Fabrication of phosphonic acid films on nitinol nanoparticles by dynamic covalent assembly

Quinones, Rosalynn; Garretson, Samantha; Behnke, Grayce; Fagan, Jonathan W.; Mueller, Karl T.; Agarwal, Sushant; Gupta, Rakesh K.

doi:10.1016/J.TSF.2017.09.048

Title: Fabrication of phosphonic acid films on nitinol nanoparticles by dynamic covalent assembly

Journal Article · Mon Sep 25 00:00:00 EDT 2017 · Thin Solid Films

DOI: https://doi.org/10.1016/J.TSF.2017.09.048 · OSTI ID:1395355

Quinones, Rosalynn ^[1]; Garretson, Samantha ^[1]; Behnke, Grayce ^[1]; Fagan, Jonathan W. ^[2]; Mueller, Karl T. ^[3];

^[4]; Gupta, Rakesh K. ^[4]

Marshall Univ., Huntington, WV (United States)
Pennsylvania State Univ., University Park, PA (United States)
Pennsylvania State Univ., University Park, PA (United States); Pacific Northwest National Lab. (PNNL), Richland, WA (United States)
West Virginia Univ., Morgantown, WV (United States)

Nitinol (NiTi) nanoparticles are a valuable metal alloy due to many unique properties that allow for medical applications. NiTi nanoparticles have the potential to form nanofluids, which can advance the thermal conductivity of fluids by controlling the surface functionalization through chemical attachment of organic acids to the surface to form self-assembled alkylphosphonate films. In this study, phosphonic functional head groups such as 16-phosphonohexadecanoic acid, octadecylphosphonic acid, and 12-aminododecylphosphonic acid were used to form an ordered and strongly chemically bounded film on the NiTi nanopowder. The surface of the NiTi nanoparticles was modified in order to tailor the chemical and physical properties to the desired application. The modified NiTi nanoparticles were characterized using infrared spectroscopy, powder X-ray diffraction, X-ray photoelectron spectroscopy, and ³¹P solid-state nuclear magnetic resonance. The interfacial bonding was identified by spectroscopic data suggesting the phosphonic head group adsorbs in a mixed bidentate/monodentate binding motif on the NiTi nanoparticles. Dynamic light scattering and scanning electron microscopy-energy dispersive X-ray spectroscopy revealed the particle sizes. Differential scanning calorimetry was used to examine the phase transitions. Zeta potential determination as a function of pH was examined to investigate the surface properties of charged nanoparticles. In conclusion, the influence of environmental stability of the surface modifications was also assessed.

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Research Organization:: Pacific Northwest National Laboratory (PNNL), Richland, WA (United States)

Sponsoring Organization:: USDOE

Grant/Contract Number:: AC05-76RL01830

OSTI ID:: 1395355

Journal Information:: Thin Solid Films, Journal Name: Thin Solid Films Vol. 642; ISSN 0040-6090

Publisher:: ElsevierCopyright Statement

Country of Publication:: United States

Language:: English

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36 MATERIALS SCIENCE
Nanoparticles
Nitinol
Phosphonic acid
Self-assembly films
Solid-state nuclear magnetic resonance
Zeta potential

Title: Fabrication of phosphonic acid films on nitinol nanoparticles by dynamic covalent assembly

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