- Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States)
- Los Alamos National Lab. (LANL), Los Alamos, NM (United States)
- SLAC National Accelerator Lab., Menlo Park, CA (United States). Linac Coherent Light Source (LCLS)
- Princeton Univ., NJ (United States)
- Publication Date:
- Research Org.:
- SLAC National Accelerator Laboratory (SLAC), Menlo Park, CA (United States); Lawrence Livermore National Laboratory (LLNL), Livermore, CA (United States)
- Sponsoring Org.:
- USDOE Laboratory Directed Research and Development (LDRD) Program
- OSTI Identifier:
- 1908433
- Grant/Contract Number:
- AC02-76SF00515; AC52-07NA27344; SC0022096; B623306
- Resource Type:
- Accepted Manuscript
- Journal Name:
- Journal of Applied Physics
- Additional Journal Information:
- Journal Volume: 132; Journal Issue: 8; Journal ID: ISSN 0021-8979
- Publisher:
- American Institute of Physics (AIP)
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 36 MATERIALS SCIENCE; interferometry; velocimetry; x-ray diffraction; free electron lasers; phase transitions; equations of state; shock compression
Citation Formats
Rastogi, Vinay, Smith, Raymond F., Swift, Damian C., Briggs, Richard, Gorman, Martin G., Krill, Connor, Coleman, Amy L., Fratanduono, Dayne E., Eggert, Jon H., Bolme, Cynthia A., Coppari, Federica, Gleason, Arianna, Lee, Hae Ja, Heimann, Philip, Duffy, Thomas S., and Wicks, June K. Femtosecond diffraction studies of the sodium chloride phase diagram under laser shock compression. United States: N. p., 2022.
Web. doi:10.1063/5.0094894.
Rastogi, Vinay, Smith, Raymond F., Swift, Damian C., Briggs, Richard, Gorman, Martin G., Krill, Connor, Coleman, Amy L., Fratanduono, Dayne E., Eggert, Jon H., Bolme, Cynthia A., Coppari, Federica, Gleason, Arianna, Lee, Hae Ja, Heimann, Philip, Duffy, Thomas S., & Wicks, June K. Femtosecond diffraction studies of the sodium chloride phase diagram under laser shock compression. United States. https://doi.org/10.1063/5.0094894
Rastogi, Vinay, Smith, Raymond F., Swift, Damian C., Briggs, Richard, Gorman, Martin G., Krill, Connor, Coleman, Amy L., Fratanduono, Dayne E., Eggert, Jon H., Bolme, Cynthia A., Coppari, Federica, Gleason, Arianna, Lee, Hae Ja, Heimann, Philip, Duffy, Thomas S., and Wicks, June K. Tue .
"Femtosecond diffraction studies of the sodium chloride phase diagram under laser shock compression". United States. https://doi.org/10.1063/5.0094894. https://www.osti.gov/servlets/purl/1908433.
@article{osti_1908433,
title = {Femtosecond diffraction studies of the sodium chloride phase diagram under laser shock compression},
author = {Rastogi, Vinay and Smith, Raymond F. and Swift, Damian C. and Briggs, Richard and Gorman, Martin G. and Krill, Connor and Coleman, Amy L. and Fratanduono, Dayne E. and Eggert, Jon H. and Bolme, Cynthia A. and Coppari, Federica and Gleason, Arianna and Lee, Hae Ja and Heimann, Philip and Duffy, Thomas S. and Wicks, June K.},
abstractNote = {The phase diagram of sodium chloride (NaCl) under laser shock compression has been studied at Linac Coherent Light Source (LCLS) at the x-ray free-electron laser facility. Both solid–solid (B1 → B2) and solid–liquid (B2 → liquid) transitions have been observed along the Hugoniot over nanosecond time scales. By combining structural measurements through in situ x-ray diffraction, pressure determination through velocimetry, and a thermal equation-of-state, the shock-compressed data are used to constrain the phase diagram of NaCl. Transformation into the B2 phase is found to occur at 28(2) GPa, and B2–liquid coexistence is observed between 54(4) and 66(6) GPa, with near full melt at 66(6) GPa. Late-time pressure release from an initial shocked B2-state results in a B2 → B1 back transformation. Our results show agreement with previous static compression data, suggesting that the time scale for melting is very rapid and that equilibrium states in NaCl are being accessed over nanosecond time scales. Finally, a multiphase equation-of-state description of NaCl incorporated into a one-dimensional hydrocode is used to interpret pressure and temperature evolution over these rapid time scales.},
doi = {10.1063/5.0094894},
journal = {Journal of Applied Physics},
number = 8,
volume = 132,
place = {United States},
year = {Tue Aug 23 00:00:00 EDT 2022},
month = {Tue Aug 23 00:00:00 EDT 2022}
}
Free Publicly Available Full Text
Publisher's Version of Record
Other availability
Search WorldCat to find libraries that may hold this journal
Save to My Library
You must Sign In or Create an Account in order to save documents to your library.
