Pressure-induced phase transformation, reversible amorphization, and anomalous visible light response in organolead bromide perovskite

Wang, Yonggang; Lu, Xujie; Yang, Wenge; Wen, Ting; Yang, Liuxiang; Ren, Xiangting; Wang, Lin; Lin, Zheshuai; Zhao, Yusheng

doi:10.1021/jacs.5b06346

Title: Pressure-induced phase transformation, reversible amorphization, and anomalous visible light response in organolead bromide perovskite

Journal Article · Tue Aug 18 00:00:00 EDT 2015 · Journal of the American Chemical Society

DOI: https://doi.org/10.1021/jacs.5b06346 · OSTI ID:1332921

Wang, Yonggang ^[1]; Lu, Xujie ^[2]; Yang, Wenge ^[3]; Wen, Ting ^[4]; Yang, Liuxiang ^[5]; Ren, Xiangting ^[6]; Wang, Lin ^[3]; Lin, Zheshuai ^[7]; Zhao, Yusheng ^[2]

Univ. of Nevada, Las Vegas, NV (United States); Carnegie Inst. of Washington, Argonne, IL (United States); Huanghe Science and Technology College, Henan (China); UNLV
Univ. of Nevada, Las Vegas, NV (United States)
Carnegie Inst. of Washington, Argonne, IL (United States); Center for High Pressure Science and Technology Advanced Research (HPSTAR), Shanghai (China)
Huanghe Science and Technology College, Henan (China)
Carnegie Inst. of Washington, Argonne, IL (United States)
Center for High Pressure Science and Technology Advanced Research (HPSTAR), Shanghai (China)
Chinese Academy of Sciences (CAS), Beijing (China)

Hydrostatic pressure, as an alternative of chemical pressure to tune the crystal structure and physical properties, is a significant technique for novel function material design and fundamental research. In this article, we report the phase stability and visible light response of the organolead bromide perovskite, CH₃NH₃PbBr₃ (MAPbBr₃), under hydrostatic pressure up to 34 GPa at room temperature: Two phase transformations below 2 GPa (from Pm3¯m to Im3¯, then to Pnma) and a reversible amorphization starting from about 2 GPa were observed, which could be attributed to the tilting of PbBr₆ octahedra and destroying of long-range ordering of MA cations, respectively. The visible light response of MAPbBr₃ to pressure was studied by in situ photoluminescence, electric resistance, photocurrent measurements and first-principle simulations. The anomalous band gap evolution during compression with red-shift followed by blue-shift is explained by the competition between compression effect and pressure-induced amorphization. Along with the amorphization process accomplished around 25 GPa, the resistance increased by 5 orders of magnitude while the system still maintains its semiconductor characteristics and considerable response to the visible light irradiation. Lastly, our results not only show that hydrostatic pressure may provide an applicable tool for the organohalide perovskites based photovoltaic device functioning as switcher or controller, but also shed light on the exploration of more amorphous organometal composites as potential light absorber.

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Research Organization:: Univ. of Nevada, Las Vegas, NV (United States)

Sponsoring Organization:: USDOE Office of Science (SC), Basic Energy Sciences (BES) (SC-22)

Grant/Contract Number:: NA0001982

OSTI ID:: 1332921

Journal Information:: Journal of the American Chemical Society, Journal Name: Journal of the American Chemical Society Journal Issue: 34 Vol. 137; ISSN 0002-7863

