Suppression of superconductivity and structural phase transitions under pressure in tetragonal FeS

Lai, Xiaofang; Liu, Ying; Lu, Xujie; Zhang, Sijia; Bu, Kejun; Jin, Changqing; Zhang, Hui; Lin, Jianhua; Huang, Fuqiang

doi:10.1038/srep31077

Title: Suppression of superconductivity and structural phase transitions under pressure in tetragonal FeS

Journal Article · Mon Aug 08 00:00:00 EDT 2016 · Scientific Reports

DOI: https://doi.org/10.1038/srep31077 · OSTI ID:1338807

Lai, Xiaofang ^[1]; Liu, Ying ^[2]; Lu, Xujie ^[3]; Zhang, Sijia ^[2]; Bu, Kejun ^[4]; Jin, Changqing ^[5]; Zhang, Hui ^[4]; Lin, Jianhua ^[1]; Huang, Fuqiang ^[6]

Peking Univ., Beijing (China)
Chinese Academy of Sciences (CAS), Beijing (China)
Los Alamos National Lab. (LANL), Los Alamos, NM (United States)
Chinese Academy of Sciences (CAS), Shanghai (China)
Chinese Academy of Sciences (CAS), Beijing (China); Collaborative Innovation Center of Quantum Matter, Beijing (China)
Peking Univ., Beijing (China); Chinese Academy of Sciences (CAS), Shanghai (China)

Pressure is a powerful tool to study iron-based superconductors. Here, we report systematic high-pressure transport and structural characterizations of the newly discovered superconductor FeS. It is found that superconductor FeS (tetragonal) partly transforms to a hexagonal structure at 0.4 GPa, and then completely transforms to an orthorhombic phase at 7.4 GPa and finally to a monoclinic phase above 9.0 GPa. The superconducting transition temperature of tetragonal FeS was gradually depressed by pressure, different from the case in tetragonal FeSe. With pressure increasing, the S-Fe-S angles only slightly change but the anion height deviates farther from 1.38 Å. This change of anion height, together with the structural instability under pressure, should be closely related to the suppression of superconductivity. We also observed an anomalous metal-semiconductor transition at 6.0 GPa and an unusual increased resistance with further compression above 9.6 GPa. The former can be ascribed to the tetragonal-orthorhombic structural phase transition, and the latter to the electronic structure changes of the high-pressure monoclinic phase. Lastly, a phase diagram of tetragonal FeS as functions of pressure and temperature was mapped out for the first time, which will shed new light on understanding of the structure and physics of the superconducting FeS.

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Research Organization:: Los Alamos National Lab. (LANL), Los Alamos, NM (United States)

Sponsoring Organization:: LDRD; USDOE

Grant/Contract Number:: AC52-06NA25396

OSTI ID:: 1338807

Report Number(s):: LA-UR--16-22905

Journal Information:: Scientific Reports, Journal Name: Scientific Reports Vol. 6; ISSN 2045-2322

Publisher:: Nature Publishing GroupCopyright Statement

Country of Publication:: United States

Language:: English

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High Pressure Studies on Fe-Pnictide Superconductors Chu, C. W.; Lorenz, B. arXiv https://doi.org/10.48550/arxiv.0902.0809	text	January 2009
Why Does Undoped FeSe Become A High Tc Superconductor Under Pressure? Imai, T.; Ahilan, K.; Ning, F. L. arXiv https://doi.org/10.48550/arxiv.0902.3832	text	January 2009
Anion height dependence of Tc for the Fe-based superconductor Mizuguhci, Y.; Hara, Y.; Deguchi, K. arXiv https://doi.org/10.48550/arxiv.1001.1801	text	January 2010
Pressure-induced high-Tc superconducting phase in FeSe: correlation between anion height and Tc Okabe, H.; Takeshita, N.; Horigane, K. arXiv https://doi.org/10.48550/arxiv.1002.1832	text	January 2010
Superconductivity in Iron Compounds Stewart, G. R. arXiv https://doi.org/10.48550/arxiv.1106.1618	text	January 2011
Superconductivity in Topological Insulator Sb2Te3 Induced by Pressure Zhu, J.; Zhang, J. L.; Kong, P. P. arXiv https://doi.org/10.48550/arxiv.1306.6484	text	January 2013
Structural transition and superconductivity in hydrothermally synthesized FeX (X = S, Se) Pachmayr, Ursula; Fehn, Natalie; Johrendt, Dirk arXiv https://doi.org/10.48550/arxiv.1509.04851	text	January 2015
Pressure induced high-spin to low-spin transition in FeS evidenced by x-ray emission spectroscopy Rueff, Jean-Pascal; Kao, Chi-Chang; Struzhkin, Viktor V. arXiv https://doi.org/10.48550/arxiv.cond-mat/9806245	text	January 1998

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Synthesis, structure and superconductivity of FeS _1−x Se _x (0 ≤ x ≤ 1) solid solution crystals Guo, Zhongnan; Sun, Fan; Chen, Yuyuan CrystEngComm, Vol. 21, Issue 19 https://doi.org/10.1039/c9ce00038k	journal	January 2019
Pressure-induced superconductivity in palladium sulfide Chen, Liu-Cheng; Yu, Hao; Pang, Hong-Jie Journal of Physics: Condensed Matter, Vol. 30, Issue 15 https://doi.org/10.1088/1361-648x/aab570	journal	March 2018

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