Works referenced in this record:
Line-imaging velocimeter for shock diagnostics at the OMEGA laser facility
journal, November 2004
- Celliers, P. M.; Bradley, D. K.; Collins, G. W.
- Review of Scientific Instruments, Vol. 75, Issue 11
Melting of Tantalum at Multimegabar Pressures on the Nanosecond Timescale
journal, June 2021
- Kraus, R. G.; Coppari, F.; Fratanduono, D. E.
- Physical Review Letters, Vol. 126, Issue 25
Ramp compression of diamond to five terapascals
journal, July 2014
- Smith, R. F.; Eggert, J. H.; Jeanloz, R.
- Nature, Vol. 511, Issue 7509
Ultrafast X-Ray Diffraction Studies of the Phase Transitions and Equation of State of Scandium Shock Compressed to 82 GPa
journal, January 2017
- Briggs, R.; Gorman, M. G.; Coleman, A. L.
- Physical Review Letters, Vol. 118, Issue 2
Time-resolved infrared radiometry of NaCl crystals under shock compression between 17 and43 GPa
journal, October 2004
- Ogura, Toshiyuki; Nakamura, Kazutaka G.; Kondo, Ken-ichi
- Physical Review B, Vol. 70, Issue 14
Femtosecond diffraction studies of solid and liquid phase changes in shock-compressed bismuth
journal, November 2018
- Gorman, M. G.; Coleman, A. L.; Briggs, R.
- Scientific Reports, Vol. 8, Issue 1
Ultra-High Pressure Dynamic Compression of Geological Materials
journal, February 2019
- Duffy, Thomas S.; Smith, Raymond F.
- Frontiers in Earth Science, Vol. 7
Nonisentropic Release of a Shocked Solid
journal, December 2019
- Heighway, P. G.; Sliwa, M.; McGonegle, D.
- Physical Review Letters, Vol. 123, Issue 24
Toward an internally consistent pressure scale
journal, May 2007
- Fei, Y.; Ricolleau, A.; Frank, M.
- Proceedings of the National Academy of Sciences, Vol. 104, Issue 22
High pressure phase transformation in iron under fast compression
journal, December 2009
- Bastea, Marina; Bastea, Sorin; Becker, Richard
- Applied Physics Letters, Vol. 95, Issue 24
Equation of state of iron under core conditions of large rocky exoplanets
journal, April 2018
- Smith, Raymond F.; Fratanduono, Dayne E.; Braun, David G.
- Nature Astronomy, Vol. 2, Issue 6
Metastability of diamond ramp-compressed to 2 terapascals
journal, January 2021
- Lazicki, A.; McGonegle, D.; Rygg, J. R.
- Nature, Vol. 589, Issue 7843
Compressibility of solids
journal, January 1987
- Vinet, P.; Ferrante, J.; Rose, J. H.
- Journal of Geophysical Research, Vol. 92, Issue B9
Equations of state of MgO, Au, Pt, NaCl-B1, and NaCl-B2: Internally consistent high-temperature pressure scales
journal, December 2007
- Dorogokupets, P. I.; Dewaele, A.
