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Title: Clamp cell with in situ pressure monitoring for low-temperature neutron scattering measurements

Abstract

In this study, a clamp pressure cell for neutron scattering experiments at low temperatures and in external magnetic fields under pressure up to 2 GPa has been fabricated and tested. The cell provides optical access to the sample space that allows instantaneous pressure determination during sample loading, cooling and measuring using ruby and/or samarium doped strontium tetraborate fluorescence monitoring. Additionally, a new calibration curve of the pressure-induced shift of the 7D0-5F0 (0-0) line in the fluorescent spectrum of SrB4O7:Sm2+ for moderate pressures, P≤2 GPa, is given.

Authors:
ORCiD logo [1];  [1];  [1]; ORCiD logo [1];  [1]; ORCiD logo [2];  [1];  [1]; ORCiD logo [1]; ORCiD logo [1]
+ Show Author Affiliations
  1. Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States). Neutron Scattering Division
  2. Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States). Neutron Technologies Division
Publication Date:
Research Org.:
Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)
Sponsoring Org.:
USDOE Office of Science (SC), Basic Energy Sciences (BES)
OSTI Identifier:
1474603
Grant/Contract Number:  
AC05-00OR22725
Resource Type:
Accepted Manuscript
Journal Name:
High Pressure Research
Additional Journal Information:
Journal Volume: 38; Journal Issue: 4; Journal ID: ISSN 0895-7959
Publisher:
Taylor & Francis
Country of Publication:
United States
Language:
English
Subject:
46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND TECHNOLOGY; neutron scattering; pressure measurements; clamp cell; fluorescence

Citation Formats

Podlesnyak, Andrey A., Loguillo, Mark, Rucker, Gerald M., Haberl, Bianca, Boehler, Reinhard, Ehlers, Georg, Daemen, Luke L., Armitage, Douglas P., Frontzek, Matthias D., and Lumsden, Mark D.. Clamp cell with in situ pressure monitoring for low-temperature neutron scattering measurements. United States: N. p., 2018. Web. doi:10.1080/08957959.2018.1519560.
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Podlesnyak, Andrey A., Loguillo, Mark, Rucker, Gerald M., Haberl, Bianca, Boehler, Reinhard, Ehlers, Georg, Daemen, Luke L., Armitage, Douglas P., Frontzek, Matthias D., & Lumsden, Mark D.. Clamp cell with in situ pressure monitoring for low-temperature neutron scattering measurements. United States. https://doi.org/10.1080/08957959.2018.1519560
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Podlesnyak, Andrey A., Loguillo, Mark, Rucker, Gerald M., Haberl, Bianca, Boehler, Reinhard, Ehlers, Georg, Daemen, Luke L., Armitage, Douglas P., Frontzek, Matthias D., and Lumsden, Mark D.. Thu . "Clamp cell with in situ pressure monitoring for low-temperature neutron scattering measurements". United States. https://doi.org/10.1080/08957959.2018.1519560. https://www.osti.gov/servlets/purl/1474603.
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@article{osti_1474603,
title = {Clamp cell with in situ pressure monitoring for low-temperature neutron scattering measurements},
author = {Podlesnyak, Andrey A. and Loguillo, Mark and Rucker, Gerald M. and Haberl, Bianca and Boehler, Reinhard and Ehlers, Georg and Daemen, Luke L. and Armitage, Douglas P. and Frontzek, Matthias D. and Lumsden, Mark D.},
abstractNote = {In this study, a clamp pressure cell for neutron scattering experiments at low temperatures and in external magnetic fields under pressure up to 2 GPa has been fabricated and tested. The cell provides optical access to the sample space that allows instantaneous pressure determination during sample loading, cooling and measuring using ruby and/or samarium doped strontium tetraborate fluorescence monitoring. Additionally, a new calibration curve of the pressure-induced shift of the 7D0-5F0 (0-0) line in the fluorescent spectrum of SrB4O7:Sm2+ for moderate pressures, P≤2 GPa, is given.},
doi = {10.1080/08957959.2018.1519560},
journal = {High Pressure Research},
number = 4,
volume = 38,
place = {United States},
year = {2018},
month = {9}
}
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Journal Article:
Free Publicly Available Full Text
Publisher's Version of Record
https://doi.org/10.1080/08957959.2018.1519560
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Citation Metrics:
Cited by: 8 works
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Figures / Tables:

Figure 1 Figure 1: Schematic view and full assembly of the clamp cell used in the current study. (1) Cryostat sample stick; (2) Optical fiber; (3) Locking nut (Al-alloy); (4,11) Pistons (WC). The left piston has a hole for an optical fiber and (5) a diamond anvil; (6) Anti-extrusion rings (Cu); (7,8)more » Sample container (Teflon); (9) Inner sleeve (CuBe or NiCrAl alloy); (10) Main body (Al-alloy); (12) Support spacers (WC). b) Enlarged view of the piston (4).« less
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    Works referencing / citing this record:

    Effect of fine-tuning pore structures on the dynamics of confined water
    journal, May 2019

    • Kolesnikov, A. I.; Anovitz, L. M.; Hawthorne, F. C.
    • The Journal of Chemical Physics, Vol. 150, Issue 20
    • DOI: 10.1063/1.5096771

    Metal–organic frameworks under pressure
    journal, November 2019

    • Collings, Ines E.; Goodwin, Andrew L.
    • Journal of Applied Physics, Vol. 126, Issue 18
    • DOI: 10.1063/1.5126911
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