Anisotropic deformation of extruded magnesium alloy AZ31 under uniaxial compression: A study with simultaneous in situ synchrotron x-ray imaging and diffraction

Lu, L.; Huang, J. W.; Fan, D.; Bie, B. X.; Sun, T.; Fezzaa, K.; Gong, X. L.; Luo, S. N.

doi:10.1016/j.actamat.2016.08.029

Title: Anisotropic deformation of extruded magnesium alloy AZ31 under uniaxial compression: A study with simultaneous in situ synchrotron x-ray imaging and diffraction

Journal Article · Mon Aug 29 00:00:00 EDT 2016 · Acta Materialia

DOI: https://doi.org/10.1016/j.actamat.2016.08.029 · OSTI ID:1366734

Lu, L. ^[1]; Huang, J. W. ^[2]; Fan, D. ^[2]; Bie, B. X. ^[2]; Sun, T. ^[3]; Fezzaa, K. ^[3]; Gong, X. L. ^[4]; Luo, S. N. ^[5]

Univ. of Science and Technology of China, Anhui (People's Republic of China); Southwest Jiaotong Univ., Sichuan (People's Republic of China); The Peac Institute of Multiscale Sciences, Sichuan (People's Republic of China)
The Peac Institute of Multiscale Sciences, Sichuan (People's Republic of China)
Argonne National Lab. (ANL), Argonne, IL (United States)
Univ. of Science and Technology of China, Anhui (People's Republic of China)
Southwest Jiaotong Univ., Sichuan (People's Republic of China); The Peac Institute of Multiscale Sciences, Sichuan (People's Republic of China)

In situ synchrotron x-ray imaging and diffraction are used to investigate anisotropic deformation of an extruded magnesium alloy AZ31 under uniaxial compression along two different directions, with the loading axis (LA) either parallel or perpendicular to the extrusion direction (ED), referred to as LA∥ED and LAED, respectively. Multiscale measurements including stress–strain curves (macroscale), x-ray digital image correlation (mesoscale), and diffraction (microscale) are obtained simultaneously. Electron backscatter diffraction is performed on samples collected at various strains to characterize deformation twins. The rapid increase in strain hardening rate for the LA∥ED loading is attributed to marked {101¯2} extension twinning and subsequent homogenization of deformation, while dislocation motion leads to inhomogeneous deformation and a decrease in strain hardening rate.

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Research Organization:: Argonne National Lab. (ANL), Argonne, IL (United States)

Sponsoring Organization:: USDOE Office of Science (SC), Basic Energy Sciences (BES) (SC-22); National Natural Science Foundation of China (NSFC)

Grant/Contract Number:: AC02-06CH11357

OSTI ID:: 1366734

Journal Information:: Acta Materialia, Journal Name: Acta Materialia Journal Issue: C Vol. 120; ISSN 1359-6454

Publisher:: ElsevierCopyright Statement

Country of Publication:: United States

Language:: English

References (40)

