Cryogenic goniometer for measurements in pulsed magnetic fields fabricated via additive manufacturing technique

Willis, Ximone; Ding, Xiaxin; Singleton, John; Balakirev, Fedor F.

doi:10.1063/1.5125792

Title: Cryogenic goniometer for measurements in pulsed magnetic fields fabricated via additive manufacturing technique

Abstract

Complex high-precision mechanical devices can be fabricated using 3-dimensional printing technology with the help of computer-aided design. Using 3D stereolithography, we have constructed a cryogenic goniometer for measurements in pulsed magnetic fields of up to 100 T, at temperatures as low as 0.5 K. We review the properties of several materials tested in developing the goniometer and report on its design and performance. The goniometer allows samples to be rotated in situ to a precision of 0.2 deg, so that the field can be applied at many different angles to the samples’ symmetry directions. Following its success, we establish that 3D printing is now a viable technology for pulsed-field and other cryogenic probes.

Authors:

Willis, Ximone ^[1];

^[2];

^[2]

Univ. of Texas at Dallas, Richardson, TX (United States)
Los Alamos National Lab. (LANL), Los Alamos, NM (United States)

Publication Date:: 2020-03-06

Research Org.:: Idaho National Lab. (INL), Idaho Falls, ID (United States); Los Alamos National Lab. (LANL), Los Alamos, NM (United States)

Sponsoring Org.:: National Science Foundation (NSF); State of Florida; USDOE Office of Science (SC); USDOE Laboratory Directed Research and Development (LDRD) Program

OSTI Identifier:: 1604075

Alternate Identifier(s):: OSTI ID: 1634952

Report Number(s):: INL/JOU-20-57525-Rev000; LA-UR-19-21531
Journal ID: ISSN 0034-6748; TRN: US2104195

Grant/Contract Number:: AC07-05ID14517; 89233218CNA000001

Resource Type:: Accepted Manuscript

Journal Name:: Review of Scientific Instruments

Additional Journal Information:: Journal Volume: 91; Journal Issue: 3; Journal ID: ISSN 0034-6748

Publisher:: American Institute of Physics (AIP)

Country of Publication:: United States

Language:: English

Subject:: 47 OTHER INSTRUMENTATION; pulsed magnet; rotator; 3D printing; High Magnetic Field Science

Citation Formats


                    Willis, Ximone, Ding, Xiaxin, Singleton, John, and Balakirev, Fedor F. Cryogenic goniometer for measurements in pulsed magnetic fields fabricated via additive manufacturing technique.  United States: N. p., 2020. 
Web.  doi:10.1063/1.5125792.

Copy to clipboard


                    Willis, Ximone, Ding, Xiaxin, Singleton, John, & Balakirev, Fedor F. Cryogenic goniometer for measurements in pulsed magnetic fields fabricated via additive manufacturing technique.  United States.  https://doi.org/10.1063/1.5125792

Copy to clipboard


                    Willis, Ximone, Ding, Xiaxin, Singleton, John, and Balakirev, Fedor F. Fri .  
"Cryogenic goniometer for measurements in pulsed magnetic fields fabricated via additive manufacturing technique".  United States.  https://doi.org/10.1063/1.5125792.  https://www.osti.gov/servlets/purl/1604075.

Copy to clipboard


                    
@article{osti_1604075,

  title        = {Cryogenic goniometer for measurements in pulsed magnetic fields fabricated via additive manufacturing technique},

  author       = {Willis, Ximone and Ding, Xiaxin and Singleton, John and Balakirev, Fedor F.},

  abstractNote = {Complex high-precision mechanical devices can be fabricated using 3-dimensional printing technology with the help of computer-aided design. Using 3D stereolithography, we have constructed a cryogenic goniometer for measurements in pulsed magnetic fields of up to 100 T, at temperatures as low as 0.5 K. We review the properties of several materials tested in developing the goniometer and report on its design and performance. The goniometer allows samples to be rotated in situ to a precision of 0.2 deg, so that the field can be applied at many different angles to the samples’ symmetry directions. Following its success, we establish that 3D printing is now a viable technology for pulsed-field and other cryogenic probes.},

  doi          = {10.1063/1.5125792},

  journal      = {Review of Scientific Instruments},

  number       = 3,

  volume       = 91,

  place        = {United States},

  year         = {2020},

  month        = {3}

}

Copy to clipboard

Journal Article:

Free Publicly Available Full Text

Accepted Manuscript (DOE)

Publisher's Version of Record

https://doi.org/10.1063/1.5125792

Other availability

Search WorldCat to find libraries that may hold this journal

Save / Share:

Export Metadata

Save to My Library

Works referenced in this record:

Low Temperature Sample Holder Providing Two Degrees of Freedom in a Solenoid
journal, August 1965

Brennert, G. F.; Reed, W. A.; Fawcett, E.
Review of Scientific Instruments, Vol. 36, Issue 8
DOI: 10.1063/1.1719873

Nonmetallic gasket and miniature plastic turnbuckle diamond anvil cell for pulsed magnetic field studies at cryogenic temperatures
journal, December 2011

Graf, D. E.; Stillwell, R. L.; Purcell, K. M.
High Pressure Research, Vol. 31, Issue 4
DOI: 10.1080/08957959.2011.633909

From rapid prototyping to home fabrication: How 3D printing is changing business model innovation
journal, January 2016

Rayna, Thierry; Striukova, Ludmila
Technological Forecasting and Social Change, Vol. 102
DOI: 10.1016/j.techfore.2015.07.023

Development of a Two-Axis Rotator in Pulsed High Magnetic Fields for a Magnetic Torque Measurement
journal, January 2012

Kida, Takanori; Kotsuji, Hideyuki; Nishido, Junichi
Journal of the Physical Society of Japan, Vol. 81, Issue Suppl.B
DOI: 10.1143/JPSJS.81SB.SB067

Piezoelectrically driven rotator for use in high magnetic fields at low temperatures
journal, January 2001

Ohmichi, E.; Nagai, S.; Maeno, Y.
Review of Scientific Instruments, Vol. 72, Issue 3
DOI: 10.1063/1.1347982

Fermi-surface topologies and low-temperature phases of the filled skutterudite compounds ${CeOs}_{4} {Sb}_{12}$ and ${NdOs}_{4} {Sb}_{12}$
journal, November 2016

Ho, Pei Chun; Singleton, John; Goddard, Paul A.
Physical Review B, Vol. 94, Issue 20
DOI: 10.1103/physrevb.94.205140

Status and Development of Pulsed Magnets at the NHMFL Pulsed Field Facility
journal, June 2016

Nguyen, Doan N.; Michel, James; Mielke, Chuck H.
IEEE Transactions on Applied Superconductivity, Vol. 26, Issue 4
DOI: 10.1109/tasc.2016.2515982

Novel apparatuses for pulsed field experiments: piezoelectrically driven rotator and microcantilever
journal, May 2003

Ohmichi, E.
Physica B: Condensed Matter, Vol. 329-333
DOI: 10.1016/s0921-4526(02)02438-9

Superconducting properties and Fermi-surface topology of the quasi-two-dimensional organic superconductor λ-(BETS) ₂ GaCl ₄ (BETS≡bis(ethylene-dithio)tetraselenafulvalene)
journal, August 2001

Mielke, Charles; Singleton, John; Nam, Moon-Sun
Journal of Physics: Condensed Matter, Vol. 13, Issue 36
DOI: 10.1088/0953-8984/13/36/308

Very low friction rotator for use at low temperatures and high magnetic fields
journal, January 1999

Palm, E. C.; Murphy, T. P.
Review of Scientific Instruments, Vol. 70, Issue 1
DOI: 10.1063/1.1149571

Measurement of the angle dependence of magnetostriction in pulsed magnetic fields using a piezoelectric strain gauge
journal, August 2018

Ding, Xiaxin; Chai, Yi-Sheng; Balakirev, Fedor
Review of Scientific Instruments, Vol. 89, Issue 8
DOI: 10.1063/1.5038741