- High Pressure Research, Vol. 27, Issue 4
Hysteresis in the high pressure transformation of bcc‐ to hcp‐iron
journal, April 1991
- Taylor, R. D.; Pasternak, M. P.; Jeanloz, R.
- Journal of Applied Physics, Vol. 69, Issue 8
High strain-rate plastic flow in Al and Fe
journal, December 2011
- Smith, R. F.; Eggert, J. H.; Rudd, R. E.
- Journal of Applied Physics, Vol. 110, Issue 12
Determination of the phase boundary between the and phases in NaCl by in situ x-ray diffraction
journal, October 2003
- Nishiyama, Norimasa; Katsura, Tomoo; Funakoshi, Ken-ichi
- Physical Review B, Vol. 68, Issue 13
Freezing kinetics in overcompressed water
journal, May 2007
- Bastea, Marina; Bastea, Sorin; Reaugh, John E.
- Physical Review B, Vol. 75, Issue 17
High‐Pressure Equation of State for NaCl, KCl, and CsCl
journal, July 1971
- Decker, D. L.
- Journal of Applied Physics, Vol. 42, Issue 8
Measurement of the B 1- B 2 transition pressure in NaCl at high temperatures
journal, July 1987
- Li, Xiaoyuan; Jeanloz, Raymond
- Physical Review B, Vol. 36, Issue 1
Finite strain isotherm and velocities for single-crystal and polycrystalline NaCl at high pressures and 300°K
journal, January 1978
- Birch, Francis
- Journal of Geophysical Research, Vol. 83, Issue B3, p. 1257-1268
Melting of LiF and NaCl to 1 Mbar: Systematics of Ionic Solids at Extreme Conditions
journal, June 1997
- Boehler, Reinhard; Ross, Marvin; Boercker, David B.
- Physical Review Letters, Vol. 78, Issue 24
Two-phase equation of state for lithium fluoride
journal, February 2019
- Myint, Philip C.; Shi, Eric L.; Hamel, Sebastien
- The Journal of Chemical Physics, Vol. 150, Issue 7
Orientation and rate dependence in high strain-rate compression of single-crystal silicon
journal, December 2012
- Smith, R. F.; Minich, R. W.; Rudd, R. E.
- Physical Review B, Vol. 86, Issue 24
Melting curve of NaCl to 20 GPa from electrical measurements of capacitive current
journal, August 2015
- Li, Zeyu; Li, Jie
- American Mineralogist, Vol. 100, Issue 8-9
Time-dependence of the alpha to epsilon phase transformation in iron
journal, December 2013
- Smith, R. F.; Eggert, J. H.; Swift, D. C.
- Journal of Applied Physics, Vol. 114, Issue 22
Importance of van der Waals interaction on structural, vibrational, and thermodynamic properties of NaCl
journal, May 2018
- Marcondes, Michel L.; Wentzcovitch, Renata M.; Assali, Lucy V. C.
- Solid State Communications, Vol. 273
In situ X-Ray Diffraction of Shock-Compressed Fused Silica
journal, March 2018
- Tracy, Sally June; Turneaure, Stefan J.; Duffy, Thomas S.
- Physical Review Letters, Vol. 120, Issue 13
Melting of Sodium Chloride at Pressures to 65 kbar
journal, September 1969
- Akella, Jagannadham; Vaidya, S. N.; Kennedy, George C.
- Physical Review, Vol. 185, Issue 3
Measurement of Body-Centered Cubic Gold and Melting under Shock Compression
journal, July 2019
- Briggs, R.; Coppari, F.; Gorman, M. G.
- Physical Review Letters, Vol. 123, Issue 4
Shock‐induced melting and shear banding in single‐crystal NaCl
journal, January 1988
- Schmitt, Douglas R.; Ahrens, Thomas J.; Svendsen, Bob
- Journal of Applied Physics, Vol. 63, Issue 1
Recovery of metastable dense Bi synthesized by shock compression
journal, March 2019
- Gorman, M. G.; Coleman, A. L.; Briggs, R.
