Design and performance of an X-ray scanning microscope at the Hard X-ray Nanoprobe beamline of NSLS-II
Abstract
A hard X-ray scanning microscope installed at the Hard X-ray Nanoprobe beamline of the National Synchrotron Light Source II has been designed, constructed and commissioned. The microscope relies on a compact, high stiffness, low heat dissipation approach and utilizes two types of nanofocusing optics. It is capable of imaging with ~15 nm × 15 nm spatial resolution using multilayer Laue lenses and 25 nm × 26 nm resolution using zone plates. Fluorescence, diffraction, absorption, differential phase contrast, ptychography and tomography are available as experimental techniques. The microscope is also equipped with a temperature regulation system which allows the temperature of a sample to be varied in the range between 90 K and 1000 K. The constructed instrument is open for general users and offers its capabilities to the material science, battery research and bioscience communities.
- Authors:
-
- Brookhaven National Lab. (BNL), Upton, NY (United States)
- Brookhaven National Lab. (BNL), Upton, NY (United States); SLAC National Accelerator Lab., Menlo Park, CA (United States)
- Argonne National Lab. (ANL), Argonne, IL (United States). Advanced Photon Source (APS)
- Academia Sinica, Taipei (Taiwan). Inst. of Physics
- Publication Date:
- Research Org.:
- Brookhaven National Lab. (BNL), Upton, NY (United States)
- Sponsoring Org.:
- USDOE Office of Science (SC), Basic Energy Sciences (BES)
- OSTI Identifier:
- 1413930
- Report Number(s):
- BNL-114457-2017-JA
Journal ID: ISSN 1600-5775; JSYRES; TRN: US1800591
- Grant/Contract Number:
- SC0012704
- Resource Type:
- Accepted Manuscript
- Journal Name:
- Journal of Synchrotron Radiation (Online)
- Additional Journal Information:
- Journal Name: Journal of Synchrotron Radiation (Online); Journal Volume: 24; Journal Issue: 6; Journal ID: ISSN 1600-5775
- Publisher:
- International Union of Crystallography
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 47 OTHER INSTRUMENTATION; 36 MATERIALS SCIENCE; X-ray microscopy; multilayer Laue lenses; nanoprobes
Citation Formats
Nazaretski, E., Yan, H., Lauer, K., Bouet, N., Huang, X., Xu, W., Zhou, J., Shu, D., Hwu, Y., and Chu, Y. S. Design and performance of an X-ray scanning microscope at the Hard X-ray Nanoprobe beamline of NSLS-II. United States: N. p., 2017.
Web. doi:10.1107/S1600577517011183.
Nazaretski, E., Yan, H., Lauer, K., Bouet, N., Huang, X., Xu, W., Zhou, J., Shu, D., Hwu, Y., & Chu, Y. S. Design and performance of an X-ray scanning microscope at the Hard X-ray Nanoprobe beamline of NSLS-II. United States. https://doi.org/10.1107/S1600577517011183
Nazaretski, E., Yan, H., Lauer, K., Bouet, N., Huang, X., Xu, W., Zhou, J., Shu, D., Hwu, Y., and Chu, Y. S. Thu .
"Design and performance of an X-ray scanning microscope at the Hard X-ray Nanoprobe beamline of NSLS-II". United States. https://doi.org/10.1107/S1600577517011183. https://www.osti.gov/servlets/purl/1413930.
@article{osti_1413930,
title = {Design and performance of an X-ray scanning microscope at the Hard X-ray Nanoprobe beamline of NSLS-II},
author = {Nazaretski, E. and Yan, H. and Lauer, K. and Bouet, N. and Huang, X. and Xu, W. and Zhou, J. and Shu, D. and Hwu, Y. and Chu, Y. S.},
abstractNote = {A hard X-ray scanning microscope installed at the Hard X-ray Nanoprobe beamline of the National Synchrotron Light Source II has been designed, constructed and commissioned. The microscope relies on a compact, high stiffness, low heat dissipation approach and utilizes two types of nanofocusing optics. It is capable of imaging with ~15 nm × 15 nm spatial resolution using multilayer Laue lenses and 25 nm × 26 nm resolution using zone plates. Fluorescence, diffraction, absorption, differential phase contrast, ptychography and tomography are available as experimental techniques. The microscope is also equipped with a temperature regulation system which allows the temperature of a sample to be varied in the range between 90 K and 1000 K. The constructed instrument is open for general users and offers its capabilities to the material science, battery research and bioscience communities.},
doi = {10.1107/S1600577517011183},
journal = {Journal of Synchrotron Radiation (Online)},
number = 6,
volume = 24,
place = {United States},
year = {2017},
month = {10}
}
Web of Science
Works referencing / citing this record:
X-ray focusing with efficient high-NA multilayer Laue lenses
journal, November 2017
- Bajt, Saša; Prasciolu, Mauro; Fleckenstein, Holger
- Light: Science & Applications, Vol. 7, Issue 3
Nanospectroscopy Captures Nanoscale Compositional Zonation in Barite Solid Solutions
journal, August 2018
- Ling, Florence T.; Hunter, Heather A.; Fitts, Jeffrey P.