A 3He Cryostat for Scientific Measurements in Pulsed High Magnetic Fields
journal, January 2015

Wang, Shaoliang; Li, Liang; Liu, Mengyu
Physics Procedia, Vol. 67
DOI: 10.1016/j.phpro.2015.06.125

Fragile charge order in the nonsuperconducting ground state of the underdoped high-temperature superconductors
journal, July 2015

Tan, B. S.; Harrison, N.; Zhu, Z.
Proceedings of the National Academy of Sciences, Vol. 112, Issue 31
DOI: 10.1073/pnas.1504164112

Similar Records in DOE PAGES and OSTI.GOV collections:

Eucentric four-axis ultrahigh vacuum goniometer for reflection high-energy electron diffraction applications

Journal Article Schmehl, A ; Schulz, R R ; Mannhart, J - Review of Scientific Instruments

The design and performance of a four-axis low-profile eucentric UHV goniometer for in situ reflection high-energy electron diffraction (RHEED) studies during film deposition is reported. The design provides one translational and three rotational degrees of freedom that are fully independent. Although developed to facilitate high-pressure RHEED during the growth of oxide thin films by pulsed laser deposition, this goniometer design is applicable to other UHV techniques including molecular beam epitaxy. The goniometer requires only a single DN 100 CF flange (6 in. o.d., 100 mm i.d.), making it suitable for small deposition systems, too. Samples, attached to a resistively heatedmore »« less
https://doi.org/10.1063/1.2138687
Revealing meso-structure dynamics in additive manufacturing of energy storage via operando coherent X-ray scattering

Journal Article Lin, Cheng-Hung ; Dyro, Karol ; Chen, Olivia ; ... - Applied Materials Today

3D printing is an emerging technology for the fabrication of energy storage devices, offering advantages over traditional manufacturing methods. However, optimization and design of such devices requires an understanding of the meso-structure formation during the 3D printing process. This study utilizes operando coherent X-ray scattering, X-ray Photon Correlation Spectroscopy (XPCS), to study the spatiotemporally-resolved far-from-equilibrium dynamics during direct ink writing 3D printing. Here, Lithium Titanate (LTO) based ink is prepared and rheologically tested for its shear-thinning properties. Two-time intensity-intensity functions are calculated to be used in subsequent quantitative analysis, which allows for an overall characterization of the dynamics, description ofmore »« less
https://doi.org/10.1016/j.apmt.2021.101075

Full Text Available
Imaging of Calibrated Defects in Additively Manufactured Materials: Pulsed Thermal Tomography Nondestructive Examination of Additively Manufactured Reactor Materials and Components

Technical Report Heifetz, Alexander ; Zhang, Xin ; Saniie, Jafar ; ...

Additive manufacturing (AM, or 3D printing) for commercial nuclear energy applications is an emerging method for cost-efficient manufacturing aimed at replacing aging nuclear reactor parts and reducing costs for new construction. Known material flaws in AM include low-density regions consisting of non-sintered powder, which have to be detected to ensure the safety of long-term performance nuclear reactor components. Currently, limited options are available for nondestructive evaluation (NDE), either during or post manufacturing. As a solution to NDE of AM, we are developing pulsed thermal imaging which is non-contact, one-sided, and scalable to arbitrary size and shape of the AM parts.more »« less
https://doi.org/10.2172/1617371

Full Text Available
Prototype casting fabrication by stereolithography

Conference Cromwell, W E

A new product development technology is emerging which could have a major impact on the investment casting industry. It's identified by several names, the most common of which is STEREOLITHOGRAPHY.'' This technology involves a three-dimensional printing process which will yield plastic parts (polymer models) from solid, surface, or wireframe CAD files. The concept links a CAD database to a process which guides a laser beam to solidify liquid photo-curable polymer into a programmed shaped. The process can produce models in far less time and at far less cost than can be done by other known (conventional) model producing methods. Partsmore »« less
Full Text Available
Design and additive manufacturing of optimized electrodes for energy storage applications

Journal Article Reale Batista, Mariana Desireé ; Chandrasekaran, Swetha ; Moran, Bryan D. ; ... - Carbon

