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Title: Device and methods for determination of molecular weight distributions of polymers and distributions of other polymer properties without physical separation

Abstract

Devices and methods for determining the cumulative distribution of a polymer property in a reactor without physical separation of reaction subcomponents. The device includes a means of measuring an instantaneous property of the polymers being produced in a reaction vessel a plurality of times during a polymerization reaction as well as a means of determining the corresponding change in polymer concentration in the reaction vessel between measurements of the instantaneous polymer property The device also includes a means of computing a statistical distribution appropriate to the polymer characteristic and applying the statistical distribution to a recently measured instantaneous value of the polymer property so as to have an instantaneous distribution of the polymer property and a means of adding together the instantaneous distributions of the polymer property in order to obtain the cumulative distribution of the polymer property in the reactor.

Inventors:
; ; ;
Issue Date:
Research Org.:
Advanced Polymer Monitoring Technologies, Inc., New Orleans, LA (United States); Tulane Univ., New Orleans, LA (United States)
Sponsoring Org.:
USDOE
OSTI Identifier:
1986712
Patent Number(s):
11474044
Application Number:
16/094,542
Assignee:
Advanced Polymer Monitoring Technologies, Inc. (New Orleans, LA); Administrators of the Tulane Educational Fund (New Orleans, LA)
DOE Contract Number:  
EE0005776
Resource Type:
Patent
Resource Relation:
Patent File Date: 04/21/2017
Country of Publication:
United States
Language:
English

Citation Formats

Reed, Wayne Frederick, Montgomery, Rick D., Drenski, Michael Felix, and Wu, Aide. Device and methods for determination of molecular weight distributions of polymers and distributions of other polymer properties without physical separation. United States: N. p., 2022. Web.
Reed, Wayne Frederick, Montgomery, Rick D., Drenski, Michael Felix, & Wu, Aide. Device and methods for determination of molecular weight distributions of polymers and distributions of other polymer properties without physical separation. United States.
Reed, Wayne Frederick, Montgomery, Rick D., Drenski, Michael Felix, and Wu, Aide. Tue . "Device and methods for determination of molecular weight distributions of polymers and distributions of other polymer properties without physical separation". United States. https://www.osti.gov/servlets/purl/1986712.
@article{osti_1986712,
title = {Device and methods for determination of molecular weight distributions of polymers and distributions of other polymer properties without physical separation},
author = {Reed, Wayne Frederick and Montgomery, Rick D. and Drenski, Michael Felix and Wu, Aide},
abstractNote = {Devices and methods for determining the cumulative distribution of a polymer property in a reactor without physical separation of reaction subcomponents. The device includes a means of measuring an instantaneous property of the polymers being produced in a reaction vessel a plurality of times during a polymerization reaction as well as a means of determining the corresponding change in polymer concentration in the reaction vessel between measurements of the instantaneous polymer property The device also includes a means of computing a statistical distribution appropriate to the polymer characteristic and applying the statistical distribution to a recently measured instantaneous value of the polymer property so as to have an instantaneous distribution of the polymer property and a means of adding together the instantaneous distributions of the polymer property in order to obtain the cumulative distribution of the polymer property in the reactor.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {Tue Oct 18 00:00:00 EDT 2022},
month = {Tue Oct 18 00:00:00 EDT 2022}
}

Works referenced in this record:

Method and apparatus for digitizing a wide frequency bandwidth signal
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Method and Apparatus for Reducing the Contribution of Noise to Digitally Sampled Signals
patent-application, September 2011