- Scientific Reports, Vol. 8, Issue 1
Multimodal X-ray imaging of nanocontainer-treated macrophages and calcium distribution in the perilacunar bone matrix
journal, February 2020
- Stachnik, Karolina; Warmer, Martin; Mohacsi, Istvan
- Scientific Reports, Vol. 10, Issue 1
Effect of CeO 2 nanomaterial surface functional groups on tissue and subcellular distribution of Ce in tomato ( Solanum lycopersicum )
journal, January 2019
- Li, Jieran; Tappero, Ryan V.; Acerbo, Alvin S.
- Environmental Science: Nano, Vol. 6, Issue 1
Bi-continuous pattern formation in thin films via solid-state interfacial dealloying studied by multimodal characterization
journal, January 2019
- Zhao, Chonghang; Kisslinger, Kim; Huang, Xiaojing
- Materials Horizons, Vol. 6, Issue 10
In-situ synchrotron x-ray studies of the microstructure and stability of In 2 O 3 epitaxial films
journal, October 2017
- Highland, M. J.; Hruszkewycz, S. O.; Fong, D. D.
- Applied Physics Letters, Vol. 111, Issue 16
OMNY—A tOMography Nano crYo stage
journal, April 2018
- Holler, M.; Raabe, J.; Diaz, A.
- Review of Scientific Instruments, Vol. 89, Issue 4
Bragg coherent diffractive imaging of strain at the nanoscale
journal, March 2019
- Karpov, Dmitry; Fohtung, Edwin
- Journal of Applied Physics, Vol. 125, Issue 12
Design, characterization, and performance of a hard x-ray transmission microscope at the National Synchrotron Light Source II 18-ID beamline
journal, May 2019
- Coburn, David Scott; Nazaretski, Evgeny; Xu, Weihe
- Review of Scientific Instruments, Vol. 90, Issue 5
Microscopy Instrumentation and Nanopositioning at NSLS-II: Current Status and Future Directions
journal, September 2018
- Nazaretski, E.; Xu, W.; Yan, H.
- Synchrotron Radiation News, Vol. 31, Issue 5
High resolution tip-tilt positioning system for a next generation MLL-based x-ray microscope
journal, November 2017
- Xu, Weihe; Schlossberger, Noah; Xu, Wei
- Measurement Science and Technology, Vol. 28, Issue 12
Multimodal hard x-ray imaging with resolution approaching 10 nm for studies in material science
journal, March 2018
- Yan, Hanfei; Bouet, Nathalie; Zhou, Juan
- Nano Futures, Vol. 2, Issue 1
High-speed raster-scanning synchrotron serial microcrystallography with a high-precision piezo-scanner
journal, August 2018
- Gao, Yuan; Xu, Weihe; Shi, Wuxian
- Journal of Synchrotron Radiation, Vol. 25, Issue 5
Automatic projection image registration for nanoscale X-ray tomographic reconstruction
journal, October 2018
- Yu, Haiyan; Xia, Sihao; Wei, Chenxi
- Journal of Synchrotron Radiation, Vol. 25, Issue 6
Resolving 500 nm axial separation by multi-slice X-ray ptychography
journal, February 2019
- Huang, Xiaojing; Yan, Hanfei; He, Yan
- Acta Crystallographica Section A Foundations and Advances, Vol. 75, Issue 2
Quantitative Nanoscale 3D Imaging of Intergranular Corrosion of 304 Stainless Steel Using Hard X-Ray Nanoprobe
journal, January 2019
- Gill, Simerjeet K.; Ge, Mingyuan; Yan, Hanfei
- Journal of The Electrochemical Society, Vol. 166, Issue 11
Multi-slice ptychography with large numerical aperture multilayer Laue lenses
journal, January 2018
- Öztürk, Hande; Yan, Hanfei; He, Yan
- Optica, Vol. 5, Issue 5
Multimodal X-ray imaging of grain-level properties and performance in a polycrystalline solar cell
text, January 2019
- Ulvestad, A.; Hruszkewycz, S. O.; Holt, M. V.
- Deutsches Elektronen-Synchrotron, DESY, Hamburg
X-ray Assisted Scanning Tunneling Microscopy and Its Applications for Materials Science: The First Results on Cu Doped ZrTe3
journal, November 2019
- Yan, Hui; Shirato, Nozomi; Zhu, Xiangde
- Crystals, Vol. 9, Issue 11
High-speed raster-scanning synchrotron serial microcrystallography with a high-precision piezo-scanner
text, January 2018
- Gao, Yuan; Xu, Weihe; Shi, Wuxian
- International Union of Crystallography (IUCr)
Multimodal X-ray imaging of grain-level properties and performance in a polycrystalline solar cell
journal, May 2019
- Ulvestad, A.; Hruszkewycz, S. O.; Holt, M. V.
- Journal of Synchrotron Radiation, Vol. 26, Issue 4
X-ray focusing with efficient high-NA multilayer Laue lenses
text, January 2017
- Bajt, Saša; Prasciolu, Mauro; Fleckenstein, Holger
- Deutsches Elektronen-Synchrotron, DESY, Hamburg
OMNY - A tOMography Nano crYo stage
text, January 2018
- Holler, Mirko; Raabe, Joerg; Diaz, Ana
- ETH Zurich