Temperature-dependence of oxidation and carburization of Grade 91 steel in CO2 containing impurities

Oleksak, Richard P.; Tylczak, Joseph H.; Doğan, Ömer N.

doi:10.1016/j.corsci.2022.110147

Title: Temperature-dependence of oxidation and carburization of Grade 91 steel in CO₂ containing impurities

Abstract

Future CO₂ based power systems require steels resistant to corrosion in high-temperature CO₂-rich environments. Candidate 9Cr ferritic-martensitic steels degrade by surface oxidation and substrate carburization, both of which can be strongly affected by impurities in the CO₂. In this study we examined Grade 91 steel exposed to 95%CO₂-4%H₂O-1%O₂ with/without 0.1% SO₂ at 1 atm and 550, 600, 650° C for up to 3000 h to establish the temperature-dependence of these processes. SO₂ showed little effect on oxidation at 550-600° C but reduced carburization, while the combination of SO₂ and faster alloy diffusion at 650° C resulted in significant reduction in both oxidation and carburization.

Authors:

Oleksak, Richard P. ^[1]; Tylczak, Joseph H. ^[1]; Doğan, Ömer N. ^[1]

National Energy Technology Lab. (NETL), Albany, OR (United States)

Publication Date:: Tue Feb 01 00:00:00 EST 2022

Research Org.:: National Energy Technology Laboratory (NETL), Pittsburgh, PA, Morgantown, WV, and Albany, OR (United States)

Sponsoring Org.:: USDOE Office of Fossil Energy (FE)

OSTI Identifier:: 1888227

Alternate Identifier(s):: OSTI ID: 1843902

Grant/Contract Number:: 89243318CFE000003

Resource Type:: Accepted Manuscript

Journal Name:: Corrosion Science

Additional Journal Information:: Journal Volume: 198; Journal ID: ISSN 0010-938X

Publisher:: Elsevier

Country of Publication:: United States

Language:: English

Subject:: 36 MATERIALS SCIENCE; Steel; Carburization; High temperature corrosion; Oxidation; Direct-fired CO₂ power cycle

Citation Formats


                    Oleksak, Richard P., Tylczak, Joseph H., and Doğan, Ömer N. Temperature-dependence of oxidation and carburization of Grade 91 steel in CO2 containing impurities.  United States: N. p., 2022. 
Web.  doi:10.1016/j.corsci.2022.110147.

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                    Oleksak, Richard P., Tylczak, Joseph H., & Doğan, Ömer N. Temperature-dependence of oxidation and carburization of Grade 91 steel in CO2 containing impurities.  United States.  https://doi.org/10.1016/j.corsci.2022.110147

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                    Oleksak, Richard P., Tylczak, Joseph H., and Doğan, Ömer N. Tue .  
"Temperature-dependence of oxidation and carburization of Grade 91 steel in CO2 containing impurities".  United States.  https://doi.org/10.1016/j.corsci.2022.110147.  https://www.osti.gov/servlets/purl/1888227.

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@article{osti_1888227,

  title        = {Temperature-dependence of oxidation and carburization of Grade 91 steel in CO2 containing impurities},

  author       = {Oleksak, Richard P. and Tylczak, Joseph H. and Doğan, Ömer N.},

  abstractNote = {Future CO2 based power systems require steels resistant to corrosion in high-temperature CO2-rich environments. Candidate 9Cr ferritic-martensitic steels degrade by surface oxidation and substrate carburization, both of which can be strongly affected by impurities in the CO2. In this study we examined Grade 91 steel exposed to 95%CO2-4%H2O-1%O2 with/without 0.1% SO2 at 1 atm and 550, 600, 650° C for up to 3000 h to establish the temperature-dependence of these processes. SO2 showed little effect on oxidation at 550-600° C but reduced carburization, while the combination of SO2 and faster alloy diffusion at 650° C resulted in significant reduction in both oxidation and carburization.},

  doi          = {10.1016/j.corsci.2022.110147},

  journal      = {Corrosion Science},

  number       = ,

  volume       = 198,

  place        = {United States},

  year         = {Tue Feb 01 00:00:00 EST 2022},

  month        = {Tue Feb 01 00:00:00 EST 2022}

}

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Title: Temperature-dependence of oxidation and carburization of Grade 91 steel in CO2 containing impurities

Abstract

Citation Formats

Effect of pressure on supercritical CO 2 compatibility of structural alloys at 750 °C : Effect of pressure on supercritical CO journal, April 2016

Corrosion Behaviour of Fe–Cr–(Mn, Si) Ferritic Alloys in Wet and Dry CO2–SO2 Atmospheres at 650 °C journal, December 2017

Oxy-fuel combustion technology for coal-fired power generation journal, January 2005

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Anomalous temperature dependence of oxidation kinetics during steam oxidation of ferritic steels in the temperature range 550–650 °C journal, September 2004

Influence of novel cycle concepts on the high-temperature corrosion of power plants journal, May 2008

Corrosion of 9Cr Steel in CO2 at Intermediate Temperature I: Mechanism of Void-Induced Duplex Oxide Formation journal, September 2011