Publisher:: American Chemical Society (ACS)Copyright Statement

Country of Publication:: United States

Language:: English

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Emission enhancement and bandgap retention of a two-dimensional mixed cation lead halide perovskite under high pressure Chen, Yaping; Fu, Ruijing; Wang, Lingrui Journal of Materials Chemistry A, Vol. 7, Issue 11 https://doi.org/10.1039/c8ta11992a	journal	January 2019
New cationic Ir( iii ) complexes without “any soft substituents”: aggregation-induced emission and piezochromic luminescence Wang, Yue; Yang, Tianzhi; Liu, Xingman Journal of Materials Chemistry C, Vol. 6, Issue 45 https://doi.org/10.1039/c8tc04512g	journal	January 2018
Hydrogen-bond enhancement triggered structural evolution and band gap engineering of hybrid perovskite (C ₆ H ₅ CH ₂ NH ₃ ) ₂ PbI ₄ under high pressure Tian, Can; Liang, Yongfu; Chen, Wuhao Physical Chemistry Chemical Physics, Vol. 22, Issue 4 https://doi.org/10.1039/c9cp05904k	journal	January 2020
Pressure-induced structural transition and band gap evolution of double perovskite Cs ₂ AgBiBr ₆ nanocrystals Fu, Ruijing; Chen, Yaping; Yong, Xue Nanoscale, Vol. 11, Issue 36 https://doi.org/10.1039/c9nr07030c	journal	January 2019
Bandgap engineering in two-dimensional halide perovskite Cs ₃ Sb ₂ I ₉ nanocrystals under pressure Geng, Ting; Ma, Zhiwei; Chen, Yaping Nanoscale, Vol. 12, Issue 3 https://doi.org/10.1039/c9nr09533k	journal	January 2020
Drastic photoluminescence modulation of an organic molecular crystal with high pressure Guan, Junjie; Zhang, Chunfang; Gao, Dexiang Materials Chemistry Frontiers, Vol. 3, Issue 8 https://doi.org/10.1039/c9qm00082h	journal	January 2019
Electronic structures and elastic properties of a family of metal-free perovskites Li, Kai; Dong, Li-Yuan; Xu, Hao-Xiang Materials Chemistry Frontiers, Vol. 3, Issue 8 https://doi.org/10.1039/c9qm00133f	journal	January 2019
Advances in the application of high pressure in carbon dots Geng, Ting; Liu, Cui; Xiao, Guanjun Materials Chemistry Frontiers, Vol. 3, Issue 12 https://doi.org/10.1039/c9qm00543a	journal	January 2019
Metal halide perovskites under compression Li, Qian; Zhang, Liming; Chen, Zhongwei Journal of Materials Chemistry A, Vol. 7, Issue 27 https://doi.org/10.1039/c9ta04930d	journal	January 2019
Strategic modification of ligands for remarkable piezochromic luminescence (PCL) based on a neutral Ir( iii ) phosphor Li, Dan; Li, Guangfu; Xie, Jiaxin Journal of Materials Chemistry C, Vol. 7, Issue 35 https://doi.org/10.1039/c9tc03646f	journal	January 2019
Pressure-induced structural evolution, optical and electronic transitions of nontoxic organometal halide perovskite-based methylammonium tin chloride Wang, Lingrui; Ou, Tianji; Wang, Kai Applied Physics Letters, Vol. 111, Issue 23 https://doi.org/10.1063/1.5004186	journal	December 2017
Pressure dependence of excited-state charge-carrier dynamics in organolead tribromide perovskites Liu, X. C.; Han, J. H.; Zhao, H. F. Applied Physics Letters, Vol. 112, Issue 19 https://doi.org/10.1063/1.5030588	journal	May 2018
Characterization of colloidal nanocrystal surface structure using small angle neutron scattering and efficient Bayesian parameter estimation Winslow, Samuel W.; Shcherbakov-Wu, Wenbi; Liu, Yun The Journal of Chemical Physics, Vol. 150, Issue 24 https://doi.org/10.1063/1.5108904	journal	June 2019
Pressure responses of halide perovskites with various compositions, dimensionalities, and morphologies Li, Mei; Liu, Tianbiao; Wang, Yonggang Matter and Radiation at Extremes, Vol. 5, Issue 1 https://doi.org/10.1063/1.5133653	journal	January 2020
Simultaneous band-gap narrowing and carrier-lifetime prolongation of organic–inorganic trihalide perovskites Kong, Lingping; Liu, Gang; Gong, Jue Proceedings of the National Academy of Sciences, Vol. 113, Issue 32 https://doi.org/10.1073/pnas.1609030113	journal	July 2016
Pressure-induced semiconductor-to-metal phase transition of a charge-ordered indium halide perovskite Lin, Jia; Chen, Hong; Gao, Yang Proceedings of the National Academy of Sciences, Vol. 116, Issue 47 https://doi.org/10.1073/pnas.1907576116	journal	November 2019
Pressure-induced phase transformation of CsPbI ₃ by X-ray diffraction and Raman spectroscopy Yuan, Guan; Qin, Shan; Wu, Xiang Phase Transitions, Vol. 91, Issue 1 https://doi.org/10.1080/01411594.2017.1357180	journal	June 2017
Pressure induced transformation and subsequent amorphization of monoclinic Nb ₂ O ₅ and its effect on optical properties Guan, Zhou; Li, Quanjun; Zhang, Huafang Journal of Physics: Condensed Matter, Vol. 31, Issue 10 https://doi.org/10.1088/1361-648x/aaf9bd	journal	January 2019
Pressure-induced emission of cesium lead halide perovskite nanocrystals. Ma, Zhiwei; Liu, Zhun; Lu, Siyu Apollo - University of Cambridge Repository https://doi.org/10.17863/cam.33885	text	January 2018
Simultaneous band gap narrowing and carrier lifetime prolongation of organic-inorganic trihalide perovskites Kong, Lingping; Liu, Gang; Gong, Jue arXiv https://doi.org/10.48550/arxiv.1607.01607	text	January 2016

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