75As NMR Studies of Magnetic Properties of the Magnetic Superconductor CaK(Fe0.967Ni0.033)4As4

Ding, Qing Ping; Meier, William R.; Böhmer, Anna E.; Budk'o, Sergey L.; Canfield, Paul C.; Furukawa, Yuji

doi:10.4028/www.scientific.net/SSP.289.148

Title: ⁷⁵As NMR Studies of Magnetic Properties of the Magnetic Superconductor CaK(Fe_0.967Ni_0.033)₄As₄

Abstract

We have carried out ⁷⁵As nuclear magnetic resonance (NMR) measurements to investigate a new antiferromagnetic (AFM) state, the so-called hedgehog spin-vortex crystal (SVC) in CaK(Fe_0.9₆₇Ni_0.0₃₃)₄As₄. Here, the hedgehog SVC order is clearly demonstrated by the direct observation of internal magnetic induction along the c axis at the As1 site (close to K) and a zero net internal magnetic induction at the As2 site (close to Ca) below an AFM ordering temperature of T_N~ 45 K. In the superconducting (SC) state, the NMR signal intensity decreases suddenly just below T_c~ 20 K due to Meissner effect, evidencing the coexistence of the hedgehog SVC AFM and SC states from a microscopic point of view.

Authors:

^[1]; Meier, William R. ^[1]; Böhmer, Anna E. ^[2]; Budk'o, Sergey L. ^[1]; Canfield, Paul C. ^[1]; Furukawa, Yuji ^[1]

Ames Lab. and Iowa State Univ., Ames, IA (United States)
Ames Lab. and Iowa State Univ., Ames, IA (United States); Karlsruhe Institute of Technology, Karlsruhe (Germany)

Publication Date:: Mon Apr 01 00:00:00 EDT 2019

Research Org.:: Ames Laboratory (AMES), Ames, IA (United States)

Sponsoring Org.:: USDOE

OSTI Identifier:: 1560623

Report Number(s):: IS-J-10015
Journal ID: ISSN 1662-9779; SSP; TRN: US2000522

Grant/Contract Number:: AC02-07CH11358

Resource Type:: Accepted Manuscript

Journal Name:: Solid State Phenomena (Online)

Additional Journal Information:: Journal Name: Solid State Phenomena (Online); Journal Volume: 289; Journal ID: ISSN 1662-9779

Publisher:: Trans Tech Publications

Country of Publication:: United States

Language:: English

Subject:: 75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND SUPERFLUIDITY; Antiferromagnetic State; Iron Based Superconductor; Nuclear Magnetic Resonance; Spin-Vortex Crystal

Citation Formats


                    Ding, Qing Ping, Meier, William R., Böhmer, Anna E., Budk'o, Sergey L., Canfield, Paul C., and Furukawa, Yuji. 75As NMR Studies of Magnetic Properties of the Magnetic Superconductor CaK(Fe0.967Ni0.033)4As4.  United States: N. p., 2019. 
Web.  doi:10.4028/www.scientific.net/SSP.289.148.

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                    Ding, Qing Ping, Meier, William R., Böhmer, Anna E., Budk'o, Sergey L., Canfield, Paul C., & Furukawa, Yuji. 75As NMR Studies of Magnetic Properties of the Magnetic Superconductor CaK(Fe0.967Ni0.033)4As4.  United States.  https://doi.org/10.4028/www.scientific.net/SSP.289.148

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                    Ding, Qing Ping, Meier, William R., Böhmer, Anna E., Budk'o, Sergey L., Canfield, Paul C., and Furukawa, Yuji. Mon .  
"75As NMR Studies of Magnetic Properties of the Magnetic Superconductor CaK(Fe0.967Ni0.033)4As4".  United States.  https://doi.org/10.4028/www.scientific.net/SSP.289.148.  https://www.osti.gov/servlets/purl/1560623.

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@article{osti_1560623,

  title        = {75As NMR Studies of Magnetic Properties of the Magnetic Superconductor CaK(Fe0.967Ni0.033)4As4},

  author       = {Ding, Qing Ping and Meier, William R. and Böhmer, Anna E. and Budk'o, Sergey L. and Canfield, Paul C. and Furukawa, Yuji},

  abstractNote = {We have carried out 75As nuclear magnetic resonance (NMR) measurements to investigate a new antiferromagnetic (AFM) state, the so-called hedgehog spin-vortex crystal (SVC) in CaK(Fe0.967Ni0.033)4As4. Here, the hedgehog SVC order is clearly demonstrated by the direct observation of internal magnetic induction along the c axis at the As1 site (close to K) and a zero net internal magnetic induction at the As2 site (close to Ca) below an AFM ordering temperature of TN~ 45 K. In the superconducting (SC) state, the NMR signal intensity decreases suddenly just below Tc~ 20 K due to Meissner effect, evidencing the coexistence of the hedgehog SVC AFM and SC states from a microscopic point of view.},

  doi          = {10.4028/www.scientific.net/SSP.289.148},

  journal      = {Solid State Phenomena (Online)},

  number       = ,

  volume       = 289,

  place        = {United States},

  year         = {Mon Apr 01 00:00:00 EDT 2019},

  month        = {Mon Apr 01 00:00:00 EDT 2019}

}

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Works referenced in this record:

Pressure-induced Fermi-surface reconstruction in the iron-arsenide superconductor Ba $_{1 - x}$ K $_{x}$ Fe $_{2}$ As $_{2}$ : Evidence of a phase transition inside the antiferromagnetic phase
journal, October 2012

Hassinger, E.; Gredat, G.; Valade, F.
Physical Review B, Vol. 86, Issue 14
DOI: 10.1103/physrevb.86.140502

FeAs-Based Superconductivity: A Case Study of the Effects of Transition Metal Doping on BaFe ₂ As ₂
journal, August 2010

Canfield, Paul C.; Bud'ko, Sergey L.
Annual Review of Condensed Matter Physics, Vol. 1, Issue 1
DOI: 10.1146/annurev-conmatphys-070909-104041

Complex phase diagram of ${Ba}_{1 - x} {Na}_{x} {Fe}_{2} {As}_{2}$ : A multitude of phases striving for the electronic entropy
journal, January 2016

Wang, L.; Hardy, F.; Böhmer, A. E.
Physical Review B, Vol. 93, Issue 1
DOI: 10.1103/PhysRevB.93.014514

Magnetic fluctuations and superconducting properties of ${CaKFe}_{4} {As}_{4}$ studied by ${}^{75}{As}$ NMR
journal, September 2017

Cui, J.; Ding, Q. -P.; Meier, W. R.
Physical Review B, Vol. 96, Issue 10
DOI: 10.1103/PhysRevB.96.104512

Double-Q spin-density wave in iron arsenide superconductors
journal, January 2016

Allred, J. M.; Taddei, K. M.; Bugaris, D. E.
Nature Physics, Vol. 12, Issue 5
DOI: 10.1038/nphys3629

Vestigial chiral and charge orders from bidirectional spin-density waves: Application to the iron-based superconductors
journal, January 2016

Fernandes, R. M.; Kivelson, S. A.; Berg, E.
Physical Review B, Vol. 93, Issue 1
DOI: 10.1103/PhysRevB.93.014511

Disorder-promoted $C_{4}$ -symmetric magnetic order in iron-based superconductors
journal, April 2016

Hoyer, Mareike; Fernandes, Rafael M.; Levchenko, Alex
Physical Review B, Vol. 93, Issue 14
DOI: 10.1103/PhysRevB.93.144414

Hedgehog spin-vortex crystal stabilized in a hole-doped iron-based superconductor
journal, February 2018

Meier, William R.; Ding, Qing-Ping; Kreyssig, Andreas
npj Quantum Materials, Vol. 3, Issue 1
DOI: 10.1038/s41535-017-0076-x

Optimization of the crystal growth of the superconductor ${CaKFe}_{4} {As}_{4}$ from solution in the $FeAs − {CaFe}_{2} {As}_{2} − {KFe}_{2} {As}_{2}$ system
journal, June 2017

Meier, W. R.; Kong, T.; Bud'ko, S. L.
Physical Review Materials, Vol. 1, Issue 1
DOI: 10.1103/PhysRevMaterials.1.013401

Superconductivity in iron compounds
journal, December 2011

Stewart, G. R.
Reviews of Modern Physics, Vol. 83, Issue 4
DOI: 10.1103/RevModPhys.83.1589

Magnetically driven suppression of nematic order in an iron-based superconductor
journal, May 2014

Avci, S.; Chmaissem, O.; Allred, J. M.
Nature Communications, Vol. 5, Issue 1
DOI: 10.1038/ncomms4845

New-Structure-Type Fe-Based Superconductors: Ca A Fe ₄ As ₄ ( A = K, Rb, Cs) and Sr A Fe ₄ As ₄ ( A = Rb, Cs)
journal, March 2016

Iyo, Akira; Kawashima, Kenji; Kinjo, Tatsuya
Journal of the American Chemical Society, Vol. 138, Issue 10
DOI: 10.1021/jacs.5b12571

Stabilizing the spin vortex crystal phase in two-dimensional iron-based superconductors
journal, February 2017

O'Halloran, Joseph; Agterberg, D. F.; Chen, M. X.
Physical Review B, Vol. 95, Issue 7
DOI: 10.1103/PhysRevB.95.075104

Enhancement of the Superconducting Gap by Nesting in ${CaKFe}_{4} {As}_{4}$ : A New High Temperature Superconductor
journal, December 2016

