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Title: Design and performance of an X-ray scanning microscope at the Hard X-ray Nanoprobe beamline of NSLS-II

Journal Article · · Journal of Synchrotron Radiation (Online)
 [1];  [1];  [2];  [1];  [1];  [1];  [1];  [3];  [4];  [1]
  1. Brookhaven National Lab. (BNL), Upton, NY (United States)
  2. Brookhaven National Lab. (BNL), Upton, NY (United States); SLAC National Accelerator Lab., Menlo Park, CA (United States)
  3. Argonne National Lab. (ANL), Argonne, IL (United States). Advanced Photon Source (APS)
  4. Academia Sinica, Taipei (Taiwan). Inst. of Physics

A hard X-ray scanning microscope installed at the Hard X-ray Nanoprobe beamline of the National Synchrotron Light Source II has been designed, constructed and commissioned. The microscope relies on a compact, high stiffness, low heat dissipation approach and utilizes two types of nanofocusing optics. It is capable of imaging with ~15 nm × 15 nm spatial resolution using multilayer Laue lenses and 25 nm × 26 nm resolution using zone plates. Fluorescence, diffraction, absorption, differential phase contrast, ptychography and tomography are available as experimental techniques. The microscope is also equipped with a temperature regulation system which allows the temperature of a sample to be varied in the range between 90 K and 1000 K. The constructed instrument is open for general users and offers its capabilities to the material science, battery research and bioscience communities.

Research Organization:
Brookhaven National Laboratory (BNL), Upton, NY (United States)
Sponsoring Organization:
USDOE Office of Science (SC), Basic Energy Sciences (BES) (SC-22)
Grant/Contract Number:
SC0012704
OSTI ID:
1413930
Report Number(s):
BNL--114457-2017-JA
Journal Information:
Journal of Synchrotron Radiation (Online), Journal Name: Journal of Synchrotron Radiation (Online) Journal Issue: 6 Vol. 24; ISSN 1600-5775; ISSN JSYRES
Publisher:
International Union of CrystallographyCopyright Statement
Country of Publication:
United States
Language:
English

Cited By (24)

X-ray focusing with efficient high-NA multilayer Laue lenses journal November 2017
Nanospectroscopy Captures Nanoscale Compositional Zonation in Barite Solid Solutions journal August 2018
Multimodal X-ray imaging of nanocontainer-treated macrophages and calcium distribution in the perilacunar bone matrix journal February 2020
Effect of CeO 2 nanomaterial surface functional groups on tissue and subcellular distribution of Ce in tomato ( Solanum lycopersicum ) journal January 2019
Bi-continuous pattern formation in thin films via solid-state interfacial dealloying studied by multimodal characterization journal January 2019
In-situ synchrotron x-ray studies of the microstructure and stability of In 2 O 3 epitaxial films journal October 2017
OMNY—A tOMography Nano crYo stage journal April 2018
Bragg coherent diffractive imaging of strain at the nanoscale journal March 2019
Design, characterization, and performance of a hard x-ray transmission microscope at the National Synchrotron Light Source II 18-ID beamline journal May 2019
Microscopy Instrumentation and Nanopositioning at NSLS-II: Current Status and Future Directions journal September 2018
High resolution tip-tilt positioning system for a next generation MLL-based x-ray microscope journal November 2017
Multimodal hard x-ray imaging with resolution approaching 10 nm for studies in material science journal March 2018
High-speed raster-scanning synchrotron serial microcrystallography with a high-precision piezo-scanner journal August 2018
High-speed raster-scanning synchrotron serial microcrystallography with a high-precision piezo-scanner text January 2018
Automatic projection image registration for nanoscale X-ray tomographic reconstruction journal October 2018
Multimodal X-ray imaging of grain-level properties and performance in a polycrystalline solar cell journal May 2019
Resolving 500 nm axial separation by multi-slice X-ray ptychography journal February 2019
Quantitative Nanoscale 3D Imaging of Intergranular Corrosion of 304 Stainless Steel Using Hard X-Ray Nanoprobe journal January 2019
Multi-slice ptychography with large numerical aperture multilayer Laue lenses journal January 2018
X-ray focusing with efficient high-NA multilayer Laue lenses text January 2017
Multimodal X-ray imaging of grain-level properties and performance in a polycrystalline solar cell text January 2019
X-ray Assisted Scanning Tunneling Microscopy and Its Applications for Materials Science: The First Results on Cu Doped ZrTe3 journal November 2019
OMNY - A tOMography Nano crYo stage text January 2018
Multimodal X-ray imaging of nanocontainer-treated macrophages and calcium distribution in the perilacunar bone matrix text January 2020

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