Clamp cell with in situ pressure monitoring for low-temperature neutron scattering measurements

Podlesnyak, Andrey A.; Loguillo, Mark; Rucker, Gerald M.; Haberl, Bianca; Boehler, Reinhard; Ehlers, Georg; Daemen, Luke L.; Armitage, Douglas P.; Frontzek, Matthias D.; Lumsden, Mark D.

doi:10.1080/08957959.2018.1519560

Title: Clamp cell with in situ pressure monitoring for low-temperature neutron scattering measurements

Journal Article · 20 September 2018 · High Pressure Research

DOI: https://doi.org/10.1080/08957959.2018.1519560 · OSTI ID:1474603

^[1]; Loguillo, Mark ^[1]; Rucker, Gerald M. ^[1];

^[1]; Boehler, Reinhard ^[1];

^[2]; Daemen, Luke L. ^[1]; Armitage, Douglas P. ^[1];

^[1];

^[1]

Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States). Neutron Scattering Division
Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States). Neutron Technologies Division

In this study, a clamp pressure cell for neutron scattering experiments at low temperatures and in external magnetic fields under pressure up to 2 GPa has been fabricated and tested. The cell provides optical access to the sample space that allows instantaneous pressure determination during sample loading, cooling and measuring using ruby and/or samarium doped strontium tetraborate fluorescence monitoring. Additionally, a new calibration curve of the pressure-induced shift of the ⁷D₀-⁵F₀ (0-0) line in the fluorescent spectrum of SrB₄O₇:Sm²⁺ for moderate pressures, P≤2 GPa, is given.

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Research Organization:: Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)

Sponsoring Organization:: USDOE Office of Science (SC), Basic Energy Sciences (BES)

Grant/Contract Number:: AC05-00OR22725

OSTI ID:: 1474603

Journal Information:: High Pressure Research, Vol. 38, Issue 4; ISSN 0895-7959

Publisher:: Taylor & FrancisCopyright Statement

Country of Publication:: United States

Language:: English

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