Effects of Al:Si and (Al + Na):Si ratios on the properties of the international simple glass, part I: Physical properties

Reiser, Joelle T.; Lu, Xiaonan; Parruzot, Benjamin; Liu, Hongshen; Subramani, Tamilarasan; Kaya, Huseyin; Kissinger, Ryan M.; Crum, Jarrod V.; Ryan, Joseph V.; Navrotsky, Alexandra; Kim, Seong H.; Vienna, John D.

doi:10.1111/jace.17449

Title: Effects of Al:Si and (Al + Na):Si ratios on the properties of the international simple glass, part I: Physical properties

Journal Article · Sat Sep 26 00:00:00 UTC 2020 · Journal of the American Ceramic Society

DOI: https://doi.org/10.1111/jace.17449 · OSTI ID:1787120

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^[3]; Kaya, Huseyin ^[4];

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Energy and Environment Directorate Pacific Northwest National Laboratory Richland WA USA
Department of Chemical Engineering Materials Research Institute Pennsylvania State University University Park PA USA
School of Molecular Sciences and Center for Materials of the Universe Arizona State University Tempe AZ USA
Department of Materials Science &, Engineering Pennsylvania State University University Park PA USA

Abstract Understanding composition‐structure‐property relationships of high‐alumina nuclear waste glasses are important for vitrification of nuclear waste at the Hanford Site. Two series of glasses were designed, one with varying Al:Si ratios and the other with (Al + Na):Si ratios based on the international simple glass (ISG, a simplified nuclear waste model glass), with Al ₂ O ₃ ranging from 0 to 23 mol% (0 to 32 wt%). The glasses were synthesized and characterized using electron probe microanalysis, X‐ray photoelectron spectroscopy, small angle X‐ray scattering, high‐temperature oxide melt solution calorimetry, and infrared spectroscopy. Glasses were crystal free, and the lowest Na ₂ O and Al ₂ O ₃ glass formed an immiscible glass phase. Evolution of various properties—glass‐transition temperature, percentage of 4‐coordinated B, enthalpy of glass formation—and infrared spectroscopy results indicate that structural effects differ based on the glass series.

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Sponsoring Organization:: USDOE

Grant/Contract Number:: SC0016584

OSTI ID:: 1787120

Journal Information:: Journal of the American Ceramic Society, Journal Name: Journal of the American Ceramic Society Journal Issue: 1 Vol. 104; ISSN 0002-7820

Publisher:: Wiley-BlackwellCopyright Statement

Country of Publication:: United States

Language:: English

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