Supercapacitors exhibit fast charging/discharging ability and have attracted considerable attention within the automotive, aerospace, and telecommunication industries. Porous carbons, prized for their high electrical conductivity and high surface area, have been attractive candidates for supercapacitor electrodes. Moving to thick electrodes is one strategy to further increase energy density due to a higher volume fraction of active material. However, thick electrodes suffer from sluggish charged species transport, which is why thin electrodes are currently favored. In this work, we investigate the use of computational optimization and additive manufacturing to design and fabricate thick porous electrodes with improved performance. Electrode performance wasmore »« less
https://doi.org/10.1016/j.carbon.2023.01.044

Similar Records

Title: Cryogenic goniometer for measurements in pulsed magnetic fields fabricated via additive manufacturing technique

Abstract

Citation Formats

Low Temperature Sample Holder Providing Two Degrees of Freedom in a Solenoid journal, August 1965

Nonmetallic gasket and miniature plastic turnbuckle diamond anvil cell for pulsed magnetic field studies at cryogenic temperatures journal, December 2011

From rapid prototyping to home fabrication: How 3D printing is changing business model innovation journal, January 2016

Development of a Two-Axis Rotator in Pulsed High Magnetic Fields for a Magnetic Torque Measurement journal, January 2012

Piezoelectrically driven rotator for use in high magnetic fields at low temperatures journal, January 2001

Fermi-surface topologies and low-temperature phases of the filled skutterudite compounds CeOs 4 Sb 12 and NdOs 4 Sb 12 journal, November 2016

Status and Development of Pulsed Magnets at the NHMFL Pulsed Field Facility journal, June 2016

Novel apparatuses for pulsed field experiments: piezoelectrically driven rotator and microcantilever journal, May 2003

Superconducting properties and Fermi-surface topology of the quasi-two-dimensional organic superconductor λ-(BETS) 2 GaCl 4 (BETS≡bis(ethylene-dithio)tetraselenafulvalene) journal, August 2001

Very low friction rotator for use at low temperatures and high magnetic fields journal, January 1999

Measurement of the angle dependence of magnetostriction in pulsed magnetic fields using a piezoelectric strain gauge journal, August 2018

A 3He Cryostat for Scientific Measurements in Pulsed High Magnetic Fields journal, January 2015

Fragile charge order in the nonsuperconducting ground state of the underdoped high-temperature superconductors journal, July 2015

Low Temperature Sample Holder Providing Two Degrees of Freedom in a Solenoid
journal, August 1965

Nonmetallic gasket and miniature plastic turnbuckle diamond anvil cell for pulsed magnetic field studies at cryogenic temperatures
journal, December 2011

From rapid prototyping to home fabrication: How 3D printing is changing business model innovation
journal, January 2016

Development of a Two-Axis Rotator in Pulsed High Magnetic Fields for a Magnetic Torque Measurement
journal, January 2012

Piezoelectrically driven rotator for use in high magnetic fields at low temperatures
journal, January 2001

Fermi-surface topologies and low-temperature phases of the filled skutterudite compounds ${CeOs}_{4} {Sb}_{12}$ and ${NdOs}_{4} {Sb}_{12}$
journal, November 2016

Status and Development of Pulsed Magnets at the NHMFL Pulsed Field Facility
journal, June 2016

Novel apparatuses for pulsed field experiments: piezoelectrically driven rotator and microcantilever
journal, May 2003

Superconducting properties and Fermi-surface topology of the quasi-two-dimensional organic superconductor λ-(BETS) ₂ GaCl ₄ (BETS≡bis(ethylene-dithio)tetraselenafulvalene)
journal, August 2001

Very low friction rotator for use at low temperatures and high magnetic fields
journal, January 1999

Measurement of the angle dependence of magnetostriction in pulsed magnetic fields using a piezoelectric strain gauge
journal, August 2018

A 3He Cryostat for Scientific Measurements in Pulsed High Magnetic Fields
journal, January 2015

Fragile charge order in the nonsuperconducting ground state of the underdoped high-temperature superconductors
journal, July 2015