Method of sintering ceramic materials
Abstract
A method for sintering ceramic materials is described. A ceramic article is coated with layers of protective coatings such as boron nitride, graphite foil, and niobium. The coated ceramic article is embedded in a container containing refractory metal oxide granules and placed within a microwave oven. The ceramic article is heated by microwave energy to a temperature sufficient to sinter the ceramic article to form a densified ceramic article having a density equal to or greater than 90% of theoretical density.
- Inventors:
-
- Knoxville, TN
- Oak Ridge, TN
- Issue Date:
- Research Org.:
- Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)
- OSTI Identifier:
- 868541
- Patent Number(s):
- 5164130
- Assignee:
- Martin Marietta Energy Systems, Inc. (Oak Ridge, TN)
- Patent Classifications (CPCs):
-
C - CHEMISTRY C04 - CEMENTS C04B - LIME, MAGNESIA
- DOE Contract Number:
- AC05-84OR21400
- Resource Type:
- Patent
- Country of Publication:
- United States
- Language:
- English
- Subject:
- method; sintering; ceramic; materials; described; article; coated; layers; protective; coatings; boron; nitride; graphite; foil; niobium; embedded; container; containing; refractory; metal; oxide; granules; placed; microwave; oven; heated; energy; temperature; sufficient; sinter; form; densified; density; equal; 90; theoretical; protective coatings; theoretical density; protective coating; ceramic article; microwave oven; ceramic material; refractory metal; microwave energy; boron nitride; metal oxide; ceramic materials; temperature sufficient; container containing; wave energy; coated ceramic; sintering ceramic; densified ceramic; ceramic mater; /264/
Citation Formats
Holcombe, Cressie E, and Dykes, Norman L. Method of sintering ceramic materials. United States: N. p., 1992.
Web.
Holcombe, Cressie E, & Dykes, Norman L. Method of sintering ceramic materials. United States.
Holcombe, Cressie E, and Dykes, Norman L. Wed .
"Method of sintering ceramic materials". United States. https://www.osti.gov/servlets/purl/868541.
@article{osti_868541,
title = {Method of sintering ceramic materials},
author = {Holcombe, Cressie E and Dykes, Norman L},
abstractNote = {A method for sintering ceramic materials is described. A ceramic article is coated with layers of protective coatings such as boron nitride, graphite foil, and niobium. The coated ceramic article is embedded in a container containing refractory metal oxide granules and placed within a microwave oven. The ceramic article is heated by microwave energy to a temperature sufficient to sinter the ceramic article to form a densified ceramic article having a density equal to or greater than 90% of theoretical density.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {Wed Jan 01 00:00:00 EST 1992},
month = {Wed Jan 01 00:00:00 EST 1992}
}
Works referenced in this record:
Tensile and compressive properties of flexible graphite foils
journal, January 1986
- Dowell, M. B.; Howard, R. A.
- Carbon, Vol. 24, Issue 3
Unusual properties of microwave-sintered yttria-2wt% zirconia
journal, August 1988
- Holcombe, C. E.; Meek, T. T.; Dykes, N. L.
- Journal of Materials Science Letters, Vol. 7, Issue 8
Enhanced Thermal Shock Properties of Y 2 O 3 -2 WT.% ZrO 2 Heated Using 2.45 Ghz Radiation
journal, January 1988
- Holcombe, C. E.; Meek, T. T.; Dykes, N. L.
- MRS Proceedings, Vol. 124