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Title: Enhancing the resolution of 1 H and 13 C solid-state NMR spectra by reduction of anisotropic bulk magnetic susceptibility broadening

2D HETCOR experiments enhance the resolution of 1H and 13C solid-state NMR spectra by reducing anisotropic bulk magnetic susceptibility (ABMS) signal broadening.
Authors:
 [1] ;  [1] ;  [1] ;  [2] ; ORCiD logo [3] ;  [2] ; ORCiD logo [1]
  1. Iowa State Univ., Ames, IA (United States). Dept. of Chemistry; Ames Lab., Ames, IA (United States)
  2. Univ. of Kentucky, Lexington, KY (United States). College of Pharmacy
  3. Genentech Inc., South San Francisco, CA (United States). Dept. of Small Molecule Pharmaceutical Sciences
Publication Date:
Report Number(s):
IS-J 9484
Journal ID: ISSN 1463-9076; PPCPFQ; TRN: US1703313
Grant/Contract Number:
AC02-07CH11358; 1709972; 1710453
Type:
Accepted Manuscript
Journal Name:
Physical Chemistry Chemical Physics. PCCP (Print)
Additional Journal Information:
Journal Name: Physical Chemistry Chemical Physics. PCCP (Print); Journal Volume: 19; Journal Issue: 41; Journal ID: ISSN 1463-9076
Publisher:
Royal Society of Chemistry
Research Org:
Ames Laboratory (AMES), Ames, IA (United States)
Sponsoring Org:
USDOE; National Science Foundation (NSF)
Country of Publication:
United States
Language:
English
Subject:
37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY
OSTI Identifier:
1408913

Hanrahan, Michael P., Venkatesh, Amrit, Carnahan, Scott L., Calahan, Julie L., Lubach, Joseph W., Munson, Eric J., and Rossini, Aaron J.. Enhancing the resolution of 1 H and 13 C solid-state NMR spectra by reduction of anisotropic bulk magnetic susceptibility broadening. United States: N. p., Web. doi:10.1039/C7CP04223J.
Hanrahan, Michael P., Venkatesh, Amrit, Carnahan, Scott L., Calahan, Julie L., Lubach, Joseph W., Munson, Eric J., & Rossini, Aaron J.. Enhancing the resolution of 1 H and 13 C solid-state NMR spectra by reduction of anisotropic bulk magnetic susceptibility broadening. United States. doi:10.1039/C7CP04223J.
Hanrahan, Michael P., Venkatesh, Amrit, Carnahan, Scott L., Calahan, Julie L., Lubach, Joseph W., Munson, Eric J., and Rossini, Aaron J.. 2017. "Enhancing the resolution of 1 H and 13 C solid-state NMR spectra by reduction of anisotropic bulk magnetic susceptibility broadening". United States. doi:10.1039/C7CP04223J. https://www.osti.gov/servlets/purl/1408913.
@article{osti_1408913,
title = {Enhancing the resolution of 1 H and 13 C solid-state NMR spectra by reduction of anisotropic bulk magnetic susceptibility broadening},
author = {Hanrahan, Michael P. and Venkatesh, Amrit and Carnahan, Scott L. and Calahan, Julie L. and Lubach, Joseph W. and Munson, Eric J. and Rossini, Aaron J.},
abstractNote = {2D HETCOR experiments enhance the resolution of1H and13C solid-state NMR spectra by reducing anisotropic bulk magnetic susceptibility (ABMS) signal broadening.},
doi = {10.1039/C7CP04223J},
journal = {Physical Chemistry Chemical Physics. PCCP (Print)},
number = 41,
volume = 19,
place = {United States},
year = {2017},
month = {9}
}

Works referenced in this record:

Generalized Gradient Approximation Made Simple
journal, October 1996
  • Perdew, John P.; Burke, Kieron; Ernzerhof, Matthias
  • Physical Review Letters, Vol. 77, Issue 18, p. 3865-3868
  • DOI: 10.1103/PhysRevLett.77.3865

Soft self-consistent pseudopotentials in a generalized eigenvalue formalism
journal, April 1990