Mou, Daixiang; Kong, Tai; Meier, William R.
Physical Review Letters, Vol. 117, Issue 27
DOI: 10.1103/PhysRevLett.117.277001

Principles of Magnetic Resonance
book, January 1990

Slichter, Charles P.
Springer Series in Solid-State Sciences
DOI: 10.1007/978-3-662-09441-9

Antiferromagnetic ordering in the absence of structural distortion in $Ba {({Fe}_{1 - x} {Mn}_{x})}_{2} {As}_{2}$
journal, December 2010

Kim, M. G.; Kreyssig, A.; Thaler, A.
Physical Review B, Vol. 82, Issue 22
DOI: 10.1103/PhysRevB.82.220503

The puzzle of high temperature superconductivity in layered iron pnictides and chalcogenides
journal, October 2010

Johnston, David C.
Advances in Physics, Vol. 59, Issue 6
DOI: 10.1080/00018732.2010.513480

Principles of Magnetic Resonance
journal, January 1991

Radeglia, R.
Zeitschrift für Physikalische Chemie, Vol. 173, Issue 1
DOI: 10.1524/zpch.1991.173.part_1.127

FeAs-based superconductivity: a case study of the effects of transition metal doping on BaFe2As2
text, January 2010

Canfield, Paul C.; Bud'ko, Sergey L.
arXiv
DOI: 10.48550/arxiv.1002.0858

Superconductivity in Iron Compounds
text, January 2011

Stewart, G. R.
arXiv
DOI: 10.48550/arxiv.1106.1618

Magnetically-Driven Suppression of Nematic Order in an Iron-Based Superconductor
text, January 2013

Avci, Sevda; Chmaissem, Omar; Rosenkranz, Stephan
arXiv
DOI: 10.48550/arxiv.1303.2647

Vestigial chiral and charge orders from bidirectional spin-density waves: Application to the iron-based superconductors
text, January 2015

Fernandes, R. M.; Kivelson, S. A.; Berg, E.
arXiv
DOI: 10.48550/arxiv.1504.03656

Double-Q spin-density wave in iron arsenide superconductors
text, January 2015

Allred, J. M.; Taddei, K. M.; Bugaris, D. E.
arXiv
DOI: 10.48550/arxiv.1505.06175

Complex phase diagram of Ba$_{1-x}$Na$_{x}$Fe$_{2}$As$_{2}$: a multitude of phases striving for the electronic entropy
text, January 2015

Wang, Liran; Hardy, F.; Böhmer, A.
arXiv
DOI: 10.48550/arxiv.1510.03685

Hedgehog spin-vortex crystal stabilized in a hole-doped iron-based superconductor
text, January 2017

Meier, W. R.; Ding, Q. -P.; Kreyssig, A.
arXiv
DOI: 10.48550/arxiv.1706.01067

Spin Resonance in the New-Structure-Type Iron-Based Superconductor CaKFe4As4
text, January 2017

Iida, K.; Ishikado, M.; Nagai, Y.
arXiv
DOI: 10.48550/arxiv.1708.01006

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Similar Records

Title: 75As NMR Studies of Magnetic Properties of the Magnetic Superconductor CaK(Fe0.967Ni0.033)4As4

Abstract

Citation Formats

Pressure-induced Fermi-surface reconstruction in the iron-arsenide superconductor Ba 1 − x K x Fe 2 As 2 : Evidence of a phase transition inside the antiferromagnetic phase journal, October 2012

FeAs-Based Superconductivity: A Case Study of the Effects of Transition Metal Doping on BaFe 2 As 2 journal, August 2010

Complex phase diagram of Ba 1 − x Na x Fe 2 As 2 : A multitude of phases striving for the electronic entropy journal, January 2016

Magnetic fluctuations and superconducting properties of CaKFe 4 As 4 studied by As 75 NMR journal, September 2017

Double-Q spin-density wave in iron arsenide superconductors journal, January 2016

Vestigial chiral and charge orders from bidirectional spin-density waves: Application to the iron-based superconductors journal, January 2016

Disorder-promoted C 4 -symmetric magnetic order in iron-based superconductors journal, April 2016

Hedgehog spin-vortex crystal stabilized in a hole-doped iron-based superconductor journal, February 2018

Optimization of the crystal growth of the superconductor CaKFe 4 As 4 from solution in the FeAs − CaFe 2 As 2 − KFe 2 As 2 system journal, June 2017

Superconductivity in iron compounds journal, December 2011

Magnetically driven suppression of nematic order in an iron-based superconductor journal, May 2014

New-Structure-Type Fe-Based Superconductors: Ca A Fe 4 As 4 ( A = K, Rb, Cs) and Sr A Fe 4 As 4 ( A = Rb, Cs) journal, March 2016