- Applied Physics Letters, Vol. 114, Issue 12
Effect of non-hydrostaticity on the α-ε transition of iron
journal, December 1990
- Barge, N. Von; Boehler, R.
- High Pressure Research, Vol. 6, Issue 2
First-principles study of the rocksalt–cesium chloride relative phase stability in alkali halides
journal, October 2002
- Flórez, M.; Recio, J. M.; Francisco, E.
- Physical Review B, Vol. 66, Issue 14
Pressure-volume equation of state of the high-pressure phase of NaCl
journal, March 2002
- Sata, Nagayoshi; Shen, Guoyin; Rivers, Mark L.
- Physical Review B, Vol. 65, Issue 10
Shock drive capabilities of a 30-Joule laser at the matter in extreme conditions hutch of the Linac Coherent Light Source
journal, October 2017
- Brown, Shaughnessy Brennan; Hashim, Akel; Gleason, Arianna
- Review of Scientific Instruments, Vol. 88, Issue 10
Direct measurements of the α-ϵ transition stress and kinetics for shocked iron
journal, May 2009
- Jensen, B. J.; Gray, G. T.; Hixson, R. S.
- Journal of Applied Physics, Vol. 105, Issue 10
Grüneisen parameter of NaCl at high compressions
journal, January 1977
- Boehler, Reinhard; Getting, Ivan C.; Kennedy, George C.
- Journal of Physics and Chemistry of Solids, Vol. 38, Issue 3
The NaCl pressure standard
journal, November 1999
- Brown, J. Michael
- Journal of Applied Physics, Vol. 86, Issue 10
Transformation kinetics for the shock wave induced phase transition in cadmium sulfide crystals
journal, January 2002
- Knudson, M. D.; Gupta, Y. M.
- Journal of Applied Physics, Vol. 91, Issue 12
Nucleating a Different Coordination in a Crystal under Pressure: A Study of the
B 1 − B 2
journal, August 2021
- Badin, Matej; Martoňák, Roman
- Physical Review Letters, Vol. 127, Issue 10
Melting and refreezing of zirconium observed using ultrafast x-ray diffraction
journal, February 2020
- Radousky, Harry B.; Armstrong, Michael R.; Austin, Ryan A.
- Physical Review Research, Vol. 2, Issue 1
Molecular-dynamics studies on the shock-induced phase transition of aMgF 2
journal, August 1995
- Nishidate, Kazume; Baba, Mamoru; Sato, Tsutomu
- Physical Review B, Vol. 52, Issue 5
observation of a phase transition in silicon carbide under shock compression using pulsed x-ray diffraction
journal, June 2019
- Tracy, S. J.; Smith, R. F.; Wicks, J. K.
- Physical Review B, Vol. 99, Issue 21
Crystal structure and equation of state of Fe-Si alloys at super-Earth core conditions
journal, April 2018
- Wicks, June K.; Smith, Raymond F.; Fratanduono, Dayne E.
- Science Advances, Vol. 4, Issue 4
Determining the refractive index of shocked [100] lithium fluoride to the limit of transmissibility
journal, July 2014
- Rigg, P. A.; Knudson, M. D.; Scharff, R. J.
- Journal of Applied Physics, Vol. 116, Issue 3
Phenomenological theory of the reconstructive phase transition between the NaCl and CsCl structure types
journal, April 2003
- Tolédano, P.; Knorr, K.; Ehm, L.
- Physical Review B, Vol. 67, Issue 14
X-ray preheating of window materials in direct-drive shock-wave timing experiments
journal, December 2006
- Theobald, W.; Miller, J. E.; Boehly, T. R.
- Physics of Plasmas, Vol. 13, Issue 12
HYADES—A plasma hydrodynamics code for dense plasma studies
journal, January 1994
- Larsen, Jon T.; Lane, Stephen M.
- Journal of Quantitative Spectroscopy and Radiative Transfer, Vol. 51, Issue 1-2
First principles versus spherical ion models of the B1 and B2 phases of NaCl
journal, January 1985
- Bukowinski, M. S. T.; Aidun, John
- Journal of Geophysical Research, Vol. 90, Issue B2