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Radioactive iodine capture in silver-containing mordenites through nanoscale silver iodide formation.

Journal Article · · J. Am. Chem. Soc.
DOI:https://doi.org/10.1021/ja103110y· OSTI ID:983470

The effective capture and storage of radiological iodine ({sup 129}I) remains a strong concern for safe nuclear waste storage and safe nuclear energy. Silver-containing mordenite (MOR) is a longstanding benchmark for iodine capture; however, the molecular level understanding of this process needed to develop more effective iodine getters has remained elusive. Here we probe the structure and distribution of iodine sorbed by silver-containing MOR using differential pair distribution function analysis. While iodine is distributed between {gamma}-AgI nanoparticles on the zeolite surface and subnanometer {alpha}-AgI clusters within the pores for reduced silver MOR, in the case of unreduced silver-exchanged MOR, iodine is exclusively confined to the pores as subnanometer {alpha}-AgI. Consequently, unreduced silver-containing zeolites may offer a more secure route for radioactive iodine capture, with the potential to more effectively trap the iodine for long-term storage.

Research Organization:
Argonne National Laboratory (ANL)
Sponsoring Organization:
SC; NNSA
DOE Contract Number:
AC02-06CH11357
OSTI ID:
983470
Report Number(s):
ANL/XSD/JA-67093
Journal Information:
J. Am. Chem. Soc., Journal Name: J. Am. Chem. Soc. Journal Issue: 26 ; 2010 Vol. 132; ISSN 0002-7863; ISSN 1520-5126
Country of Publication:
United States
Language:
ENGLISH