Strong, Ductile, and Thermally Stable bcc-Mg Nanolaminates

Pathak, Siddhartha; Velisavljevic, Nenad; Baldwin, Jon Kevin Scott; Jain, Manish; Zheng, Shijian; Mara, Nathan Allan; Beyerlein, Irene

doi:10.1038/s41598-017-08302-5

Title: Strong, Ductile, and Thermally Stable bcc-Mg Nanolaminates

Journal Article · Tue Aug 15 00:00:00 EDT 2017 · Scientific Reports

DOI: https://doi.org/10.1038/s41598-017-08302-5 · OSTI ID:1392815

Pathak, Siddhartha ^[1];

^[2];

^[2]; Jain, Manish ^[1]; Zheng, Shijian ^[3];

^[4]; Beyerlein, Irene ^[5]

Univ. of Nevada, Reno, NV (United States). Dept. of Chemical and Materials Engineering
Los Alamos National Lab. (LANL), Los Alamos, NM (United States)
Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Chinese Academy of Sciences (CAS), Shenyang (China). Shenyang National Lab. for Materials Science
Los Alamos National Lab. (LANL), Los Alamos, NM (United State
Univ. of California, Santa Barbara, CA (United States). Mechanical Engineering Dept., Materials Dept.

Magnesium has attracted attention worldwide because it is the lightest structural metal. However, a high strength-to-weight ratio remains its only attribute, since an intrinsic lack of strength, ductility and low melting temperature severely restricts practical applications of Mg. Through interface strains, the crystal structure of Mg can be transformed and stabilized from a simple hexagonal (hexagonal close packed hcp) to body center cubic (bcc) crystal structure at ambient pressures. Here, we demonstrate that when introduced into a nanocomposite bcc Mg is far more ductile, 50% stronger, and retains its strength after extended exposure to 200°C, which is 0.5 times its homologous temperature. These findings reveal an alternative solution to obtaining lightweight metals critically needed for future energy efficiency and fuel savings.

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Research Organization:: Los Alamos National Laboratory (LANL)

Sponsoring Organization:: USDOE Office of Science (SC); National Science Foundation (NSF); USDOE National Nuclear Security Administration (NNSA)

Grant/Contract Number:: AC52-06NA25396; NA0001974; AC02-06CH11357; AC02-06CH11357

OSTI ID:: 1392815

Report Number(s):: LA-UR-17-27197

Journal Information:: Scientific Reports, Journal Name: Scientific Reports Journal Issue: 1 Vol. 7; ISSN 2045-2322

Country of Publication:: United States

Language:: English

References (101)

