Isosymmetric pressure-induced bonding increase changes compression behavior of clinopyroxenes across jadeite-aegirine solid solution in subduction zones
Abstract
Pyroxenes are among the most important minerals of Earth's crust and upper mantle and play significant role in controlling subduction at convergent margins. In this study, synchrotron-based single-crystal X-ray diffraction experiments were carried out on a natural aegirine [NaFe3+Si2O6] sample at ambient temperature and high pressures to 60 GPa, simulating conditions within the coldest part of a subduction zone consisting of old lithosphere. The diffraction data reveal no obvious sign of structural phase transition in aegirine within this pressure range; however, several relevant structural parameter trends change noticeably at approximately 24 GPa, indicating the presence of the previously predicted isosymmetric bonding change, related to increase of coordination number of Na+ at M2 site. The pressure-volume data, fit with third-order Birch-Murnaghan (BM3) equation of state over the whole pressure range, yields KT0 = 126(2) GPa and K'T0 = 3.3(1), while separate BM3 fits performed for the 0–24.0 GPa and 29.9–60.4 GPa pressure ranges give KT0 = 118(3) GPa, K'T0 = 4.2(3) and KT0 = 133(2) GPa, K'T0 = 3.0(1), suggesting that the structure stiffens as a result of the new bond formation. Aegirine exhibits strong anisotropic compression with unit strain axial ratios ε1:ε2:ε3 = 1.00:2.44:1.64. Structural refinements reveal that NaO8 polyhedronmore »
- Authors:
-
[2];
[2];
[2]
- Chinese Academy of Sciences, Guiyang (China); Univ. of Hawai'i at Mānoa, Honolulu HI (United States); Univ. of Chinese Academy of Sciences, Beijing (China)
- Univ. of Hawai'i at Mānoa, Honolulu HI (United States)
- Chinese Academy of Sciences, Guiyang (China)
- Univ. of Arizona, Tucson, AZ (United States)
- Publication Date:
- Research Org.:
- Argonne National Lab. (ANL), Argonne, IL (United States). Advanced Photon Source (APS)
- Sponsoring Org.:
- USDOE Office of Science (SC), Basic Energy Sciences (BES); National Science Foundation (NSF)
- OSTI Identifier:
- 1355027
- Grant/Contract Number:
- FG02-94ER14466; AC02-06CH11357
- Resource Type:
- Accepted Manuscript
- Journal Name:
- Journal of Geophysical Research. Solid Earth
- Additional Journal Information:
- Journal Volume: 122; Journal Issue: 1; Journal ID: ISSN 2169-9313
- Publisher:
- American Geophysical Union
- Country of Publication:
- United States
- Language:
- ENGLISH
- Subject:
- 58 GEOSCIENCES; pyroxenes; high pressure; synchrotron single‐crystal X‐ray diffraction; bonding transition; mantle; subduction zone
Citation Formats
Xu, Jingui, Zhang, Dongzhou, Fan, Dawei, Downs, Robert T., Hu, Yi, and Dera, Przemyslaw K. Isosymmetric pressure-induced bonding increase changes compression behavior of clinopyroxenes across jadeite-aegirine solid solution in subduction zones. United States: N. p., 2016.
Web. doi:10.1002/2016JB013502.
Xu, Jingui, Zhang, Dongzhou, Fan, Dawei, Downs, Robert T., Hu, Yi, & Dera, Przemyslaw K. Isosymmetric pressure-induced bonding increase changes compression behavior of clinopyroxenes across jadeite-aegirine solid solution in subduction zones. United States. https://doi.org/10.1002/2016JB013502
Xu, Jingui, Zhang, Dongzhou, Fan, Dawei, Downs, Robert T., Hu, Yi, and Dera, Przemyslaw K. Wed .
"Isosymmetric pressure-induced bonding increase changes compression behavior of clinopyroxenes across jadeite-aegirine solid solution in subduction zones". United States. https://doi.org/10.1002/2016JB013502. https://www.osti.gov/servlets/purl/1355027.
@article{osti_1355027,
title = {Isosymmetric pressure-induced bonding increase changes compression behavior of clinopyroxenes across jadeite-aegirine solid solution in subduction zones},
author = {Xu, Jingui and Zhang, Dongzhou and Fan, Dawei and Downs, Robert T. and Hu, Yi and Dera, Przemyslaw K.},
abstractNote = {Pyroxenes are among the most important minerals of Earth's crust and upper mantle and play significant role in controlling subduction at convergent margins. In this study, synchrotron-based single-crystal X-ray diffraction experiments were carried out on a natural aegirine [NaFe3+Si2O6] sample at ambient temperature and high pressures to 60 GPa, simulating conditions within the coldest part of a subduction zone consisting of old lithosphere. The diffraction data reveal no obvious sign of structural phase transition in aegirine within this pressure range; however, several relevant structural parameter trends change noticeably at approximately 24 GPa, indicating the presence of the previously predicted isosymmetric bonding change, related to increase of coordination number of Na+ at M2 site. The pressure-volume data, fit with third-order Birch-Murnaghan (BM3) equation of state over the whole pressure range, yields KT0 = 126(2) GPa and K'T0 = 3.3(1), while separate BM3 fits performed for the 0–24.0 GPa and 29.9–60.4 GPa pressure ranges give KT0 = 118(3) GPa, K'T0 = 4.2(3) and KT0 = 133(2) GPa, K'T0 = 3.0(1), suggesting that the structure stiffens as a result of the new bond formation. Aegirine exhibits strong anisotropic compression with unit strain axial ratios ε1:ε2:ε3 = 1.00:2.44:1.64. Structural refinements reveal that NaO8 polyhedron is the most compressible and SiO4 tetrahedron has the lowest compressibility. Lastly, the consequence of bonding transition is that the compressional behavior of aegirine below ~24 GPa and above that pressure is quite different, with likely consequences for relevant thermodynamic parameters and ion diffusion coefficients.},
doi = {10.1002/2016JB013502},
journal = {Journal of Geophysical Research. Solid Earth},
number = 1,
volume = 122,
place = {United States},
year = {Wed Nov 23 00:00:00 EST 2016},
month = {Wed Nov 23 00:00:00 EST 2016}
}
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