Apparatus for producing nanoscale ceramic powders
Abstract
An apparatus provides high temperature and short residence time conditions for the production of nanoscale ceramic powders. The apparatus includes a confinement structure having a multiple inclined surfaces for confining flame located between the surfaces so as to define a flame zone. A burner system employs one or more burners to provide flame to the flame zone. Each burner is located in the flame zone in close proximity to at least one of the inclined surfaces. A delivery system disposed adjacent the flame zone delivers an aerosol, comprising an organic or carbonaceous carrier material and a ceramic precursor, to the flame zone to expose the aerosol to a temperature sufficient to induce combustion of the carrier material and vaporization and nucleation, or diffusion and oxidation, of the ceramic precursor to form pure, crystalline, narrow size distribution, nanophase ceramic particles.
- Inventors:
-
- Andover, MA
- Windham, NH
- Little Compton, RI
- Issue Date:
- OSTI Identifier:
- 870053
- Patent Number(s):
- 5447708
- Application Number:
- 08/061,069
- Assignee:
- Physical Sciences, Inc. (Andover, MA)
- Patent Classifications (CPCs):
-
B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01J - CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY
B - PERFORMING OPERATIONS B82 - NANOTECHNOLOGY B82Y - SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES
- Resource Type:
- Patent
- Country of Publication:
- United States
- Language:
- English
- Subject:
- apparatus; producing; nanoscale; ceramic; powders; provides; temperature; residence; time; conditions; production; confinement; structure; multiple; inclined; surfaces; confining; flame; located; define; zone; burner; employs; burners; provide; close; proximity; delivery; disposed; adjacent; delivers; aerosol; comprising; organic; carbonaceous; carrier; material; precursor; expose; sufficient; induce; combustion; vaporization; nucleation; diffusion; oxidation; form; pure; crystalline; narrow; size; distribution; nanophase; particles; narrow size; inclined surface; inclined surfaces; ceramic powder; apparatus provides; ceramic powders; size distribution; residence time; disposed adjacent; ceramic particles; close proximity; temperature sufficient; ceramic precursor; carrier material; ceramic particle; nanoscale ceramic; phase ceramic; multiple inclined; nanophase ceramic; time conditions; producing nanoscale; confinement structure; /423/501/
Citation Formats
Helble, Joseph J, Moniz, Gary A, and Morse, Theodore F. Apparatus for producing nanoscale ceramic powders. United States: N. p., 1995.
Web.
Helble, Joseph J, Moniz, Gary A, & Morse, Theodore F. Apparatus for producing nanoscale ceramic powders. United States.
Helble, Joseph J, Moniz, Gary A, and Morse, Theodore F. Sun .
"Apparatus for producing nanoscale ceramic powders". United States. https://www.osti.gov/servlets/purl/870053.
@article{osti_870053,
title = {Apparatus for producing nanoscale ceramic powders},
author = {Helble, Joseph J and Moniz, Gary A and Morse, Theodore F},
abstractNote = {An apparatus provides high temperature and short residence time conditions for the production of nanoscale ceramic powders. The apparatus includes a confinement structure having a multiple inclined surfaces for confining flame located between the surfaces so as to define a flame zone. A burner system employs one or more burners to provide flame to the flame zone. Each burner is located in the flame zone in close proximity to at least one of the inclined surfaces. A delivery system disposed adjacent the flame zone delivers an aerosol, comprising an organic or carbonaceous carrier material and a ceramic precursor, to the flame zone to expose the aerosol to a temperature sufficient to induce combustion of the carrier material and vaporization and nucleation, or diffusion and oxidation, of the ceramic precursor to form pure, crystalline, narrow size distribution, nanophase ceramic particles.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {1995},
month = {1}
}
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Works referenced in this record:
Ultrafine BaPb1-xBixO3 powders prepared by the spray-ICP technique
journal, June 1987
- Ono, Tomoshige; Kagawa, Masahiro; Syono, Yasuhiko
- Plasma Chemistry and Plasma Processing, Vol. 7, Issue 2
Production of ultrafine metal oxide aerosol particles by thermal decomposition of metal alkoxide vapors
journal, December 1986
- Okuyama, Kikuo; Kousaka, Yasuo; Tohge, Noboru
- AIChE Journal, Vol. 32, Issue 12
Synthesis, characterization, and properties of nanophase TiO 2
journal, December 1988
- Siegel, R. W.; Ramasamy, S.; Hahn, H.
- Journal of Materials Research, Vol. 3, Issue 6
Research opportunities on clusters and cluster-assembled materials—A Department of Energy, Council on Materials Science Panel Report
journal, June 1989
- Andres, R. P.; Averback, R. S.; Brown, W. L.
- Journal of Materials Research, Vol. 4, Issue 3
Aggregation and growth of submicron oxide particles in flames
journal, May 1982
- Ulrich, Gail D.; Rieh, John W.
- Journal of Colloid and Interface Science, Vol. 87, Issue 1
Basic research needs on high temperature ceramics for energy applications
journal, June 1980
- Bowen, H. Kent
- Materials Science and Engineering, Vol. 44, Issue 1
Production of Monodispersed Colloidal Particles
journal, August 1985
- Matijevic, Egon
- Annual Review of Materials Science, Vol. 15, Issue 1
Effects of solute ion and grain size on superplasticity of ZrO2 polycrystals
journal, January 1991
- Wakai, Fumihiro; Nagano, Takayuki
- Journal of Materials Science, Vol. 26, Issue 1
Overview Of Fiber Optic Research At Brown University
conference, February 1990
- Morse, T. F.
- OE/FIBERS '89, SPIE Proceedings
Synthesis of Solid, Spherical Zirconia Particles by Spray Pyrolysis
journal, January 1990
- Zhang, Shi-Chang; Messing, Gary L.; Borden, Michael
- Journal of the American Ceramic Society, Vol. 73, Issue 1
Experimental control of ultrafine TiO2 particle generation from thermal decomposition of titanium tetraisopropoxide vapor
journal, January 1989
- Okuyama, Kikuo; Jeung, Ji-Taek; Kousaka, Yasuo
- Chemical Engineering Science, Vol. 44, Issue 6
Nanometer Oxide Ceramic Particles With Controlled Agglomeration
journal, March 1991
- Helble, Joseph
- Materials and Processing Report, Vol. 5, Issue 12
Factors determining the primary particle size of flame-generated inorganic aerosols
journal, March 1989
- Helble, Joseph J.; Sarofim, Adel F.
- Journal of Colloid and Interface Science, Vol. 128, Issue 2
Aerosol flow reactor production of fine Y 1 Ba 2 Cu 3 O 7 powder: Fabrication of superconducting ceramics
journal, May 1988
- Kodas, T. T.; Engler, E. M.; Lee, V. Y.
- Applied Physics Letters, Vol. 52, Issue 19
Laser Synthesis of Si/C/N Powders from 1,1,1,3,3,3-Hexamethyldisilazane
journal, August 1986
- Rice, Gary W.
- Journal of the American Ceramic Society, Vol. 69, Issue 8