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On the effective lattice parameter of binary alloys Lubarda, V. A. Mechanics of Materials, Vol. 35, Issue 1-2 https://doi.org/10.1016/s0167-6636(02)00196-5	journal	January 2003
Magnesium Mordike, B. L.; Ebert, T. Materials Science and Engineering: A, Vol. 302, Issue 1 https://doi.org/10.1016/s0921-5093(00)01351-4	journal	April 2001
Tensile testing of free-standing Cu, Ag and Al thin films and Ag/Cu multilayers Huang, Haibo; Spaepen, F. Acta Materialia, Vol. 48, Issue 12 https://doi.org/10.1016/s1359-6454(00)00128-2	journal	July 2000
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Strength and ductility with {10͞11} — {10͞12} double twinning in a magnesium alloy Lentz, M.; Risse, M.; Schaefer, N. Nature Communications, Vol. 7, Issue 1 https://doi.org/10.1038/ncomms11068	journal	April 2016
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Atomic-level study of twin nucleation from face-centered-cubic/body-centered-cubic interfaces in nanolamellar composites Han, W. Z.; Carpenter, J. S.; Wang, J. Applied Physics Letters, Vol. 100, Issue 1 https://doi.org/10.1063/1.3675447	journal	January 2012
High-pressure behavior and thermoelastic properties of niobium studied by in situ x-ray diffraction Zou, Yongtao; Qi, Xintong; Wang, Xuebing Journal of Applied Physics, Vol. 116, Issue 1 https://doi.org/10.1063/1.4887436	journal	July 2014
First-principles study of the structure of Mg/Nb multilayers Kumar, Anil; Beyerlein, Irene J.; Wang, Jian Applied Physics Letters, Vol. 105, Issue 7 https://doi.org/10.1063/1.4893700	journal	August 2014
An interface facet driven Rayleigh instability in high-aspect-ratio bimetallic nanolayered composites Zheng, Shijian; Carpenter, John S.; Wang, Jian Applied Physics Letters, Vol. 105, Issue 11 https://doi.org/10.1063/1.4895560	journal	September 2014
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Reducing deformation anisotropy to achieve ultrahigh strength and ductility in Mg at the nanoscale Yu, Q.; Qi, L.; Mishra, R. K. Proceedings of the National Academy of Sciences, Vol. 110, Issue 33 https://doi.org/10.1073/pnas.1306371110	journal	July 2013
Thermal stability of self-supported nanolayered Cu/Nb films Misra, A.; Hoagland, R. G.; Kung ‡, H. Philosophical Magazine, Vol. 84, Issue 10 https://doi.org/10.1080/14786430310001659480	journal	April 2004
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The Tension of Metallic Films Deposited by Electrolysis Stoney, G. G. Proceedings of the Royal Society A: Mathematical, Physical and Engineering Sciences, Vol. 82, Issue 553 https://doi.org/10.1098/rspa.1909.0021	journal	May 1909
NbZr multilayers. I. Structure and superconductivity Lowe, W. P.; Geballe, T. H. Physical Review B, Vol. 29, Issue 9 https://doi.org/10.1103/PhysRevB.29.4961	journal	May 1984
High-pressure structural phase transition in Mg Olijnyk, H.; Holzapfel, W. B. Physical Review B, Vol. 31, Issue 7 https://doi.org/10.1103/PhysRevB.31.4682	journal	April 1985
Equation of state and high-pressure/high-temperature phase diagram of magnesium Stinton, G. W.; MacLeod, S. G.; Cynn, H. Physical Review B, Vol. 90, Issue 13 https://doi.org/10.1103/PhysRevB.90.134105	journal	October 2014
Dimensionally Induced Structural transformations in Titanium-Aluminum Multilayers Banerjee, Rajarshi; Ahuja, Rajiv; Fraser, Hamish L. Physical Review Letters, Vol. 76, Issue 20 https://doi.org/10.1103/PhysRevLett.76.3778	journal	May 1996
NbZr multilayers. I. Structure and superconductivity Lowe, W. P.; Geballe, T. H. Physical Review B, Vol. 29, Issue 9 https://doi.org/10.1103/physrevb.29.4961	journal	May 1984
High-pressure structural phase transition in Mg Olijnyk, H.; Holzapfel, W. B. Physical Review B, Vol. 31, Issue 7 https://doi.org/10.1103/physrevb.31.4682	journal	April 1985
Equation of state and high-pressure/high-temperature phase diagram of magnesium Stinton, G. W.; MacLeod, S. G.; Cynn, H. Physical Review B, Vol. 90, Issue 13 https://doi.org/10.1103/physrevb.90.134105	journal	October 2014
Dimensionally Induced Structural transformations in Titanium-Aluminum Multilayers Banerjee, Rajarshi; Ahuja, Rajiv; Fraser, Hamish L. Physical Review Letters, Vol. 76, Issue 20 https://doi.org/10.1103/physrevlett.76.3778	journal	May 1996
Stress reduction in sputter deposited films using nanostructured compliant layers by high working-gas pressures Karabacak, Tansel; Senkevich, Jay. J.; Wang, Gwo-Ching Journal of Vacuum Science & Technology A: Vacuum, Surfaces, and Films, Vol. 23, Issue 4 https://doi.org/10.1116/1.1861940	journal	July 2005
Weight Loss with Magnesium Alloys Pollock, T. M. Science, Vol. 328, Issue 5981 https://doi.org/10.1126/science.1182848	journal	May 2010
A lightweight shape-memory magnesium alloy Ogawa, Y.; Ando, D.; Sutou, Y. Science, Vol. 353, Issue 6297 https://doi.org/10.1126/science.aaf6524	journal	July 2016
Thermal stability of nanocrystalline Nb produced by severe plastic deformation Popova, E. N.; Popov, V. V.; Romanov, E. P. The Physics of Metals and Metallography, Vol. 101, Issue 1 https://doi.org/10.1134/S0031918X06010078	journal	January 2006
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Thermal stability of nanocrystalline Nb produced by severe plastic deformation Popova, E. N.; Popov, V. V.; Romanov, E. P. The Physics of Metals and Metallography, Vol. 101, Issue 1 https://doi.org/10.1134/s0031918x06010078	journal	January 2006
The size effects in hardness of polycrystalline niobium Golovin, Yu. I.; Isaenkova, M. G.; Krymskaya, O. A. Technical Physics Letters, Vol. 36, Issue 4 https://doi.org/10.1134/s1063785010040231	journal	April 2010
The crystallography and deformation modes of hexagonal close-packed metals Partridge, P. G. International Materials Reviews, Vol. 12, Issue 1 https://doi.org/10.1179/095066067790138184	journal	January 1967
The crystallography and deformation modes of hexagonal close-packed metals Partridge, P. G. International Materials Reviews, Vol. 12, Issue 1 https://doi.org/10.1179/imr.1967.12.1.169	journal	January 1967
The crystallography and deformation modes of hexagonal close-packed metals Partridge, P. G. Metallurgical Reviews, Vol. 12, Issue 1 https://doi.org/10.1179/mtlr.1967.12.1.169	journal	January 1967

