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Title: Method of sintering ceramic materials

Abstract

A method for sintering ceramic materials is described. A ceramic article is coated with layers of protective coatings such as boron nitride, graphite foil, and niobium. The coated ceramic article is embedded in a container containing refractory metal oxide granules and placed within a microwave oven. The ceramic article is heated by microwave energy to a temperature sufficient to sinter the ceramic article to form a densified ceramic article having a density equal to or greater than 90% of theoretical density.

Inventors:
 [1];  [2]
  1. Knoxville, TN
  2. Oak Ridge, TN
Issue Date:
Research Org.:
Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)
OSTI Identifier:
868541
Patent Number(s):
5164130
Assignee:
Martin Marietta Energy Systems, Inc. (Oak Ridge, TN)
Patent Classifications (CPCs):
C - CHEMISTRY C04 - CEMENTS C04B - LIME, MAGNESIA
DOE Contract Number:  
AC05-84OR21400
Resource Type:
Patent
Country of Publication:
United States
Language:
English
Subject:
method; sintering; ceramic; materials; described; article; coated; layers; protective; coatings; boron; nitride; graphite; foil; niobium; embedded; container; containing; refractory; metal; oxide; granules; placed; microwave; oven; heated; energy; temperature; sufficient; sinter; form; densified; density; equal; 90; theoretical; protective coatings; theoretical density; protective coating; ceramic article; microwave oven; ceramic material; refractory metal; microwave energy; boron nitride; metal oxide; ceramic materials; temperature sufficient; container containing; wave energy; coated ceramic; sintering ceramic; densified ceramic; ceramic mater; /264/

Citation Formats

Holcombe, Cressie E, and Dykes, Norman L. Method of sintering ceramic materials. United States: N. p., 1992. Web.
Holcombe, Cressie E, & Dykes, Norman L. Method of sintering ceramic materials. United States.
Holcombe, Cressie E, and Dykes, Norman L. Wed . "Method of sintering ceramic materials". United States. https://www.osti.gov/servlets/purl/868541.
@article{osti_868541,
title = {Method of sintering ceramic materials},
author = {Holcombe, Cressie E and Dykes, Norman L},
abstractNote = {A method for sintering ceramic materials is described. A ceramic article is coated with layers of protective coatings such as boron nitride, graphite foil, and niobium. The coated ceramic article is embedded in a container containing refractory metal oxide granules and placed within a microwave oven. The ceramic article is heated by microwave energy to a temperature sufficient to sinter the ceramic article to form a densified ceramic article having a density equal to or greater than 90% of theoretical density.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {Wed Jan 01 00:00:00 EST 1992},
month = {Wed Jan 01 00:00:00 EST 1992}
}

Works referenced in this record:

Tensile and compressive properties of flexible graphite foils
journal, January 1986


Unusual properties of microwave-sintered yttria-2wt% zirconia
journal, August 1988


Enhanced Thermal Shock Properties of Y 2 O 3 -2 WT.% ZrO 2 Heated Using 2.45 Ghz Radiation
journal, January 1988