Silicon nitride/silicon carbide composite densified materials prepared using composite powders

Dunmead, Stephen D; Weimer, Alan W; Carroll, Daniel F; Eisman, Glenn A; Cochran, Gene A; Susnitzky, David W; Beaman, Donald R; Nilsen, Kevin J

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Title: Silicon nitride/silicon carbide composite densified materials prepared using composite powders

Abstract

Prepare silicon nitride-silicon carbide composite powders by carbothermal reduction of crystalline silica powder, carbon powder and, optionally, crystalline silicon nitride powder. The crystalline silicon carbide portion of the composite powders has a mean number diameter less than about 700 nanometers and contains nitrogen. The composite powders may be used to prepare sintered ceramic bodies and self-reinforced silicon nitride ceramic bodies.

Inventors:

Dunmead, Stephen D ^[1]; Weimer, Alan W ^[1]; Carroll, Daniel F ^[1]; Eisman, Glenn A ^[1]; Cochran, Gene A ^[1]; Susnitzky, David W ^[1]; Beaman, Donald R ^[1]; Nilsen, Kevin J ^[1]

Midland, MI

Issue Date:: Tue Jul 01 00:00:00 EDT 1997

Research Org.:: Lawrence Livermore National Laboratory (LLNL), Livermore, CA (United States)

OSTI Identifier:: 871028

Patent Number(s):: 5643843

Application Number:: 08/678199

Assignee:: Dow Chemical Company (Midland, MI)

Patent Classifications (CPCs):: B - PERFORMING OPERATIONS B82 - NANOTECHNOLOGY B82Y - SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES

C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01B - NON-METALLIC ELEMENTS

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B - PERFORMING OPERATIONS B82 - NANOTECHNOLOGY B82Y - SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES
B82Y30/00 - Nanotechnology for materials or surface science, e.g. nanocomposites

C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01B - NON-METALLIC ELEMENTS
C01B21/0685 - {Preparation by carboreductive nitridation}

C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01P - INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
C01P2004/62 - Submicrometer sized, i.e. from 0.1-1 micrometer
C01P2004/64 - Nanometer sized, i.e. from 1-100 nanometer
C01P2006/10 - Solid density
C01P2006/12 - Surface area

C - CHEMISTRY C04 - CEMENTS C04B - LIME, MAGNESIA
C04B35/584 - based on silicon nitride
C04B35/593 - obtained by pressure sintering

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DOE Contract Number:: 86X-SK761C

Resource Type:: Patent

Country of Publication:: United States

Language:: English

Subject:: silicon; nitride; carbide; composite; densified; materials; prepared; powders; prepare; nitride-silicon; carbothermal; reduction; crystalline; silica; powder; carbon; optionally; portion; mean; diameter; 700; nanometers; contains; nitrogen; sintered; ceramic; bodies; self-reinforced; silica powder; carbide composite; nitride powder; silicon nitride; silicon carbide; crystalline silicon; sintered ceramic; carbon powder; composite powders; ceramic bodies; nitride ceramic; carbide portion; carbothermal reduction; crystalline silica; materials prepared; silicon nitride-; silicon nitride-silicon; nitride-silicon carbide; contains nitrogen; -silicon carbide; prepare silicon; /501/

Citation Formats


                    Dunmead, Stephen D, Weimer, Alan W, Carroll, Daniel F, Eisman, Glenn A, Cochran, Gene A, Susnitzky, David W, Beaman, Donald R, and Nilsen, Kevin J. Silicon nitride/silicon carbide composite densified materials prepared using composite powders.  United States: N. p., 1997. 
        Web.

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                    Dunmead, Stephen D, Weimer, Alan W, Carroll, Daniel F, Eisman, Glenn A, Cochran, Gene A, Susnitzky, David W, Beaman, Donald R, & Nilsen, Kevin J. Silicon nitride/silicon carbide composite densified materials prepared using composite powders.  United States.

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                    Dunmead, Stephen D, Weimer, Alan W, Carroll, Daniel F, Eisman, Glenn A, Cochran, Gene A, Susnitzky, David W, Beaman, Donald R, and Nilsen, Kevin J. Tue .  
        "Silicon nitride/silicon carbide composite densified materials prepared using composite powders".  United States.  https://www.osti.gov/servlets/purl/871028.

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@article{osti_871028,

  title        = {Silicon nitride/silicon carbide composite densified materials prepared using composite powders},

  author       = {Dunmead, Stephen D and Weimer, Alan W and Carroll, Daniel F and Eisman, Glenn A and Cochran, Gene A and Susnitzky, David W and Beaman, Donald R and Nilsen, Kevin J},

  abstractNote = {Prepare silicon nitride-silicon carbide composite powders by carbothermal reduction of crystalline silica powder, carbon powder and, optionally, crystalline silicon nitride powder. The crystalline silicon carbide portion of the composite powders has a mean number diameter less than about 700 nanometers and contains nitrogen. The composite powders may be used to prepare sintered ceramic bodies and self-reinforced silicon nitride ceramic bodies.},

  doi          = {},

  journal      = {},
number       = ,

  volume       = ,

  place        = {United States},

  year         = {Tue Jul 01 00:00:00 EDT 1997},

  month        = {Tue Jul 01 00:00:00 EDT 1997}

}

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Works referenced in this record:

Synthetic Raw Materials for Ceramics
book, January 1989

Nagai, Akira; Kimura, Yoshitaka
Advanced Technical Ceramics
https://doi.org/10.1016/B978-0-12-654630-9.50007-3

