Probing the electrolyte/electrode interface with vibrational sum frequency generation spectroscopy: A review

Chowdhury, Azhad U.; Muralidharan, Nitin; Daniel, Claus; Amin, Ruhul; Belharouak, Ilias

doi:10.1016/j.jpowsour.2021.230173

Title: Probing the electrolyte/electrode interface with vibrational sum frequency generation spectroscopy: A review

Journal Article · Sun Jun 20 00:00:00 UTC 2021 · Journal of Power Sources

DOI: https://doi.org/10.1016/j.jpowsour.2021.230173 · OSTI ID:1808390

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Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)

Over the past decades, Lithium-ion batteries have seen extensive improvements, and as a result are now the primary choice in many applications for their power, energy, and durability. In recent years, battery cost has reduced by orders of magnitude through adoption of new materials and processes. Despite these advances, interfaces in these battery systems are yet to be fully understood. This is seen as a major limitation to further increase cycle life, calendar life, abuse tolerance, and performances. A major obstacle is a lack of comprehensive understanding of the complex dynamic chemical processes occurring at the electrolyte/electrode interface. In this context, vibrational sum frequency generation (vSFG) spectroscopy possesses the unique capability of probing a molecularly thin interfacial layer to obtain molecular-level information through nonlinear optical interaction. Probing the molecular level processes at the interfaces using such a versatile technique would be a game changer in the advancement of current battery research knowledge. This review article summarizes recent vSFG studies on the electrolyte/electrode interface of various electrode materials and nonaqueous electrolytes for LIBs and discusses future research perspectives. Finally, overall, this focused review highlights the advantages and versatility of vSFG that can be used to further advance present-day battery research.

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Research Organization:: Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)

Sponsoring Organization:: USDOE

Grant/Contract Number:: AC05-00OR22725

OSTI ID:: 1808390

Journal Information:: Journal of Power Sources, Journal Name: Journal of Power Sources Vol. 506; ISSN 0378-7753

Publisher:: ElsevierCopyright Statement

Country of Publication:: United States

Language:: English

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Title: Probing the electrolyte/electrode interface with vibrational sum frequency generation spectroscopy: A review

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