Magnesium alloy applications in automotive structures Easton, Mark; Beer, Aiden; Barnett, Matthew JOM, Vol. 60, Issue 11 https://doi.org/10.1007/s11837-008-0150-8	journal	November 2008
A self consistent approach of the large deformation polycrystal viscoplasticity Molinari, A.; Canova, G. R.; Ahzi, S. Acta Metallurgica, Vol. 35, Issue 12 https://doi.org/10.1016/0001-6160(87)90297-5	journal	December 1987
A self-consistent anisotropic approach for the simulation of plastic deformation and texture development of polycrystals: Application to zirconium alloys Lebensohn, R. A.; Tomé, C. N. Acta Metallurgica et Materialia, Vol. 41, Issue 9 https://doi.org/10.1016/0956-7151(93)90130-K	journal	September 1993
A constitutive model for hcp materials deforming by slip and twinning Staroselsky, A.; Anand, L. International Journal of Plasticity, Vol. 19, Issue 10 https://doi.org/10.1016/S0749-6419(03)00039-1	journal	October 2003
Magnesium Mordike, B. L.; Ebert, T. Materials Science and Engineering: A, Vol. 302, Issue 1 https://doi.org/10.1016/S0921-5093(00)01351-4	journal	April 2001
Microstructure evolution under compressive plastic deformation of magnesium at different temperatures and strain rates Klimanek, P.; Pötzsch, A. Materials Science and Engineering: A, Vol. 324, Issue 1-2 https://doi.org/10.1016/S0921-5093(01)01297-7	journal	February 2002
Strain hardening of titanium: role of deformation twinning Salem, Ayman A.; Kalidindi, Surya R.; Doherty, Roger D. Acta Materialia, Vol. 51, Issue 14 https://doi.org/10.1016/S1359-6454(03)00239-8	journal	August 2003
Influence of grain size on the compressive deformation of wrought Mg–3Al–1Zn Barnett, M. R.; Keshavarz, Z.; Beer, A. G. Acta Materialia, Vol. 52, Issue 17 https://doi.org/10.1016/j.actamat.2004.07.015	journal	October 2004
Strain hardening due to deformation twinning in α-titanium: Constitutive relations and crystal-plasticity modeling Salem, A. A.; Kalidindi, S. R.; Semiatin, S. L. Acta Materialia, Vol. 53, Issue 12 https://doi.org/10.1016/j.actamat.2005.04.014	journal	July 2005
Deformation and texture evolution in AZ31 magnesium alloy during uniaxial loading Yi, S. -B.; Davies, C. H. J.; Brokmeier, H. -G. Acta Materialia, Vol. 54, Issue 2 https://doi.org/10.1016/j.actamat.2005.09.024	journal	January 2006
The texture and anisotropy of magnesium–zinc–rare earth alloy sheets Bohlen, Jan; Nürnberg, Marcus R.; Senn, Jeremy W. Acta Materialia, Vol. 55, Issue 6 https://doi.org/10.1016/j.actamat.2006.11.013	journal	April 2007
Simulation of deformation twins and deformation texture in an AZ31 Mg alloy under uniaxial compression Choi, S.; Shin, E.; Seong, B. Acta Materialia, Vol. 55, Issue 12 https://doi.org/10.1016/j.actamat.2007.03.015	journal	July 2007
Reorientation and stress relaxation due to twinning: Modeling and experimental characterization for Mg Clausen, B.; Tomé, C. N.; Brown, D. W. Acta Materialia, Vol. 56, Issue 11 https://doi.org/10.1016/j.actamat.2008.01.057	journal	June 2008
Deformation twinning in AZ31: Influence on strain hardening and texture evolution Knezevic, Marko; Levinson, Amanda; Harris, Ryan Acta Materialia, Vol. 58, Issue 19 https://doi.org/10.1016/j.actamat.2010.07.041	journal	November 2010
Temperature dependency of slip and twinning in plane strain compressed magnesium single crystals Chapuis, Adrien; Driver, Julian H. Acta Materialia, Vol. 59, Issue 5 https://doi.org/10.1016/j.actamat.2010.11.064	journal	March 2011
Twinning and grain subdivision during dynamic deformation of a Mg AZ31 sheet alloy at room temperature Dudamell, N. V.; Ulacia, I.; Gálvez, F. Acta Materialia, Vol. 59, Issue 18 https://doi.org/10.1016/j.actamat.2011.07.047	journal	October 2011
In situ X-ray diffraction and crystal plasticity modeling of the deformation behavior of extruded Mg–Li–(Al) alloys: An uncommon tension–compression asymmetry Lentz, Martin; Klaus, Manuela; Beyerlein, Irene J. Acta Materialia, Vol. 86 https://doi.org/10.1016/j.actamat.2014.12.003	journal	March 2015
The role of twinning deformation on the hardening response of polycrystalline magnesium from discrete dislocation dynamics simulations Fan, Haidong; Aubry, Sylvie; Arsenlis, Athanasios Acta Materialia, Vol. 92 https://doi.org/10.1016/j.actamat.2015.03.039	journal	June 2015
High-speed synchrotron X-ray phase contrast imaging for analysis of low-Z composite microstructure Yeager, J. D.; Luo, S. N.; Jensen, B. J. Composites Part A: Applied Science and Manufacturing, Vol. 43, Issue 6 https://doi.org/10.1016/j.compositesa.2012.01.013	journal	June 2012
Plastic anisotropy and the role of non-basal slip in magnesium alloy AZ31B Agnew, Sean R.; Duygulu, Özgür International Journal of Plasticity, Vol. 21, Issue 6 https://doi.org/10.1016/j.ijplas.2004.05.018	journal	June 2005
Modeling the effect of twinning and detwinning during strain-path changes of magnesium alloy AZ31 Proust, Gwénaëlle; Tomé, Carlos N.; Jain, Ashutosh International Journal of Plasticity, Vol. 25, Issue 5 https://doi.org/10.1016/j.ijplas.2008.05.005	journal	May 2009
Twinning effects in a rod-textured AM30 Magnesium alloy Ma, Q.; El Kadiri, H.; Oppedal, A. L. International Journal of Plasticity, Vol. 29 https://doi.org/10.1016/j.ijplas.2011.08.001	journal	February 2012
