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Trace Explosive Detection using Photothermal Deflection Spectroscopy

Journal Article · · Journal of Applied Physics
DOI:https://doi.org/10.1063/1.2908181· OSTI ID:966728

Satisfying the conditions of high sensitivity and high selectivity using portable sensors that are also reversible is a challenge. Miniature sensors such as microcantilevers offer high sensitivity but suffer from poor selectivity due to the lack of sufficiently selective receptors. Although many of the mass deployable spectroscopic techniques provide high selectivity, they do not have high sensitivity. Here, we show that this challenge can be overcome by combining photothermal spectroscopy on a bimaterial microcantilever with the mass induced change in the cantilever's resonance frequency. Detection using adsorption-induced resonant frequency shift together with photothermal deflection spectroscopy shows extremely high selectivity with a subnanogram limit of detection for vapor phase adsorbed explosives, such as pentaerythritol tetranitrate (PETN), cyclotrimethylene trinitramine (RDX), and trinitrotoluene (TNT).

Research Organization:
Oak Ridge National Laboratory (ORNL)
Sponsoring Organization:
ORNL work for others
DOE Contract Number:
AC05-00OR22725
OSTI ID:
966728
Journal Information:
Journal of Applied Physics, Journal Name: Journal of Applied Physics Journal Issue: 9 Vol. 103; ISSN JAPIAU; ISSN 0021-8979
Country of Publication:
United States
Language:
English

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