Stabilizing the spin vortex crystal phase in two-dimensional iron-based superconductors journal, February 2017

Enhancement of the Superconducting Gap by Nesting in CaKFe 4 As 4 : A New High Temperature Superconductor journal, December 2016

Principles of Magnetic Resonance book, January 1990

Antiferromagnetic ordering in the absence of structural distortion in Ba ( Fe 1 − x Mn x ) 2 As 2 journal, December 2010

The puzzle of high temperature superconductivity in layered iron pnictides and chalcogenides journal, October 2010

Principles of Magnetic Resonance journal, January 1991

FeAs-based superconductivity: a case study of the effects of transition metal doping on BaFe2As2 text, January 2010

Superconductivity in Iron Compounds text, January 2011

Magnetically-Driven Suppression of Nematic Order in an Iron-Based Superconductor text, January 2013

Vestigial chiral and charge orders from bidirectional spin-density waves: Application to the iron-based superconductors text, January 2015

Double-Q spin-density wave in iron arsenide superconductors text, January 2015

Complex phase diagram of Ba$_{1-x}$Na$_{x}$Fe$_{2}$As$_{2}$: a multitude of phases striving for the electronic entropy text, January 2015

Hedgehog spin-vortex crystal stabilized in a hole-doped iron-based superconductor text, January 2017

Spin Resonance in the New-Structure-Type Iron-Based Superconductor CaKFe4As4 text, January 2017

Title: ⁷⁵As NMR Studies of Magnetic Properties of the Magnetic Superconductor CaK(Fe_0.967Ni_0.033)₄As₄

Pressure-induced Fermi-surface reconstruction in the iron-arsenide superconductor Ba $_{1 - x}$ K $_{x}$ Fe $_{2}$ As $_{2}$ : Evidence of a phase transition inside the antiferromagnetic phase
journal, October 2012

FeAs-Based Superconductivity: A Case Study of the Effects of Transition Metal Doping on BaFe ₂ As ₂
journal, August 2010

Complex phase diagram of ${Ba}_{1 - x} {Na}_{x} {Fe}_{2} {As}_{2}$ : A multitude of phases striving for the electronic entropy
journal, January 2016

Magnetic fluctuations and superconducting properties of ${CaKFe}_{4} {As}_{4}$ studied by ${}^{75}{As}$ NMR
journal, September 2017

Double-Q spin-density wave in iron arsenide superconductors
journal, January 2016

Vestigial chiral and charge orders from bidirectional spin-density waves: Application to the iron-based superconductors
journal, January 2016

Disorder-promoted $C_{4}$ -symmetric magnetic order in iron-based superconductors
journal, April 2016

Hedgehog spin-vortex crystal stabilized in a hole-doped iron-based superconductor
journal, February 2018

Optimization of the crystal growth of the superconductor ${CaKFe}_{4} {As}_{4}$ from solution in the $FeAs − {CaFe}_{2} {As}_{2} − {KFe}_{2} {As}_{2}$ system
journal, June 2017

Superconductivity in iron compounds
journal, December 2011

Magnetically driven suppression of nematic order in an iron-based superconductor
journal, May 2014

New-Structure-Type Fe-Based Superconductors: Ca A Fe ₄ As ₄ ( A = K, Rb, Cs) and Sr A Fe ₄ As ₄ ( A = Rb, Cs)
journal, March 2016

Stabilizing the spin vortex crystal phase in two-dimensional iron-based superconductors
journal, February 2017

Enhancement of the Superconducting Gap by Nesting in ${CaKFe}_{4} {As}_{4}$ : A New High Temperature Superconductor
journal, December 2016

Principles of Magnetic Resonance
book, January 1990

Antiferromagnetic ordering in the absence of structural distortion in $Ba {({Fe}_{1 - x} {Mn}_{x})}_{2} {As}_{2}$
journal, December 2010

The puzzle of high temperature superconductivity in layered iron pnictides and chalcogenides
journal, October 2010

Principles of Magnetic Resonance
journal, January 1991

FeAs-based superconductivity: a case study of the effects of transition metal doping on BaFe2As2
text, January 2010

Superconductivity in Iron Compounds
text, January 2011

Magnetically-Driven Suppression of Nematic Order in an Iron-Based Superconductor
text, January 2013

Vestigial chiral and charge orders from bidirectional spin-density waves: Application to the iron-based superconductors
text, January 2015

Double-Q spin-density wave in iron arsenide superconductors
text, January 2015

Complex phase diagram of Ba$_{1-x}$Na$_{x}$Fe$_{2}$As$_{2}$: a multitude of phases striving for the electronic entropy
text, January 2015

Hedgehog spin-vortex crystal stabilized in a hole-doped iron-based superconductor
text, January 2017

Spin Resonance in the New-Structure-Type Iron-Based Superconductor CaKFe4As4
text, January 2017