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Title: Procedures for the synthesis of ethylenediamine bisborane and ammonia borane

A method for synthesizing ammonia borane includes (a) preparing a reaction mixture in one or more solvents, the reaction mixture containing sodium borohydride, at least one ammonium salt, and ammonia; and (b) incubating the reaction mixture at temperatures between about 0.degree. C. to about room temperature in an ambient air environment under conditions sufficient to form ammonia borane. Methods for synthesizing ethylenediamine bisborane, and methods for dehydrogenation of ethylenediamine bisborane are also described.
Inventors:
; ; ;
Issue Date:
OSTI Identifier:
1338064
Assignee:
PURDUE RESEARCH FOUNDATION (West Lafayette, IN) GFO
Patent Number(s):
9,534,002
Application Number:
13/809,316
Contract Number:
FG36-06GO86050
Resource Relation:
Patent File Date: 2011 Jul 06
Research Org:
PURDUE RESEARCH FOUNDATION, West Lafayette, IN (United States)
Sponsoring Org:
USDOE
Country of Publication:
United States
Language:
English
Subject:
37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY; 54 ENVIRONMENTAL SCIENCES

Other works cited in this record:

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