Clamp cell with in situ pressure monitoring for low-temperature neutron scattering measurements
Abstract
In this study, a clamp pressure cell for neutron scattering experiments at low temperatures and in external magnetic fields under pressure up to 2 GPa has been fabricated and tested. The cell provides optical access to the sample space that allows instantaneous pressure determination during sample loading, cooling and measuring using ruby and/or samarium doped strontium tetraborate fluorescence monitoring. Additionally, a new calibration curve of the pressure-induced shift of the 7D0-5F0 (0-0) line in the fluorescent spectrum of SrB4O7:Sm2+ for moderate pressures, P≤2 GPa, is given.
- Authors:
-
- Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States). Neutron Scattering Division
- Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States). Neutron Technologies Division
- Publication Date:
- Research Org.:
- Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)
- Sponsoring Org.:
- USDOE Office of Science (SC), Basic Energy Sciences (BES)
- OSTI Identifier:
- 1474603
- Grant/Contract Number:
- AC05-00OR22725
- Resource Type:
- Accepted Manuscript
- Journal Name:
- High Pressure Research
- Additional Journal Information:
- Journal Volume: 38; Journal Issue: 4; Journal ID: ISSN 0895-7959
- Publisher:
- Taylor & Francis
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND TECHNOLOGY; neutron scattering; pressure measurements; clamp cell; fluorescence
Citation Formats
Podlesnyak, Andrey A., Loguillo, Mark, Rucker, Gerald M., Haberl, Bianca, Boehler, Reinhard, Ehlers, Georg, Daemen, Luke L., Armitage, Douglas P., Frontzek, Matthias D., and Lumsden, Mark D.. Clamp cell with in situ pressure monitoring for low-temperature neutron scattering measurements. United States: N. p., 2018.
Web. doi:10.1080/08957959.2018.1519560.
Podlesnyak, Andrey A., Loguillo, Mark, Rucker, Gerald M., Haberl, Bianca, Boehler, Reinhard, Ehlers, Georg, Daemen, Luke L., Armitage, Douglas P., Frontzek, Matthias D., & Lumsden, Mark D.. Clamp cell with in situ pressure monitoring for low-temperature neutron scattering measurements. United States. https://doi.org/10.1080/08957959.2018.1519560
Podlesnyak, Andrey A., Loguillo, Mark, Rucker, Gerald M., Haberl, Bianca, Boehler, Reinhard, Ehlers, Georg, Daemen, Luke L., Armitage, Douglas P., Frontzek, Matthias D., and Lumsden, Mark D.. Thu .
"Clamp cell with in situ pressure monitoring for low-temperature neutron scattering measurements". United States. https://doi.org/10.1080/08957959.2018.1519560. https://www.osti.gov/servlets/purl/1474603.
@article{osti_1474603,
title = {Clamp cell with in situ pressure monitoring for low-temperature neutron scattering measurements},
author = {Podlesnyak, Andrey A. and Loguillo, Mark and Rucker, Gerald M. and Haberl, Bianca and Boehler, Reinhard and Ehlers, Georg and Daemen, Luke L. and Armitage, Douglas P. and Frontzek, Matthias D. and Lumsden, Mark D.},
abstractNote = {In this study, a clamp pressure cell for neutron scattering experiments at low temperatures and in external magnetic fields under pressure up to 2 GPa has been fabricated and tested. The cell provides optical access to the sample space that allows instantaneous pressure determination during sample loading, cooling and measuring using ruby and/or samarium doped strontium tetraborate fluorescence monitoring. Additionally, a new calibration curve of the pressure-induced shift of the 7D0-5F0 (0-0) line in the fluorescent spectrum of SrB4O7:Sm2+ for moderate pressures, P≤2 GPa, is given.},
doi = {10.1080/08957959.2018.1519560},
journal = {High Pressure Research},
number = 4,
volume = 38,
place = {United States},
year = {2018},
month = {9}
}
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Effect of fine-tuning pore structures on the dynamics of confined water
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