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Title: Pronounced grain boundary network evolution in nanocrystalline Cu subjected to large cyclic strains

Abstract

The grain boundary network of nanocrystalline Cu foils was modified by the application of cyclic loadings and elevated temperatures. Broadly, the changes to the boundary network were directly correlated with the applied temperature and accumulated strain, including a 300% increase in the twin length fraction. By independently varying each treatment variable, a matrix of grain boundary statistics was built to check the plausibility of hypothesized mechanisms against their expected temperature and stress/strain dependences. These comparisons allow the field of candidate mechanisms to be significantly narrowed. Most importantly, the effects of temperature and strain on twin length fraction were found to be strongly synergistic, with the combined effect being ~150% that of the summed individual contributions. Looking beyond scalar metrics, an analysis of the grain boundary network showed that twin related domain formation favored larger sizes and repeated twin variant selection over the creation of many small domains with diverse variants.

Authors:
 [1];  [2];  [3];  [4]
  1. Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States); Univ. of California, Irvine, CA (United States)
  2. École Polytechnique Fédérale de Lausanne (Switzerland)
  3. Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States)
  4. Univ. of California, Irvine, CA (United States)
Publication Date:
Research Org.:
Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States)
Sponsoring Org.:
USDOE National Nuclear Security Administration (NNSA)
OSTI Identifier:
1633519
Report Number(s):
LLNL-JRNL-752223
Journal ID: ISSN 0884-2914; 938313
Grant/Contract Number:  
AC52-07NA27344
Resource Type:
Accepted Manuscript
Journal Name:
Journal of Materials Research
Additional Journal Information:
Journal Volume: 34; Journal Issue: 1; Journal ID: ISSN 0884-2914
Publisher:
Materials Research Society
Country of Publication:
United States
Language:
English
Subject:
36 MATERIALS SCIENCE; Nanostructure; grain boundaries; fatigue

Citation Formats

Bober, David B., LaGrange, Thomas, Kumar, Mukul, and Rupert, Timothy J. Pronounced grain boundary network evolution in nanocrystalline Cu subjected to large cyclic strains. United States: N. p., 2018. Web. doi:10.1557/jmr.2018.334.
Bober, David B., LaGrange, Thomas, Kumar, Mukul, & Rupert, Timothy J. Pronounced grain boundary network evolution in nanocrystalline Cu subjected to large cyclic strains. United States. https://doi.org/10.1557/jmr.2018.334
Bober, David B., LaGrange, Thomas, Kumar, Mukul, and Rupert, Timothy J. Tue . "Pronounced grain boundary network evolution in nanocrystalline Cu subjected to large cyclic strains". United States. https://doi.org/10.1557/jmr.2018.334. https://www.osti.gov/servlets/purl/1633519.
@article{osti_1633519,
title = {Pronounced grain boundary network evolution in nanocrystalline Cu subjected to large cyclic strains},
author = {Bober, David B. and LaGrange, Thomas and Kumar, Mukul and Rupert, Timothy J.},
abstractNote = {The grain boundary network of nanocrystalline Cu foils was modified by the application of cyclic loadings and elevated temperatures. Broadly, the changes to the boundary network were directly correlated with the applied temperature and accumulated strain, including a 300% increase in the twin length fraction. By independently varying each treatment variable, a matrix of grain boundary statistics was built to check the plausibility of hypothesized mechanisms against their expected temperature and stress/strain dependences. These comparisons allow the field of candidate mechanisms to be significantly narrowed. Most importantly, the effects of temperature and strain on twin length fraction were found to be strongly synergistic, with the combined effect being ~150% that of the summed individual contributions. Looking beyond scalar metrics, an analysis of the grain boundary network showed that twin related domain formation favored larger sizes and repeated twin variant selection over the creation of many small domains with diverse variants.},
doi = {10.1557/jmr.2018.334},
journal = {Journal of Materials Research},
number = 1,
volume = 34,
place = {United States},
year = {Tue Nov 13 00:00:00 EST 2018},
month = {Tue Nov 13 00:00:00 EST 2018}
}

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