Angular X-ray Cross-Correlation Analysis (AXCCA): Basic Concepts and Recent Applications to Soft Matter and Nanomaterials
Abstract
Angular X-ray cross-correlation analysis (AXCCA) is a technique which allows quantitative measurement of the angular anisotropy of X-ray diffraction patterns and provides insights into the orientational order in the system under investigation. This method is based on the evaluation of the angular cross-correlation function of the scattered intensity distribution on a two-dimensional (2D) detector and further averaging over many diffraction patterns for enhancement of the anisotropic signal. Over the last decade, AXCCA was successfully used to study the anisotropy in various soft matter systems, such as solutions of anisotropic particles, liquid crystals, colloidal crystals, superlattices composed by nanoparticles, etc. This review provides an introduction to the technique and gives a survey of the recent experimental work in which AXCCA in combination with micro- or nanofocused X-ray microscopy was used to study the orientational order in various soft matter systems.
- Authors:
-
[2];
[6]
- Univ. of California, San Diego, La Jolla, CA (United States). Dept. of Physics; Deutsches Elektronen-Synchrotron (DESY), Hamburg (Germany)
- European X-ray Free-Electron Laser (XFEL), Hamburg (Germany)
- Univ. of Tubingen (Germany). Inst. for Physical and Theoretical Chemistry; Univ. of Tubingen (Germany). Sensors & Analytics LISA+. Center for Light-Matter Interaction
- Univ. of Tubingen (Germany). Sensors & Analytics LISA+. Center for Light-Matter Interaction; Univ. of Tubingen (Germany). Inst. of Applied Physics
- Russian Academy of Sciences (RAS), Moscow (Russian Federation). Federal Scientific Research Center “Crystallography and Photonics”; Russian Academy of Sciences (RAS), Chernogolovka (Russian Federation). Inst. of Solid State Physics
- Deutsches Elektronen-Synchrotron (DESY), Hamburg (Germany); National Research Nuclear Univ., Moscow (Russian Federation). MEPhI (Moscow Engineering Physics Institute)
- Publication Date:
- Research Org.:
- Univ. of California, San Diego, CA (United States)
- Sponsoring Org.:
- USDOE Office of Science (SC), Basic Energy Sciences (BES). Materials Sciences & Engineering Division
- OSTI Identifier:
- 1801495
- Grant/Contract Number:
- SC0001805
- Resource Type:
- Accepted Manuscript
- Journal Name:
- Materials
- Additional Journal Information:
- Journal Volume: 12; Journal Issue: 21; Journal ID: ISSN 1996-1944
- Publisher:
- MDPI
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 36 MATERIALS SCIENCE; 37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY; 71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSICS; Chemistry; Materials Science; Metallurgy & Metallurgical Engineering; Physics
Citation Formats
Zaluzhnyy, Ivan, Kurta, Ruslan, Scheele, Marcus, Schreiber, Frank, Ostrovskii, Boris, and Vartanyants, Ivan. Angular X-ray Cross-Correlation Analysis (AXCCA): Basic Concepts and Recent Applications to Soft Matter and Nanomaterials. United States: N. p., 2019.
Web. doi:10.3390/ma12213464.
Zaluzhnyy, Ivan, Kurta, Ruslan, Scheele, Marcus, Schreiber, Frank, Ostrovskii, Boris, & Vartanyants, Ivan. Angular X-ray Cross-Correlation Analysis (AXCCA): Basic Concepts and Recent Applications to Soft Matter and Nanomaterials. United States. https://doi.org/10.3390/ma12213464
Zaluzhnyy, Ivan, Kurta, Ruslan, Scheele, Marcus, Schreiber, Frank, Ostrovskii, Boris, and Vartanyants, Ivan. Wed .
"Angular X-ray Cross-Correlation Analysis (AXCCA): Basic Concepts and Recent Applications to Soft Matter and Nanomaterials". United States. https://doi.org/10.3390/ma12213464. https://www.osti.gov/servlets/purl/1801495.
@article{osti_1801495,
title = {Angular X-ray Cross-Correlation Analysis (AXCCA): Basic Concepts and Recent Applications to Soft Matter and Nanomaterials},
author = {Zaluzhnyy, Ivan and Kurta, Ruslan and Scheele, Marcus and Schreiber, Frank and Ostrovskii, Boris and Vartanyants, Ivan},
abstractNote = {Angular X-ray cross-correlation analysis (AXCCA) is a technique which allows quantitative measurement of the angular anisotropy of X-ray diffraction patterns and provides insights into the orientational order in the system under investigation. This method is based on the evaluation of the angular cross-correlation function of the scattered intensity distribution on a two-dimensional (2D) detector and further averaging over many diffraction patterns for enhancement of the anisotropic signal. Over the last decade, AXCCA was successfully used to study the anisotropy in various soft matter systems, such as solutions of anisotropic particles, liquid crystals, colloidal crystals, superlattices composed by nanoparticles, etc. This review provides an introduction to the technique and gives a survey of the recent experimental work in which AXCCA in combination with micro- or nanofocused X-ray microscopy was used to study the orientational order in various soft matter systems.},
doi = {10.3390/ma12213464},
journal = {Materials},
number = 21,
volume = 12,
place = {United States},
year = {Wed Oct 23 00:00:00 EDT 2019},
month = {Wed Oct 23 00:00:00 EDT 2019}
}
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Works referencing / citing this record:
Structural Study of a Self-Assembled Gold Mesocrystal Grain by Coherent X-ray Diffraction Imaging
preprint, January 2021
- Carnis, J.; Kirner, F.; Lapkin, D.
- arXiv