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The Enhanced Electrochemical Performance of Nanocrystalline Li[Li₀.₂₆Ni₀.₁₁Mn₀.₆₃]O₂ Synthesized by the Molten-Salt Method for Li-ion batteries

Abstract

Nanocrystalline Li[Li₀.₂₆Ni₀.₁₁Mn₀.₆₃]O₂ were easily prepared by using Ni₀.₁₅Mn₀.₅(OH)₂ and Li₂CO₃ as precursors and KCl as melt-salt for the high capacity materials of Li-ion storage. The obtained nanoparticles showed same morphology of polygonal shape and the particle size distribution increased with increasing sinter temperature. The Li[Li₀.₂₆Ni₀.₁₁Mn₀.₆₃]O₂ electrode sintered at 800 °C for 12 h exhibits a reversible capacity of more than 300 mAh g⁻¹ at 0.1 C rate between 2 V and 4.8 V and the capacity retention remains 86% and 90% after 90 cycles at the rate of 0.5 C and 1 C, respectively. These superior electrochemical performances are discussed in detail and ascribed to the low dimension and well-crystallized particles. The low dimension provides a short diffusion path and fast transport channels for the lithium ion insertion/extraction reactions and the well-crystallized structure restrains the elimination of oxide ion vacancies and metal ions rearrangement during charge–discharge cycling.
Publication Date:
Jan 01, 2014
Product Type:
Journal Article
Resource Relation:
Journal Name: Electrochimica Acta; Journal Volume: 117; Other Information: Copyright (c) 2013 Elsevier Science B.V., Amsterdam, The Netherlands, All rights reserved.; Country of input: International Atomic Energy Agency (IAEA)
Subject:
37 INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY; 77 NANOSCIENCE AND NANOTECHNOLOGY; CRYSTALS; DISTRIBUTION; ELECTRODES; EXTRACTION; LITHIUM; LITHIUM IONS; MOLTEN SALTS; NANOPARTICLES; NANOSTRUCTURES; OXIDES; PARTICLE SIZE; SYNTHESIS
OSTI ID:
22321859
Country of Origin:
United Kingdom
Language:
English
Other Identifying Numbers:
Journal ID: ISSN 0013-4686; CODEN: ELCAAV; Other: PII: S0013-4686(13)02357-8; TRN: GB15R1009028068
Availability:
Available from http://dx.doi.org/10.1016/j.electacta.2013.11.124
Submitting Site:
INIS
Size:
page(s) 285-291
Announcement Date:
Apr 03, 2015

Citation Formats

ZhenYao, Wang, Biao, Li, Jin, Ma, and DingGuo, Xia. The Enhanced Electrochemical Performance of Nanocrystalline Li[Li₀.₂₆Ni₀.₁₁Mn₀.₆₃]O₂ Synthesized by the Molten-Salt Method for Li-ion batteries. United Kingdom: N. p., 2014. Web. doi:10.1016/J.ELECTACTA.2013.11.124.
ZhenYao, Wang, Biao, Li, Jin, Ma, & DingGuo, Xia. The Enhanced Electrochemical Performance of Nanocrystalline Li[Li₀.₂₆Ni₀.₁₁Mn₀.₆₃]O₂ Synthesized by the Molten-Salt Method for Li-ion batteries. United Kingdom. https://doi.org/10.1016/J.ELECTACTA.2013.11.124
ZhenYao, Wang, Biao, Li, Jin, Ma, and DingGuo, Xia. 2014. "The Enhanced Electrochemical Performance of Nanocrystalline Li[Li₀.₂₆Ni₀.₁₁Mn₀.₆₃]O₂ Synthesized by the Molten-Salt Method for Li-ion batteries." United Kingdom. https://doi.org/10.1016/J.ELECTACTA.2013.11.124.
@misc{etde_22321859,
title = {The Enhanced Electrochemical Performance of Nanocrystalline Li[Li₀.₂₆Ni₀.₁₁Mn₀.₆₃]O₂ Synthesized by the Molten-Salt Method for Li-ion batteries}
author = {ZhenYao, Wang, Biao, Li, Jin, Ma, and DingGuo, Xia}
abstractNote = {Nanocrystalline Li[Li₀.₂₆Ni₀.₁₁Mn₀.₆₃]O₂ were easily prepared by using Ni₀.₁₅Mn₀.₅(OH)₂ and Li₂CO₃ as precursors and KCl as melt-salt for the high capacity materials of Li-ion storage. The obtained nanoparticles showed same morphology of polygonal shape and the particle size distribution increased with increasing sinter temperature. The Li[Li₀.₂₆Ni₀.₁₁Mn₀.₆₃]O₂ electrode sintered at 800 °C for 12 h exhibits a reversible capacity of more than 300 mAh g⁻¹ at 0.1 C rate between 2 V and 4.8 V and the capacity retention remains 86% and 90% after 90 cycles at the rate of 0.5 C and 1 C, respectively. These superior electrochemical performances are discussed in detail and ascribed to the low dimension and well-crystallized particles. The low dimension provides a short diffusion path and fast transport channels for the lithium ion insertion/extraction reactions and the well-crystallized structure restrains the elimination of oxide ion vacancies and metal ions rearrangement during charge–discharge cycling.}
doi = {10.1016/J.ELECTACTA.2013.11.124}
journal = []
volume = {117}
journal type = {AC}
place = {United Kingdom}
year = {2014}
month = {Jan}
}