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High temperature strength retention of Cu/Nb nanolaminates through dynamic strain ageing Liu, Zhilin; Snel, J.; Boll, T. arXiv https://doi.org/10.48550/arxiv.2008.06241	text	January 2020
Elevated and cryogenic temperature micropillar compression of magnesium–niobium multilayer films Thomas, K.; Mohanty, G.; Wehrs, J. Journal of Materials Science, Vol. 54, Issue 15 https://doi.org/10.1007/s10853-019-03422-x	journal	May 2019
Interface Facilitated Reorientation of Mg Nanolayers in Mg-Nb Nanolaminates Chen, Y.; Gong, M. Y.; Shao, S. JOM, Vol. 71, Issue 4 https://doi.org/10.1007/s11837-019-03360-8	journal	February 2019
Structure and properties of pseudomorphically transformed bcc Mg in Mg/Nb multilayered nanolaminates studied using synchrotron X-ray diffraction Jain, Manish; Velisavljevic, Nenad; Baldwin, J. Kevin Journal of Applied Physics, Vol. 126, Issue 2 https://doi.org/10.1063/1.5097249	journal	July 2019
Direct observation of the hcp-bcc phase transition and melting along the principal Hugoniot of Mg Beason, M. T.; Mandal, A.; Jensen, B. J. Physical Review B, Vol. 101, Issue 2 https://doi.org/10.1103/physrevb.101.024110	journal	January 2020
Room temperature deformation mechanisms of Mg/Nb nanolayered composites Ardeljan, Milan; Knezevic, Marko; Jain, Manish Journal of Materials Research, Vol. 33, Issue 10 https://doi.org/10.1557/jmr.2018.107	journal	May 2018
Cracking and Toughening Mechanisms in Nanoscale Metallic Multilayer Films: A Brief Review Zhou, Qing; Ren, Yue; Du, Yin Applied Sciences, Vol. 8, Issue 10 https://doi.org/10.3390/app8101821	journal	October 2018

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