Carburisation of ferritic Fe–Cr alloys by low carbon activity gases journal, September 2011

Non-steady state carburisation of martensitic 9–12%Cr steels in CO2 rich gases at 550°C journal, November 2014

Creep of MARBN-type 9Cr martensitic steel in gaseous CO2 environment journal, October 2021

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Corrosion behavior and lifetime prediction of VM12, Sanicro 25 and Inconel 617 in supercritical carbon dioxide at 600 °C journal, October 2020

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Corrosion of Fe–9Cr–(Mn, Si) alloys in CO2–H2O–SO2 gases journal, September 2015

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Comparison of the corrosion of materials in supercritical carbon dioxide, air, and argon environments journal, November 2021

Title: Temperature-dependence of oxidation and carburization of Grade 91 steel in CO₂ containing impurities

Effect of pressure on supercritical CO ₂ compatibility of structural alloys at 750 °C : Effect of pressure on supercritical CO
journal, April 2016

Corrosion Behaviour of Fe–Cr–(Mn, Si) Ferritic Alloys in Wet and Dry CO2–SO2 Atmospheres at 650 °C
journal, December 2017

Oxy-fuel combustion technology for coal-fired power generation
journal, January 2005

High-Temperature Oxidation of Steels in Direct-Fired CO2 Power Cycle Environments
journal, October 2021

Anomalous temperature dependence of oxidation kinetics during steam oxidation of ferritic steels in the temperature range 550–650 °C
journal, September 2004

Influence of novel cycle concepts on the high-temperature corrosion of power plants
journal, May 2008

Corrosion of 9Cr Steel in CO2 at Intermediate Temperature I: Mechanism of Void-Induced Duplex Oxide Formation
journal, September 2011

Carburisation of ferritic Fe–Cr alloys by low carbon activity gases
journal, September 2011

Non-steady state carburisation of martensitic 9–12%Cr steels in CO2 rich gases at 550°C
journal, November 2014

Creep of MARBN-type 9Cr martensitic steel in gaseous CO2 environment
journal, October 2021

Effect of Specimen Thickness on the Degradation of Mechanical Properties of Ferritic-Martensitic P91 Steel by Direct-fired Supercritical CO2 Power Cycle Environment
journal, November 2020

Corrosion behavior and lifetime prediction of VM12, Sanicro 25 and Inconel 617 in supercritical carbon dioxide at 600 °C
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Effect of Surface Finish on High-Temperature Oxidation of Steels in CO2, Supercritical CO2, and Air
journal, October 2019

Effect of Alloy Composition and Exposure Conditions on the Selective Oxidation Behavior of Ferritic Fe–Cr and Fe–Cr–X Alloys
journal, September 2010

Effect of Sulphur on the Oxidation Behaviour of Possible Construction Materials for Heat Exchangers in Oxyfuel Plants in the Temperature Range 550–700 °C
journal, September 2017

The effect of microstructure on the oxidation and carburisation of 9Cr-1Mo steel exposed to CO2
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Mechanisms of Breakaway Oxidation and Application to a Chromia-Forming Steel
journal, January 1999

Compatibility of FBR structural materials with supercritical carbon dioxide
journal, September 2011

High temperature oxidation of steels in CO2 containing impurities
journal, March 2020

Corrosion of Fe–9Cr–(Mn, Si) alloys in CO2–H2O–SO2 gases
journal, September 2015

Corrosion of austenitic and ferritic-martensitic steels exposed to supercritical carbon dioxide
journal, October 2011

The oxidation behaviour of the 9 % Cr steel P92in CO ₂ - and H ₂ O-rich gases relevant to oxyfuel environments
journal, February 2010

Comparative Study on High Temperature Oxidation of T92 Steel in Dry and Wet Oxyfuel Environments
journal, July 2015

Effect of SO ₂ on oxidation of metallic materials in CO ₂ /H ₂ O-rich gases relevant to oxyfuel environments : Effect of SO
journal, December 2013

Effect of CO2 gas pressure on composition, growth rate, and structure of duplex oxide formed on 9Cr steel at 550 °C
journal, February 2020

Demonstration of the Allam Cycle: An Update on the Development Status of a High Efficiency Supercritical Carbon Dioxide Power Process Employing Full Carbon Capture
journal, July 2017

High-temperature Oxidation Behavior of 9Cr Ferritic-steel in Carbon Dioxide
journal, January 2014

On the breakaway oxidation of Fe9Cr1Mo steel in high pressure CO2
journal, May 2017

Adsorption of Carbon Dioxide, Water Vapor, Nitrogen, and Sulfur Dioxide on Activated Carbon for Capture from Flue Gases: Competitive Adsorption and Selectivity Aspects
journal, March 2021

High-Temperature Oxidation of Commercial Alloys in Supercritical CO2 and Related Power Cycle Environments
journal, June 2018

A study of breakaway oxidation of 9Cr–1Mo steel in a Hot CO ₂ atmosphere using Raman spectroscopy
journal, October 2017

Comparison of the corrosion of materials in supercritical carbon dioxide, air, and argon environments
journal, November 2021