Effect of dislocation transmutation on modeling hardening mechanisms by twinning in magnesium Oppedal, A. L.; El Kadiri, H.; Tomé, C. N. International Journal of Plasticity, Vol. 30-31 https://doi.org/10.1016/j.ijplas.2011.09.002	journal	March 2012
A crystal plasticity theory for latent hardening by glide twinning through dislocation transmutation and twin accommodation effects El Kadiri, H.; Oppedal, A. L. Journal of the Mechanics and Physics of Solids, Vol. 58, Issue 4 https://doi.org/10.1016/j.jmps.2009.12.004	journal	April 2010
Modeling the temperature dependent effect of twinning on the behavior of magnesium alloy AZ31B sheet Jain, A.; Agnew, S. R. Materials Science and Engineering: A, Vol. 462, Issue 1-2 https://doi.org/10.1016/j.msea.2006.03.160	journal	July 2007
Influence of {10-12} extension twinning on the flow behavior of AZ31 Mg alloy Jiang, Lan; Jonas, John J.; Luo, Alan A. Materials Science and Engineering: A, Vol. 445-446 https://doi.org/10.1016/j.msea.2006.09.069	journal	February 2007
Twinning and the ductility of magnesium alloys Barnett, M. R. Materials Science and Engineering: A, Vol. 464, Issue 1-2 https://doi.org/10.1016/j.msea.2007.02.109	journal	August 2007
Effect of crystal orientation on the mechanical properties and strain hardening behavior of magnesium alloy AZ31 during uniaxial compression Wang, Bingshu; Xin, Renlong; Huang, Guangjie Materials Science and Engineering: A, Vol. 534 https://doi.org/10.1016/j.msea.2011.12.013	journal	February 2012
Deformation and spallation of a magnesium alloy under high strain rate loading Wang, M.; Lu, L.; Li, C. Materials Science and Engineering: A, Vol. 661 https://doi.org/10.1016/j.msea.2016.03.009	journal	April 2016
Microstructures and textures of pure magnesium deformed in plane-strain compression Nave, Mark Denis; Barnett, Matthew Robert Scripta Materialia, Vol. 51, Issue 9 https://doi.org/10.1016/j.scriptamat.2004.07.002	journal	November 2004
Effect of composition on the texture and deformation behaviour of wrought Mg alloys Stanford, N.; Barnett, M. Scripta Materialia, Vol. 58, Issue 3 https://doi.org/10.1016/j.scriptamat.2007.09.054	journal	February 2008
Activation mode dependent {10−12} twinning characteristics in a polycrystalline magnesium alloy Park, Sung Hyuk; Hong, Seong-Gu; Lee, Chong Soo Scripta Materialia, Vol. 62, Issue 4 https://doi.org/10.1016/j.scriptamat.2009.10.027	journal	February 2010
Detwinning and strain hardening of an extruded magnesium alloy during compression Sarker, D.; Chen, D. L. Scripta Materialia, Vol. 67, Issue 2 https://doi.org/10.1016/j.scriptamat.2012.04.007	journal	July 2012
Phase retrieval and differential phase-contrast imaging with low-brilliance X-ray sources Pfeiffer, Franz; Weitkamp, Timm; Bunk, Oliver Nature Physics, Vol. 2, Issue 4, p. 258-261 https://doi.org/10.1038/nphys265	journal	March 2006
On the possibilities of x‐ray phase contrast microimaging by coherent high‐energy synchrotron radiation Snigirev, A.; Snigireva, I.; Kohn, V. Review of Scientific Instruments, Vol. 66, Issue 12 https://doi.org/10.1063/1.1146073	journal	December 1995
Gas gun shock experiments with single-pulse x-ray phase contrast imaging and diffraction at the Advanced Photon Source Luo, S. N.; Jensen, B. J.; Hooks, D. E. Review of Scientific Instruments, Vol. 83, Issue 7 https://doi.org/10.1063/1.4733704	journal	July 2012
Note: Dynamic strain field mapping with synchrotron X-ray digital image correlation Lu, L.; Fan, D.; Bie, B. X. Review of Scientific Instruments, Vol. 85, Issue 7 https://doi.org/10.1063/1.4887343	journal	July 2014
Transient x-ray diffraction with simultaneous imaging under high strain-rate loading Fan, D.; Lu, L.; Li, B. Review of Scientific Instruments, Vol. 85, Issue 11 https://doi.org/10.1063/1.4900861	journal	November 2014
The Deformation and Ageing of Mild Steel: III Discussion of Results Hall, E. O. Proceedings of the Physical Society. Section B, Vol. 64, Issue 9 https://doi.org/10.1088/0370-1301/64/9/303	journal	September 1951
HiSPoD : a program for high-speed polychromatic X-ray diffraction experiments and data analysis on polycrystalline samples Sun, Tao; Fezzaa, Kamel Journal of Synchrotron Radiation, Vol. 23, Issue 4 https://doi.org/10.1107/S1600577516005804	journal	June 2016

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Macrodeformation twinning in a textured aluminum alloy via dynamic equal channel angular pressing Qi, D. K.; Tang, M. X.; Lu, L. Journal of Materials Science, Vol. 54, Issue 5 https://doi.org/10.1007/s10853-018-3102-x	journal	November 2018
Understanding the High Strength and Good Ductility in LPSO-Containing Mg Alloy Using Synchrotron X-ray Diffraction Wang, Jie; Wang, Leyun; Zhu, Gaoming Metallurgical and Materials Transactions A, Vol. 49, Issue 11 https://doi.org/10.1007/s11661-018-4881-z	journal	August 2018
Capture Deformation Twinning in Mg during Shock Compression with Ultrafast Synchrotron X-Ray Diffraction Chen, S.; Li, Y. X.; Zhang, N. B. Physical Review Letters, Vol. 123, Issue 25 https://doi.org/10.1103/physrevlett.123.255501	journal	December 2019
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