Mechanical Properties and Microstructure of Si₃N₄ Matrix Composite with Nano-Meter Scale SiC Particles
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Sasaki, Gen; Nakase, Hirofumi; Suganuma, Katsuaki
Journal of the Ceramic Society of Japan, Vol. 100, Issue 1160
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On the Preparation of Fine Silicon Nitride Powders
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Schwier, G.
Progress in Nitrogen Ceramics
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Influence of Starting Powder Characteristics on Mechanical Properties of SiC-particle/Si₃N₄ Composites
journal, January 1992

Akimune, Yoshio; Ogasawara, Toshio; Hirosaki, Naoto
Journal of the Ceramic Society of Japan, Vol. 100, Issue 1160
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Silicon Nitride: Relations between Powder Characteristics and Sinterability
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Cambier, F.; Leriche, A.; Gilbart, E.
The Physics and Chemistry of Carbides, Nitrides and Borides
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SiC-Si ₃N₄ Gradient Composite Ceramics by Special Hip Processing
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Dongliang, Jiang; Jihong, She; Shouhong, Tan
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Comparison of the Surface Charge Behavior of Commercial Silicon Nitride and Silicon Carbide Powders
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Adsorption of Gases in Multimolecular Layers
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Reactions within quartz-carbon mixtures in a nitrogen atmosphere
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Computer-Assisted Microscopy
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Russ, John C.
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Synthesis of nitrogen ceramic povvders by carbothermal reduction and nitridation Part 1 Silicon nitride
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Cho, Y. W.; Charles, J. A.
Materials Science and Technology, Vol. 7, Issue 4
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Synthesis of Silicon Nitride Powder from Silica Reduction
journal, December 1982

Inoue, Hiroshi; Komeya, Katsutoshi; Tsuge, Akihiko
Journal of the American Ceramic Society, Vol. 65, Issue 12
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A Comparative Study of Three Silicon Nitride Powders, Obtained by Three Different Syntheses
journal, August 1993

van Dijen, F. K.; Kerber, A.; Vogt, Uwe
Key Engineering Materials, Vol. 89-91
https://doi.org/10.4028/www.scientific.net/KEM.89-91.19

Preparation of Silicon Nitride from Silica
journal, October 1984

Zhang, Shi-Chang; Cannon, W. Roger
Journal of the American Ceramic Society, Vol. 67, Issue 10
https://doi.org/10.1111/j.1151-2916.1984.tb19684.x

Synthesis of silicon nitride by carbothermal reduction and nitriding of silica: Control of kinetics and morphology
journal, January 1992

Ličko, T.; Figusch, V.; Púchyová, J.
Journal of the European Ceramic Society, Vol. 9, Issue 3
https://doi.org/10.1016/0955-2219(92)90008-2

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Title: Silicon nitride/silicon carbide composite densified materials prepared using composite powders

Abstract

Citation Formats

Synthetic Raw Materials for Ceramics book, January 1989

Mechanical Properties and Microstructure of Si3N4 Matrix Composite with Nano-Meter Scale SiC Particles journal, January 1992

On the Preparation of Fine Silicon Nitride Powders book, January 1983

Influence of Starting Powder Characteristics on Mechanical Properties of SiC-particle/Si3N4 Composites journal, January 1992

Silicon Nitride: Relations between Powder Characteristics and Sinterability book, January 1990

SiC-Si 3N4 Gradient Composite Ceramics by Special Hip Processing book, January 1992

Comparison of the Surface Charge Behavior of Commercial Silicon Nitride and Silicon Carbide Powders journal, December 1988

Adsorption of Gases in Multimolecular Layers journal, February 1938

Reactions within quartz-carbon mixtures in a nitrogen atmosphere journal, January 1992

Computer-Assisted Microscopy book, January 1990

Synthesis of nitrogen ceramic povvders by carbothermal reduction and nitridation Part 1 Silicon nitride journal, April 1991

Synthesis of Silicon Nitride Powder from Silica Reduction journal, December 1982

A Comparative Study of Three Silicon Nitride Powders, Obtained by Three Different Syntheses journal, August 1993

Preparation of Silicon Nitride from Silica journal, October 1984

Synthesis of silicon nitride by carbothermal reduction and nitriding of silica: Control of kinetics and morphology journal, January 1992

Synthetic Raw Materials for Ceramics
book, January 1989

Mechanical Properties and Microstructure of Si₃N₄ Matrix Composite with Nano-Meter Scale SiC Particles
journal, January 1992

On the Preparation of Fine Silicon Nitride Powders
book, January 1983

Influence of Starting Powder Characteristics on Mechanical Properties of SiC-particle/Si₃N₄ Composites
journal, January 1992

Silicon Nitride: Relations between Powder Characteristics and Sinterability
book, January 1990

SiC-Si ₃N₄ Gradient Composite Ceramics by Special Hip Processing
book, January 1992

Comparison of the Surface Charge Behavior of Commercial Silicon Nitride and Silicon Carbide Powders
journal, December 1988

Adsorption of Gases in Multimolecular Layers
journal, February 1938

Reactions within quartz-carbon mixtures in a nitrogen atmosphere
journal, January 1992

Computer-Assisted Microscopy
book, January 1990

Synthesis of nitrogen ceramic povvders by carbothermal reduction and nitridation Part 1 Silicon nitride
journal, April 1991

Synthesis of Silicon Nitride Powder from Silica Reduction
journal, December 1982

A Comparative Study of Three Silicon Nitride Powders, Obtained by Three Different Syntheses
journal, August 1993

Preparation of Silicon Nitride from Silica
journal, October 1984

Synthesis of silicon nitride by carbothermal reduction and nitriding of silica: Control of kinetics and morphology
journal, January 1992